• Title/Summary/Keyword: Volume calibration

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Uncertainty of Total Alkaloids and Reducing Sugar Determination in Flue-cured Tobacco (황색종 담배중 전알카로이드와 환원당 분석에 대한 불확도 측정)

  • 백순옥;장기철;이운철;한상빈
    • Journal of the Korean Society of Tobacco Science
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    • v.23 no.1
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    • pp.45-52
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    • 2001
  • This study was carried out to evaluate the uncertainty in the analysis of total alkaloids and reducing sugar content in flue-cured tobacco. The sources of uncertainty associated with the analysis of total alkaloids and reducing sugar were the weighing of sample, the preparation of extracting solution, the addition of extracting solution into the sample, the preparation of standard solution, the precision of calibration curve for standard solution, the reproducibility of analysis, and the determination of water content in tobacco, etc. For the calculating uncertainties, Type A of uncertainty was evaluated by the statistical analysis of a series of observation, and Type B by the information based on supplier’s catalogue and/or certificated of calibration. It was shown that the main source of uncertainty was caused by the calibration curve of standard solution, the reproducibility of analysis, the volume measurement of 1$m\ell$, and the purity of nicotine reference material in the preparation of standard solution. The uncertainty in the addition of extracting solution, the sample weighing, the volume measurement of 100$m\ell$, and the determination of water content of tobacco contributed relatively little to the overall uncertainty. The expanded uncertainty of total alkaloids and reducing sugar in flue-cured tobacco at 95% level of confidence was $\pm$0.12% and $\pm$0.54%, respectively.

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Study on Robot Calibration Using Multi-measurement Coordinate System (다중 측정 좌표계를 이용한 로봇 캘리브레이션 방법 연구)

  • Lim, Saeng-Ki;Kim, Jung-Tae;Borm, Jin-Hwan;Choi, Jae-Sung
    • Journal of the Korean Society for Precision Engineering
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    • v.16 no.3 s.96
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    • pp.164-173
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    • 1999
  • Robot calibration needs accurate measurements of robot end-effector position at a number of different robot configurations. One of the efficient ways of the measurement is "Touching on Jig" method suggested in [7], which utilizes a touch sensor and a fixture consisting of various sizes of blocks. By moving the end-effector to touch the surface of a block whose position relative to the other is known, the end-effector position relative to the fixture coordinate system can be obtained at the instant of touching. However, the global size of fixture is too small to cover the various configurations of the robot. Because of the manufacturing difficulties, the fixture cannot be manufactured large enough for well distributed position measurement. It results in the improvement of robot accuracy only in the limited space near to the fixture rather than over the whole space of the robot working volume. The paper proposes a method to resolve the above problem by measuring the end-effector positions with respect to several different coordinate system using the same measurement devices. It is found that the proposed method leads the improvements of robot position accuracy over the large space of working volume. The experimental studies are performed to show the validity of the method and their results are discussed.

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Development of Ultrasound Phantom for Volume Calibration (부피 측정을 위한 초음파 팬텀 개발)

  • Kim, Hye-Young;Lee, Ji-Hae;Lee, Kyung-Ja;Suh, Hyun-Suk;Lee, Re-Na
    • Progress in Medical Physics
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    • v.19 no.4
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    • pp.227-230
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    • 2008
  • The purpose of this study was to design and construct an ultrasound phantom for volume calibration and evaluate the volume measurement accuracy of a 2 dimensional ultrasonic system. Ultrasound phantom was designed, constructed and tested. The phantom consisted of a background material and a target. The background was made by mixing agarose gel with water. A target, made with an elastic material, was filled with water to vary its volume and shape and inserted into background material. To evaluate accuracy of a 2 dimensional ultrasonic system (128XP, ACUSON), three different shapes of targets (a sphere, 2 ellipsoids and a triangular prism) were constructed. In case of ellipsoid shape, two targets, one with same size length and width (ellipsoid 1) and another with the length 2 times longer than width (ellipsoid 2) were examined. The target volumes of each shape were varied from 94cc to 450cc and measurement accuracy was examined. The volume difference between the real and measured target of the sphere shape ranged between 6.7 and 11%. For the ellipsoid targets, the differences ranged from 9.2 to 10.5% with ellipsoid 1 and 25.7% with ellipsoid 2. The volume difference of the triangular prism target ranged between 20.8 and 35%. An easy and simple method of constructing an ultrasound phantom was introduced and it was possible to check the volume measurement accuracy of an ultrasound system.

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Error analysis and Performance test of the Volumetric interferometer for Absolute distance measurement (삼차원 좌표 측정을 위한 부피 간섭계의 오차분석 및 성능평가)

  • Rhee, H.G.;Chu, J.Y.;Kim, S.W.
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2002.10a
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    • pp.387-390
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    • 2002
  • In this paper, we accomplish uncertainty evaluation and performance test of the volumetric interferometer using two spherical wavefronts emitted from the ends of two single mode fibers. We verify that the volumetric interferometer has the volume uncertainty of 690nm through the error analysis and it has the resolution of 0.1 0.1$\mu\textrm{m}$ for x axis which is the same order of repeatability for x axis. Also, we obtain the systematic error of $1\mu\textrm{m}$ for $60\times 60\times 20 mm^3$ working volume using self-calibration with an artifact plate.

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Evaluation of Clinical Risk according to Multi-Leaf Collimator Positioning Error in Spinal Radiosurgery (척추 방사선수술 시 다엽콜리메이터 위치 오차의 임상적 위험성 평가)

  • Dong‑Jin Kang;Geon Oh;Young‑Joo Shin;Jin-Kyu Kang;Jae-Yong Jung;Boram Lee
    • Journal of radiological science and technology
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    • v.46 no.6
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    • pp.527-533
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    • 2023
  • The purpose of this study is to evaluate the clinical risk of spinal radiosurgery by calculating the dose difference due to dose calculation algorithm and multi-leaf collimator positioning error. The images acquired by the CT simulator were recalculated by correcting the multi-leaf collimator position in the dose verification program created using MATLAB and applying stoichiometric calibration and Monte Carlo algorithm. With multi-leaf collimator positioning error, the clinical target volume (CTV) showed a dose difference of up to 13% in the dose delivered to the 95% volume, while the gross tumor volume (GTV) showed a dose difference of 9%. The average dose delivered to the total volume showed dose variation from -8.9% to 9% and -10.1% to 10.2% for GTV and CTV, respectively. The maximum dose delivered to the total volume of the spinal cord showed a dose difference from -14.2% to 19.6%, and the dose delivered to the 0.35 ㎤ volume showed a dose difference from -15.5% to 19.4%. In future research, automating the linkage between treatment planning systems and dose verification programs would be useful for spinal radiosurgery.

Development of 3-D Volume PIV (3차원 Volume PIV의 개발)

  • Choi, Jang-Woon;Nam, Koo-Man;Lee, Young-Ho;Kim, Mi-Young
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.27 no.6
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    • pp.726-735
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    • 2003
  • A Process of 3-D Particle image velocimetry, called here, as '3-D volume PIV' was developed for the full-field measurement of 3-D complex flows. The present method includes the coordinate transformation from image to camera, calibration of camera by a calibrator based on the collinear equation, stereo matching of particles by the approximation of the epipolar lines, accurate calculation of 3-D particle positions, identification of velocity vectors by 3-D cross-correlation equation, removal of error vectors by a statistical method followed by a continuity equation criterior, and finally 3-D animation as the post processing. In principle, as two frame images only are necessary for the single instantaneous analysis 3-D flow field, more effective vectors are obtainable contrary to the previous multi-frame vector algorithm. An Experimental system was also used for the application of the proposed method. Three analog CCD camera and a Halogen lamp illumination were adopted to capture the wake flow behind a bluff obstacle. Among 200 effective particle s in two consecutive frames, 170 vectors were obtained averagely in the present study.

A Noise Re-radiation Calibration Technique in Interferometric Synthetic Aperture Radiometer for Sub-Y-type Array at Ka-Band

  • Seo Seungwon;Kim Sunghyun;Choi Junho;Park Hyuk;Lee Hojin;Kim Yonghoon;Kang Gumsil
    • Proceedings of the KSRS Conference
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    • 2004.10a
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    • pp.577-580
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    • 2004
  • To overcome with large size noise source distribution network design difficulty in interferometric radiometer system, especially for sub-Y-type array, a new on-board calibration technique using noise re-radiation is proposed in this paper. The suggested calibration technique is using noise re-radiation effect of center antenna after noise source injection from matched load. This approach is especially proper to sub-Y-type array interferometric synthetic aperture radiometer in mm-wave frequency band. Compared with noise injection network of a conventional synthetic aperture radiometer, the system mass, volume, and hardware complexity is reduced and cost-effective. Only one internal noise source, matched load, is used for injection using noise re-radiation technique a small set of sub-Y receiver channels is calibrated. Detailed calibration scenario is discussed and simulation results about noise re­radiation effect are presented.

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The Use of Vibro-acoustical Reciprocity to Estimate Source Strength and Airborne Noise Synthesis (구조-음향 상반성 원리를 이용한 공기기인 소음원의 강도 추정 및 소음 합성)

  • Kim, Yoon-Jae;Byun, Jae-Hwan;Kang, Yeon-June;Hong, Jin-Chul;Kwon, O-Jun;Kang, Koo-Tae
    • Transactions of the Korean Society for Noise and Vibration Engineering
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    • v.19 no.1
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    • pp.42-49
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    • 2009
  • In this paper, an alternative method was introduced to conduct a transfer path analysis for airborne noise. The method used the transfer function matrix composed of acoustic transfer functions that are referenced by the input voltage of a calibration source. A calibration factor which is converting a virtual voltage to source strength was deduced by vibro-acoustical reciprocity theorem. The calibration factor is then multiplied to the virtual input voltage to estimate the operational source strength. Three loudspeakers were used to noise sources of acrylic half car model. The method was applied to airborne noise transfer path analysis of the half car. The estimated source strength by transfer path analysis was compared the deduced source strength by vibro-acoustical reciprocity to verify the method.

A Study on the Measurement Uncertainty of Pipe Prover (파이프 프루버의 측정불확도에 관한 연구)

  • Lim, Ki-Won
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.24 no.10
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    • pp.1388-1398
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    • 2000
  • A pipe prover is a flowmeter calibrator used in flow measurement field. Gravimetric and volumetric methods were applied to determine the basic volume of the pipe prover. Uncertainty of its basic volume measurement was evaluated in accordance with the procedure recommended by International Organization for Standardization. The combined standard uncertainty of determining the basic volume was estimated from the sensitivity coefficient and the standard uncertainty of independent variables. It was found that the uncertainties of the weighing and volume measurements have dominant influence on that of the basic volume determination. With the quantitative analysis of the sensitivity coefficient, the contribution of the each variable uncertainty to the combined standard uncertainty of the basic volume is shown clearly.

Phase Identification of Nano-Phase Materials using Convergent Beam Electron Diffraction (CBED) Technique

  • Kim, Gyeung-Ho;Ahn, Jae-Pyoung
    • Applied Microscopy
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    • v.36 no.spc1
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    • pp.47-56
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    • 2006
  • Improvements are made to existing primitive cell volume measurement method to provide a real-time analysis capability for the phase analysis of nanocrystalline materials. Simplification is introduced in the primitive cell volume calculation leading to fast and reliable method for nano-phase identification and is applied to the phase analysis of Mo-Si-N nanocoating layer. In addition, comparison is made between real-time and film measurements for their accuracy of calculated primitive cell volume values and factors governing the accuracy of the method are determined. About 5% accuracy in primitive cell determination is obtained from camera length calibration and this technique is used to investigate the cell volume variation in WC-TiC core-shell microstructure. In addition to chemical compositional variation in core-shell type structure, primitive cell volume variation reveals additional information on lattice coherency strain across the interface.