• 한국해안·해양공학회논문집
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• 제29권5호
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• pp.239-246
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• 2017

현장에서 파고와 주기만을 관측한 경우 주로 개별파 분석법을 사용하여 다양한 파랑 특성을 산정한다. 본 논문에서는 MATLAB 언어를 이용하여 개별파 분석 프로그램을 개발하였다. 영점 상향 교차법과 영점 하향 교차법을 이용하여 1) 평균해면 보정, 2) 영점 교차 시간 산정, 3) 개별파고 산정, 4) 자료 관측기간 변화 등의 기능을 수행할 수 있다. 해모수 1호에 설치된 레이더(WaveGuide Radar)를 사용하여 관측된 시간간격 0.2초 자료를 대상으로 개발된 프로그램의 적용성을 검토하였다. 조석성분 제거 및 영점 교차 시간 산정은 선형 혹은 2차원으로 내삽하였다. 개별 파고 산정은 Goda 방법이 적정한 것으로 판단되었으며, 본 연구에서 제안한 방법은 차후 후속 연구를 통하여 개선할 여지가 있는 것으로 판단된다. 대표파의 특징은 샘플의 유한성 등으로 인하여 영점상향교차법과 영점하향교차법으로 산정한 결과가 상이하다는 것을 알 수 있다.

• 한국염색가공학회지
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• 제5권4호
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• pp.29-41
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• 1993

In order to surface Hydrophobilization of Poly(ethylene terephthalate) (PET) fiber samples were treated in the atmosphere of CF$_{4}$ or $C_{2}$F$_{6}$glow discharge. The sample used in this study was PET film which is 75$\mu$m thick made by Teijin, O-Type(Japan). The cleaned samples were placed in plasma reactor made of pyrex glass cylinder, and plasma processing was carried out by glow discharge of CF$_{4}$ or $C_{2}$F$_{6}$ gas, being continuously fed by gas flow and continuously pumped out by a vacuum system. Electric power source for generate plasma state was sustained alternating current(60Hz) and voltage was sustained 600 volt. The duration of plasma treatment varied from 15 to 120 seconds except special case, the monomer gase pressure varied from 0.02 to 0.3 Torr and power range was 10 to 90 watts. The hydrophobic features of changed PET surface were evaluated by contact angle measurement and surface chemical characteristics were analyzed by ESCA. Results can be summerized as follows. 1. The most favorable setting position of substrate was the center area between the two electrodes. 2. $C_{2}$F$_{6}$ discharge current was lower than that of CF$_{4}$ when same voltage was sustained. Treated efficiency between CF$_{4}$ and $C_{2}$F$_{6}$ did not revealed significant differences under same electric power(wattage). 3. When monomer pressure is very low below 0.02 torr, as though substrate is exposed to CF$_{4}$ or $C_{2}$F$_{6}$ plasma, it tend to be hydrophilic through a little of fluorine bond and a great deal of oxidizing reaction. 4. There brought good hydrophobilization when monomer pressure was more 0.1 torr and duration of glow discharge treatment was over 45 seconds. When monomer pressure was too high, discharge current became low. Although prolong the duration, there was no more high hydrophobilization. 5. According to ESCA analysis, there were a little CF bond and a prevailing CF$_{2}$ bond in CF$_{4}$-treated substrate. There were CF$_{3}$, a little CF and a prevailing CF$_{2}$ bond in $C_{2}$F$_{6}$-treated substrate.d substrate.

• 한국환경농학회지
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• 제36권4호
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• pp.288-292
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• 2017

BACKGROUND: Silicon tetrachloride reacts with moisture in the atmosphere to generate hydrogen chloride, which affects the environment. Since silicon tetrachloride and its by-products are dispersed in the atmosphere in a short time after the silicon tetrachloride release into the atmosphere, it is difficult to directly assess the extent of environmental impact. In the present study, the exposure test of silicon tetrachloride or hydrogen chloride was examined in order to establish the criterion of the range affected by the silicon tetrachloride release, and the actual crops in the area exposed to silicon tetrachloride leakage were analyzed. METHODS AND RESULTS: For the experiment of exposure to silicon tetrachloride or hydrogen chloride, the leaves of red-pepper and corn were used in glass sealed containers. In the actual accident area, 59 samples from 10 different kinds of crops were collected. The pretreatment of the sample was performed by freezing and grinding, and then extracted using distilled water. The pH and concentration of chloride ($Cl^-$) ion of the extracted solution were measured using pH meter and ion chromatograph, respectively. CONCLUSION: Exposure to silicon tetrachloride caused visible damage, increasing the concentration of chloride ion, and decreasing the pH as well as hydrochloric acid. In the actual crops of the affected area, the tendency was the same as the result of the laboratory test, and the range of influence could be estimated through the concentration of $Cl^-$ ion over 2,000 mg/kg, and the correlation evaluation between the concentration of $Cl^-$ and pH. Therefore, the concentration of $Cl^-$ ion and the correlation between $Cl^-$ and pH would be considered as the factors to estimate the influence range of silicon tetrachloride release.

• 패션비즈니스
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• 제15권5호
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• pp.43-54
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• 2011

Digital Textile Printing(DTP) is appropriate for quick response system(QRS) and is closely connected with high value added fashion industry. Fashion products of high price are mainly silk and cotton. For high quality DTP products, it is important to optimize the parameters of media, pre and after-treatment, ink, printer, etc. DTP for these two fiber materials is also accompanied certainly with steaming as after-treatment process for coloration. Role of steam is like water in exhaustion dyeing. Steam can diffuse dye or ink in printing paste to fiber. Quality of DTP products depend on after-treatment processes such as steaming, washing, drying. Current production amount of DTP is smaller than one of conventional textile printing. However conventional after-treatment system has been using so far. This is mismatched with DTP in terms of process efficiency, spot work of small lot, quality control. In this study, continuous after-treatment system has been suitably designed for DTP that washing and drying are available after steaming. So, It is possible to improve efficiency of DTP process. Especially, the effects of after-treatment process, such as temperature of heat drum, steaming time on printability, color difference, color fastness were examined. Two types of samples(cotton knit and silk fabrics) were used. The results were obtained as follows : First, there is no a wide difference between the K/S values of cotton and silk treated with continuous after-treatment system and those of sample treated with conventional printing after-treatment method. So it is more effective to use the continuous after-treatment system than conventional printing after-treatment system in case of the daily throughput of 1,000 yards below. Second, after continuous after-treatment for DTP, K/S values were increased and lightness($L^*$) values were decreased. ${\Delta}E$ values were below 2.3. Third, DTP samples treated with continuous after-treatment system were tested for fastness(washing, light, rubbing). Grades of fastness(washing, light, rubbing) were above 3 grade.

• 한국식품과학회지
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• 제15권4호
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• pp.414-420
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• 1983

1. 김치의 주 산패균인 L. plantarum을 김치로부터 분리하고 내열성시험을 행한 결과 D 값은 $61{\sim}69.5^{\circ}C$에서 $1.08{\sim}0.18$분이었으며 z 값은 $10.5^{\circ}C$ 이었다. 2. 김치의 살균시 열전달 속도에 미치는 인자를 검토한 결과 탈기는 $80^{\circ}C$ 에서 10분, 두께는 $1{\sim}1.5cm$, 고형물대 국물비는 9 대 1 의 조건이 적정조건임을 알수 있었고, 밀봉시 가능한 한 봉입공기량이 최소로 되는 것이 바람직하였다. 3. 김치의 열확산도는 생김치일 때 $1.15{\times}10^{-3}cm^{2}/s$ 이었으나 탈기할수록 점차 증가하여 $80^{\circ}C$, 15분 탈기 하였을 때 $1.44{\times}10^{-3}cm^{2}/s$ 이었다. 4. 김치의 살균온도 및 시간에 따른 저장실험을 행한 결과 살균온도 $80{\sim}90^{\circ}C$ 에서는 10분 이상, $95^{\circ}C$ 에서 7분 이상의 조건이 장기보존 가능성을 나타내었다. 5. 회분열수식 살균기에서 파우치 김치를 살균할 때는 $95^{\circ}C$ 이상의 고온살균은 부적당한 것으로 판단되었으며, 열수의 공급과 회수 및 냉각수 공급시간이 김치의 살균에 큰 영향을 미쳤다.

• Restorative Dentistry and Endodontics
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• 제22권1호
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• pp.144-155
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• 1997

This study evaluated shear bond strength between porcelain and resin cement according to various surface treatments of porcelain, and surface condition of debonded porcelain. 50 porcelain specimens(Celay block A2M7) and composite resin specimens(Clearfil Photo-Bright) were prepared, and divided into 5 experimental groups according to the treatment method of porcelain surface. 5 experimental groups by surface treatments were as follows; CONTROL Group : No surface treatment was done on the surface of porcelains. SAND Group : The surface of porcelains were sandblasted with $50{\mu}m$ aluminum oxide for 5 seconds. HF Group: The surface of porcelains were etched with 8% Hydrofluoric acid for 4 minutes. SIL Group: The surface of porcelains were coated with silane coupling agent and heated at $100^{\circ}C$ for 5 minutes. SAND+HF+SIL Group : The surface of porcelains were sandblasted with $50{\mu}m$ aluminum oxide for 5 seconds and etched with 8% Hydrofluoric acid for 4 minutes, and coated with silane coupling agent and heated at $100^{\circ}C$ for 5 minutes. After surface treatments on the prepared porcelain surface two pastes of Panavia 21$^{(R)}$ were mixed, they were applied between composite resin block and porcelain surface, and then excessive resin cements were removed, and its margin was surrounded with Oxyguard II. All specimens were stored for 24 hours in water at $37^{\circ}C$ and tested with Instron testing machine between porcelains and resin cements, and debonded porcelain surfaces were observed under Scanning Electon Microscope(Hitachi S-2300) at 20kvp. The values from each group were compared statistically by Student's t-test. The obtained results were as follows; 1. The shear bond strength without surface treatment of porcelain was the lowest among all experimental groups(p<0.05). 2. The detached porcelain surface with sandblasting alone had more remarkable cracks than with only Hydrofluoric Acid or Silane coupling 2gent, but showed the lowest value of shear bond strength among surface treated groups(p<0.05), 3. When porcelain surface was treated by hydrofluoric acid, it affected shear bond strength more than silane coupling agent, but there were no significant statistical differences(p>0.05). 4. When three methods were combined to increase shear bond strength between porcelains and resin cements, its value was the highest than the others(p<0.05). 5. In Scannig Electron Micrograph of detached porcelain surface with no treatment, the sample revealed adhesive failure between the porcelain and resin cement whereas detached porcelain surface with combination of three method cohesive failure on the porcelain.

• Journal of Biosystems Engineering
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• 제43권3호
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• pp.237-246
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• 2018

Purpose: This study (a) investigated the effect of microwave power intensity and sample thickness on microwave drying characteristics of radish strips, and (b) determined the best-fit drying model for describing experimental drying data, effective moisture diffusivity ($D_{eff}$), and activation energy ($E_a$) for all drying conditions. Methods: A domestic microwave oven was modified for microwave drying and equipped with a small fan installed on the left upper side for removing water vapor during the drying process. Radishes were cut into two fixed-size strip shapes (6 and 9 mm in thickness). For drying experiments, the applied microwave power intensities ranged from 180 to 630 W at intervals of 90 W. Six drying models were evaluated to delineate the experimental drying curves of both radish strip samples. The effective moisture diffusivity ($D_{eff}$) was determined from Fick's diffusion method, and the Arrhenius equation was applied to calculate the activation energy ($E_a$). Results: The drying time was profoundly decreased as the microwave power intensity was increased regardless of the thickness of the radish strips; however, the drying rate of thicker strips was faster than that of the thinner strips up to a certain moisture content of the strip samples. The majority of the applied drying models were suitable to describe the drying characteristics of the radish strips for all drying conditions. Among the drying models, based on the model indices, the best model was the Page model. The range of estimated $D_{eff}$ for both strip samples was from $2.907{\times}10^{-9}$ to $1.215{\times}10^{-8}m^2/s$. $E_a$ for the 6- and 9-mm strips was 3.537 and 3.179 W/g, respectively. Conclusions: The microwave drying characteristics varied depending on the microwave power intensity and the thickness of the strips. In order to produce high-quality dried radish strips, the microwave power intensity should be lower than 180 W.

• 에너지공학
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• 제26권4호
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• pp.92-99
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• 2017

국내에서는 국토부 7대 신산업, 산업부 8대 신산업으로 제로에너지빌딩이 지정되었으며, 건물외피의 단열성능 극대화와 건물 기기 효율향상 및 신재생 보급 확대를 위해 부처간 융합을 통해 제로에너지빌딩 보급 활성화 달성을 목표로 하고 있다. 국내에서 시행 중인 제로에너지빌딩 인증제에 해당되는 건물에너지효율등급 1++이상이 되는 건축물들의 부하(냉방, 난방, 급탕, 조명, 환기)들의 에너지소요량을 분석하여 대략적인 부하들의 수준을 파악하고 제로에너지빌딩 인증제 고도화를 위한 기초 자료로 활용될 수 있도록 하는 목적이 있다. 제로에너지빌딩 인증에 해당되는 건축물은 2017년 기준 61개 가량 되는 것으로 파악되고 있으며, 패시브 측면과 액티브 측면을 고려하여 5대 부하별 대략적인 기준 값과 1차 에너지소요량을 산정하였다. 부하기준 산정을 위한 데이터의 표본이 적어 명확한 기준이 된다고 보기는 어려우나 앞으로 제로에너지빌딩 인증 기준을 고도화하기 위해 다양한 방법들을 적용하여 해석할 필요성이 있다고 판단된다.

• 한국식품위생안전성학회지
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• 제8권4호
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• pp.231-240
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• 1993

This study was carried out to find out the content of injurious heavy metals, such as mercury, lead, cadmium and arsenic of marine fish which had been captured in adjacent sea of Korea. From March, 1 to April, 30 in 1993. 60 sample of fishes were collected the adult fish and young fish. These samples were analyzed by the Mercury Analyzer and Inductively Coupled Plasma Emission Spectro Analyzer. The results of the study were summarized as follows: (1) The content of mercury in Therafra chalcograma was 0.112$\pm$0.034 ppm which was higher than other fishes, but Pseudosciaena manchurica and Pampus argenteus had lower (P<0.05). Although lead content of Trichiurus lepturus was 0.359$\pm$0.056 ppm, which was higher than other fishes. The lead content of Theragra chalcograma had lower to the almost same level. The cadmium content of the Theragra chalcograma was 0.069$\pm$0.010 ppm which was higher than other samples, but Pseudosciaena manchurica had 0.039$\pm$0.020 ppm to lower level. Though there was some fluctuation in the arsenic content which was 0.433~3.752 ppm, the arsenic content of Therafra chalcograma was 3.752$\pm$2.873 ppm which was the higher than any other fishes. But there are not statistical significances. (2) Heavy metal content by the maturity of the fishes: Mercury content of the old Pseudosciaena manchurica was 0.055$\pm$0.15 ppm comparing to the young's result of 0.030$\pm$0.009 ppm (P<0.05). Though there were some differences according to the maturity, but thee was no statistical significance. (3) In view of the correlation of the heavy metal content, for Pseudosciaena manchurica, high correlation was founded to r=0.6437 between mercury and cadmium (P<0.05). Though the content of mercury, arsenic cadmium and lead had positive correlation (r=0.2725) and negative correlation (r=-0.3958), but there was no significance at all. The other fishes were not found correlation between the heavy metal content. Positive correlation was found between age with mercury in Pseudociaena manchurica (r=0.7018, P<0.05). The negative correlation of age with lead content in the Pseudociaena Manchurica was signigicant (P<0.05). The correlation coefficient was r=-0.7623. The age with mercury content in Coloabis saira had high correlation (r=0.7201, P<0.05). Through the above analysis, it can get conclusion that injurious heavy metal content of the fishes in Korea such a mercury, lead, cadmium and arsenic were at the level of natural content. At present, guidelines of maximum residue level allowed at foreign countries about the injurious heavy metal have been used according to the kinds of fish but our government guideline for the marine fishes in only total mercury below 0.7 ppm and lead below 2 ppm. So more aggressive guidelines for the allowance level of heavy metals in marine fishes are required for the safety of foods.

• 한국식품위생안전성학회지
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• 제25권2호
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• pp.118-121
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• 2010

아세설팜칼륨, 싸이클라메이트, 삭카린나트륨, 수크랄로스, 스테비오사이드, 아스파탐을 HPLC/MS/MS를 이용하여 동시 분석한 결과 각 감미료 별로 고유한 스펙트럼을 얻어 정량하여 머므름 시간은 2.26~9.96로 10분 이내로 분석이 가능하였다. 각각 감미료의 상관계수($R^2$)은 0.9986~0.9999로 양호한 직선상의 그래프를 얻을 수 있었고 각각의 감미료를 단계적으로 희석하여 분석한 결과 검출한계는 아세설팜칼륨, 싸이클라메이트 삭카린나트륨, 수크랄로스, 스테비오사이트, 및 아스파탐의 경우 0.02 mg/kg이었다. 시료에 대한 6종의 감미료에 대한 분석법의 회수율은 과자 87.4~106.9%, 캔디 99.8~114.7%로 전반적으로 좋은 회수율을 보여 어린이기호식품에서의 감미료 분석에 적용하였다.