• Restorative Dentistry and Endodontics
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• 제19권2호
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• pp.447-459
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• 1994

The purpose of this study is to evaluate of shear bond strength of light-curing composite resin to light-curing glass ionomer cement. Composite resin and glass ionomer cement have been widely used as an esthetic filling materials in dental clinics. To achieve better clinical results, sandwich technic was developed with conpensating for disadvantages of these two materials. Especially, light-curing glass ionomer cement provided greately improved bonding strength of teeth or composite resin, and then excellent clinical results can be acquired. In this study, 6 commercial light-curing glass ionomer cements(3 commercial restorative materials : Fuji II LC, Variglass VLC, Vitremer, and 3 commercial lining materials : Fuji Lining LC, Baseline VLC, Vitrebond) were devided two groups. According to manufacturer's appointment, no surface treatment was referred to N groups. Supposing. of clinical practice, surface grinding with water spray at 320 grit sand paper, 40 seconds etching with 37% phosphoric acid, 20 seconds washing, 20 seconds air drying was referred to N groups. Totally 12 experimental groups were devided, and all 120 specimens from 10 specimens of each groups were made. After light-curing composite resin was bonded to light-curing glass ionomer cement, shear bond strength was tested by Instron universal testing machine between glass ionomer cement and composit resin. The data were analyzed statistically by Student's t-test and ANOVA. The obtained results were as follows; 1. In light-curing glass ionomer cement, restorative materials showed higher shear bond strength to composite resin than lining materials(p<0.05). 2. Variglass VLC of restorative material group and Baseline VLC of lining material group have highest shear bond strength to composite resin(p<0.001). 3. In light-curing glass ionomer cement, surface grinding and acid etching reduced shear bond strength to composite resin(p<0.001)}. 4. VGN group 1s highest shear bond strength to composite resin, VBE group is lowest shear bond strength to composite resin(p<0.001).

• 접착 및 계면
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• 제17권2호
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• pp.62-66
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• 2016

수용성 접착제의 경화 공정은 일반적으로 열풍건조기를 대부분 사용하고 있다. 열풍건조기는 열에 의해서만 수용성 접착제를 경화시키는 방법으로서, 충분한 경화를 위해 $100^{\circ}C$ 이상의 높은 온도와 최소 20 min 이상의 경화 공정을 요구하는 단점을 가지고 있다. 경화 과정 중에 온도가 너무 높을 경우, 접착제의 점도가 낮아져 접착에 방해가 될 수 있으며, 경화 과정 중에 발생하는 수분에 의해 경화 조건이 일정하게 유지되기 어렵다. 본 연구에서는 제습 막 건조기 시스템을 활용하여, 수용성 접착제의 경화 공정을 일정하게 유지시키고 공정 중의 제습을 통해 건조공기의 공급으로 경화시간을 단축하고자 한다. 제습 막 건조기 시스템을 활용한 최적의 경화 조건을 찾고, 제습 막 건조기 시스템의 효과를 확인하기 위하여, 제습 막 건조기와 강제순환 건조기를 적용한 경화 과정을 통해 접착력(peel strength)을 측정하여 비교 분석해 보았다.

• 한국축산식품학회지
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• 제23권1호
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• pp.32-38
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• 2003

식염농도 7%의 염지액을 이용하여 돼지고기 등심을 염지할 때에 염지온도와 기간이 염지육의 이화학적 특성과 기호성에 미치는 영향을 검토하였다. 열지온도 1$0^{\circ}C$에서 15일째에 염지육의 pH와 보수력이 현저히 저하되었다. 염지온도 1$0^{\circ}C$에서 염지액과 염지육 표면부위의 일반세균수는 12째에 현저히 많아졌으나 중심부위는 거의 검출되지 않았다. 임시 온도가 높을수록 염지기간에 관계없이 식염 침투가 빠르고 염지육 식염함량이 많아졌으며, 표면부위에 대한 중심분위의 식염함량 비율은 염지기간이 길수록 크게 나타났다. 염지육의 식염함량은 가열에 의하여 적어졌다. 염지 가열육의 짠맛과 풍미는 염지 초기에는 높은 온도에서, 후기에는 낮은 온도에서 우수하였다. 열지 가열육은 1$^{\circ}C$에서 12일, 5$^{\circ}C$에서 9일 염지하여 제조하면 기호성이 우수하였다.

• 한국산학기술학회논문지
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• 제16권11호
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• pp.7910-7916
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• 2015

본 연구에서는 팽창재 및 수축저감제 사용량 변화에 따른 초고성능 콘크리트(UHPC)의 양생조건별 역학적 특성 및 자기수축 특성에 대해 검토하였다. 그 결과 양생조건에 따른 UHPC의 역학적 특성으로 $90^{\circ}C$ 증기양생을 한 시험체는 모두 190 MPa 이상의 압축강도를 나타냈고 $20^{\circ}C$ 수중양생을 한 경우에는 재령 91일에서 증기양생을 한 시험체와 동등한 수준으로 발현되었다. 인장강도는 $90^{\circ}C$ 증기양생의 경우 23.4 MPa의 높은 수준으로 나타났으며 $20^{\circ}C$에서는 다소 저하하였다. 자기 수축 특성으로 양생조건에 따른 최종 수축량의 변화는 나타나지 않았다. 팽창재 및 수축저감제 사용에 따른 UHPC의 압축강도는 $90^{\circ}C$ 증기양생을 한 경우 190 MPa 이상 발현하였다. 자기수축 특성은 팽창재와 수축저감제를 복합 사용한 경우 약 45% 정도 수축저감 효과가 있는 것으로 나타났고 양생조건에 따른 차이는 발생하지 않았다.

• The Korean Journal of Ceramics
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• 제6권2호
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• pp.103-106
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• 2000

The effects of replacement level, curing method and chemical admixtures were investigated in the cement-fly ash paste. The strength of cement-fly ash paste is lower than that of controlled cement paste only and the differences increase with replacement level. However, in steam curing, strength of cement-fly ash pastes is improved, especially, at early ages. In order to improve early strength, the use of $Na_2SO_4$in cement-fly ash paste increases the quality of concrete. In addition, improvement of strength of concrete including 30% of fly ash can be obtained and achieves the highest strength compared to other concrete mixtures.

• Bulletin of the Korean Chemical Society
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• 제33권2호
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• pp.473-482
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• 2012

A novel malemide epoxy containing Co(II), Ni(II) and Cu(II) ions have been synthesized by curing malemide epoxy resin (MIEB-13) and Co(II), Ni(II) and Cu(II) complexes of macrocyclic bis-hydrazone Schiff base. The Schiff base was synthesized by reacting 1,4-dicarbnyl phenyl dihydrazide with 2,6-diformyl-4-methyl phenol. The Schiff base and its Co(II), Ni(II) and Cu(II) complexes have been characterized by elemental analyses, spectral (IR, $^1H$ NMR, UV-vis., FAB mass, ESR), thermal and magnetic data. The curing reaction of maleimide epoxy compound with metal complexes was studied as curing agents. The stability of cured samples was studied by thermo-gravimetric analyses and which have excellent chemical (acid/alkali/solvent) and water absorption resistance. Further, the scanning electron microscopy (SEM) and definitional scanning colorimetric (DSC) techniques were confirmed the phase homogeneity of the cured systems.

• 한국건축시공학회:학술대회논문집
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• 한국건축시공학회 2002년도 학술.기술논문발표회
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• pp.63-66
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• 2002

In this study, it does a high volume flyash substituted concrete experiments in two curing temperature circumstances - 35$^{\circ}C$, 2$0^{\circ}C$. High volume flyash concrete is tested in fresh concrete properties and hardeded concrete properties. In the fresh concrete test items, there is slump, air contents, concrete setting tests. 3, 7, and 28 days water curing compressive strength is measured in the hardened concrete test. The purpose of this study is to submit a various flyash concrete data for application to field. The result of this study is that the best strength is developed at the plain concrete cured 2$0^{\circ}C$ and Mixing F43 shows the best strength among specimens which cured at 35$^{\circ}C$

• 펄프종이기술
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• 제34권4호
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• pp.16-21
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• 2002

It was observed that drying temperature and curing time in the paper coating process as well as Tg of the latex used as a binder, greatly affected the properties of the coated paper such as roughness, paper and print gloss, K & N ink drop, and ink set-off. The higher drying temperature induced faster water evaporation and change in binding density, which caused an increase in paper roughness, ink gloss and ink set-off, but decrease in paper gloss and K & N ink drop. The increased curing time promoted latex filming and redistribution of the binder in coating layer. This increased pick strength and ink gloss, but decreased ink trapping. Finally, the higher Tg of the latex showed the wider changing range of these properties.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 1998년도 가을 학술발표회 논문집(I)
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• pp.185-190
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• 1998

Corrosion of steel reinforcement is the most significant factor of deterioration in reinforced concrete structures. Chloride ion is considered one of the most common culprits on the corrosion of steels in concrete. The main objective of this study is understanding behavior of chloride ion in hardened cement pastes at different stages of curing. Cement pastes with water-cement ratio of 0.5 are allowed to hydrate in sealed containers for 28, 70, 180 days. And than pore solution is expressed. It was found that the $Cl^-$ concentrations in pore solution is decreased with increasing curing time in all Nacl addition level, the $OH^-$ concentrations is increased to 70 days but decrease at 180 days in all Nacl addition level. The $Cl^-$/$OH^-$ in pore solution is increased with increasing curing time in all Nacl addition level, however $Cl^-$/$OH^-$ of maximum Nacl addition level(Nacl 0.54% by weight of cement) is under the onset of depassivation level 0.3.

• Bulletin of the Korean Chemical Society
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• 제31권8호
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• pp.2272-2278
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• 2010

A new hybrid thermosetting maleimido epoxy compound 4-(N-maleimidophenyl) glycidylether (N-MPGE) is prepared by reacting N-(4-hydroxyphenyl) maleimide (HPM) with Epichlorohydrin by using benzyltrimethylammonium chloride as a catalyst. The resulting compound possesses both the oxirane ring and maleimide group. The curing reaction of these maleimidophenyl glycidylether epoxy compound (N-MPGE) with amines as curing agents such as ethylendiamine (EDA), diethylentriamine (DETA) and triethylenetetramine (TETA), aminoethylpiperazine (AEP) and isophoronediamine, IPDA), are studied. Incorporation of maleimide groups in the epichlorohydrin provides cyclic imide structure and high cross-linking density to the cured resins. The cured samples exhibited good thermal stability, excellent chemical (acid/alkali/solvent) and water absorption resistance. Morphological studies by the SEM technique further confirmed the phase homogeneity net work of the cured systems.