• Journal of environmental and Sanitary engineering
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• v.11 no.1
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• pp.63-70
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• 1996

The synthesis of high purity and ultra-fine $BaTiO_3$ by precipitation with gaseous $NH_3$ as precipitator was investigated to find an alternative process to solve various problems of recent wet methods. A synthesis process for $BaTiO_3$ powder using $NH_3$ gas as a precipitator in a bubble column reactor was experimentally successful in developing the production process of piezoelectric ceramic $BaTiO_3$ powder. And a 2.33m1/sec is approprite for the feed flow rate, $BaTiO_3$ powder produced under above the condition is spherical type, its particle size was about $0.2{\mu}m$.

• Journal of the Korean Society for Precision Engineering
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• v.31 no.1
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• pp.75-81
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• 2014

Laser beam machining has been known as efficient for glass micromachining. It is usually used the ultra-short pulsed laser which is time-consuming and uneconomic process. In order to use economic and powerful long pulsed laser, indirect processing called laser-induced backside wet etching (LIBWE) is good alternative method. In this paper, micromachining of glass using Nd:YAG laser with nanosecond pulsed beam has been attempted. In order to improve shape accuracy, combined processing with magnetic stirrer has been widely used. Magnetic stirrer acts to circulate the solution and remove the bubble but it is not suitable for deep hole machining. To get better effect, ultrasonic vibration was applied for improving shape accuracy.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2004.10a
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• pp.709-713
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• 2004

Characteristics of laser-assisted wet etching of titanium in phosphoric acid were investigated to examine the feasibility of this method for fabrication of high aspect ratio microchannels. Laser power, number of scans, etchant concentration, position of beam waist and scanning speed were taken into consideration as the major process parameters exerting the temperature distribution and the cross sectional profile of etched channels. Experimental results indicated that laser power influences on both etch width and depth while number of scans and scanning speed mainly affect on the etch depth. At a low etchant concentration, the cross sectional profile of an etched channel becomes a U-shape but it gradually turns into a V-shape as the concentration increases. On the other hand, surface of the laser beam focus with respect to the sample surface is found to be a key factor determining the bubble dynamics and thus the process stability. It is demonstrated that metallic microchannels with different cross sectional profiles can be fabricated by properly controlling the process parameters. Microchannels of aspect ratio up to 8 with the width and depth ranges of 8∼32 m and 50∼300 m, respectively, were fabricated.

• Journal of the Korean Ceramic Society
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• v.56 no.5
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• pp.513-520
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• 2019

This study reports the improvement of mechanical properties of Al₂O₃ porous ceramics from colloidal suspension with the addition of carbon fiber by direct foaming. The initial colloidal suspension of Al₂O₃ was partially hydrophobized by surfactant to stabilize wet foam with the addition of carbon fiber from 2 to 8 wt% as stabilizer. The influence of carbon fiber on the air content, bubble size, pore size and pore distribution in terms of wet foam stability and physical properties of porous ceramics were discussed. The viscosity of the colloidal suspension was increased giving solid like properties with the increased in carbon fiber content. The mechanical properties of the sintered porous samples were investigated by Hertzian indentation test. The results show the wet foam stability of more than 90% corresponds to compressive loading of 156.48 N and elastic modulus of 57.44 MPa of sintered sample with 8 wt% of carbon fiber content.

• Journal of the Korean Ceramic Society
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• v.53 no.6
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• pp.604-609
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• 2016

This study reports on wet-foam stability with respect to porous ceramics from a particle-stabilized colloidal suspension that is achieved through the addition of polymethyl methacrylate (PMMA) using a wet process. To stabilize the wet foam, an initial colloidal suspension of $Al_2O_3$ was partially hydrophobized by the surfactant propyl gallate (2 wt.%) and $SiO_2$ was added as a stabilizer. The influence of the PMMA content on the bubble size, pore size, and pore distribution in terms of the contact angle, surface tension, adsorption free energy, and Laplace pressure are described in this paper. The results show a wet-foam stability of more than 83%, which corresponds to a particle free energy of $2.7{\times}10^{-12}J$ and a pressure difference of 61.1 mPa for colloidal particles with 20 wt.% of PMMA beads. It was possible to control the uniform distribution of the open/closed pores by increasing the PMMA content and by adding thick struts, leading to the achievement of a higher-stability wet foam for use in porous ceramics.

• Journal of the Korean Ceramic Society
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• v.56 no.3
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• pp.211-232
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• 2019

Porous ceramics are promising materials for a number of functional and structural applications that include thermal insulation, filters, bio-scaffolds for tissue engineering, and preforms for composite fabrication. These applications take advantage of the special characteristics of porous ceramics, such as low thermal mass, low thermal conductivity, high surface area, controlled permeability, and low density. In this review, we emphasize the direct foaming method, a simple and versatile approach that allows the fabrication of porous ceramics with tailored microstructure, along with distinctive properties. The wet foam stability is achieved under the controlled addition of amphiphiles to the colloidal suspension, which induce in situ hydrophobization, allowing the wet foam to resist coarsening and Ostwald ripening upon drying and sintering. Different components, like contact angle, adsorption free energy, air content, bubble size, and Laplace pressure, play vital roles in the stabilization of the particle stabilized wet foam to the porous ceramics. The mechanical behavior of the load-displacements curves of sintered samples was investigated using Herzian indentations testes. From the collected results, we found that microporous structures with pore sizes from 30 ㎛ to 570 ㎛ and the porosity within the range from 70% to 85%.

• Journal of Environmental Science International
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• v.29 no.11
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• pp.1025-1032
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• 2020

This work was performed to develop a dip injection wet scrubber (DIWS) system with chlorine dioxide as the oxidant. The exhaust pollutants from a lime kiln of paper-mill were introduced to the system. When NaClO₃ was used to oxidize NO into NO₂, the oxidation was unsatisfactory and the combination of HNO₃ or H₂SO₄ was required for 100% oxidation. ClO₂ is recommended to oxidize NO and SO₂ effectively. With the combination of 1^st stage of DIWS and ClO₂, 57.1% of NOx and 98% of SO₂ were effectively removed. In the case of 2^nd stage of DIWS and ClO₂, 93.5% of NOx and 99% of SO₂ were removed. The ClO₂+DIWS process was superior to the ClO₂+Scrubber process in terms of investment, running cost and NOx removal efficiency.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.20 no.10
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• pp.1-8
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• 2021

Cylinder liners used in diesel engines of combat equipment are prone to cavitation due to wet cooling. The damage caused by erosion and corrosion due to cavitation has a fatal effect on the performance and lifespan of a diesel engine. Therefore, a study was conducted to improve the durability of cylinder liners. Two surface treatment techniques were proposed: nitriding and chrome plating. It was observed that the amount of erosion on the surface of nitride-treated cylinder liners was high because the surface-treated part eroded due to its weak impact resistance against the bubble explosion generated by cavitation. In contrast, the chrome-plated cylinder liner had a lower amount of erosion among the specimens subjected to the accelerated test. These results verified that the resistance of chrome-plated liners against cavitation is high. Therefore, it can withstand the impact of bubble explosion. If the chrome plating thickness is set with reference to the KS standard, an exceptional durability of abrasion, wear resistance, and corrosion resistance can be obtained. If the thickness is set between 120~250㎛, it is expected that the durability of the cylinder liner can be improved. Although a recovery method for corroded cylinder liners is suggested, the proposed method has an inherent risk of crack generation. Therefore, further research is required to solve this problem.

• Nuclear Engineering and Technology
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• v.54 no.12
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• pp.4585-4600
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• 2022

A pool scrubber is often used as a wet-type design to mitigate the consequence of a severe nuclear accident. While studies indicated higher decontamination performance of a deeper pool, utilizing a very tall pool can be problematic due to potential structural stability and water backflow issues. This study proposes, as an alternative to a single pool system, a pool scrubber system composed of serially connected multiple pools with lower heights. Since large fraction of aerosol removal takes place in the injection region, serially connected pool scrubber system is expected to enhance the overall decontamination capability of a pool scrubber system. To support the analysis of the proposed system's decontamination capability, a new computer model was developed in the study to describe the bubble size dependent effect on aerosol removal including the effect of pool residence time. The accuracy of the new model was examined against experimental data for its validation. The proposed scrubber system composed of serially connected multiple shorter pools is found to have much improved decontamination performance over the current single pool system design.

• Journal of Wetlands Research
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• v.18 no.3
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• pp.286-291
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• 2016

This study was carried out to evaluate the feasibility of air-stripping by DIWS(Dip Injection Wet Scrubber) system on high concentration of ammonia wastewater more than 10,000 mg/L. In the case of changing temperature from $30^{\circ}C$ to $70^{\circ}C$ maintaining pH 12.5 within the 72 hours, the removal efficiency of T-N by the present treatment plant was increased to 90.5% which was initially kept 70.3%. Although the high concentration of T-N with 9,120~12,955 mg/L was treated by micro-bubble through DIWS system maintaining the temperature of $30^{\circ}C$ within the 20 hours, the removal efficiency of T-N reached 91.9%, which indicated the possibility of air-stripping.