• E2M - 전기 전자와 첨단 소재
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• 제7권1호
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• pp.32-41
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• 1994

In this study, the TSC spectroscopy has been applied to investigate the influence of structural change due to a process of curing reaction on the electrical properties of epoxy composites cured with acid-anhydride. Five TSC peaks appeared in -160-250[.deg.C]: in the low temperature region below glass transition temperature(T$\_$g/), three relaxation mode peaks due to action of side chains, substitution group or terminal groups have been observed, a peak associated with T$\_$g/, appeared in 110[.deg. C] and p peak due to ionic space charges located in 150[.deg.C]. Each peak was separated into elementary peaks by the partial polarization procedure, and the distribution of activation energy and relaxation time were analized to clearify the origin of each peak. Also, overaboundantly added hardener separated a .betha. peak near 10[.deg. C] into two peaks of .betha.$\_$1/(10.deg. C) and .betha.$\_$2/(20.deg. C) according to increasement of forming field, and the separated hardener was oxidated thermally with increasing surrounding temperatures. The expansion of the free volume need in molecular motion and the reduction of the structural packing density through thermal oxidation process increased TSC between .alpha. peak and .betha. peak and decreased T$\_$g/.

• 한국식품조리과학회지
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• 제28권6호
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• pp.763-771
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• 2012

Physicochemical and sensory characteristics of pound cakes containing Angelica gigas NAKAI(Korean Angelica) with various levels of rice flour were investigated in this study. There were significant differences in the specific gravity of dough, and it had the lowest value of 0.848 in the control group. The weight of pound cakes was significantly increased by addition of rice flour, but the volume, specific volume and baking loss rate were significantly decreased by addition of rice flour. The moisture content and pH of pound cakes were found to increase with increasing rice flour content. DPPH radical scavenging activity of the control group was 51.02%, whereas pound cakes with rice flour ranged from 51.90~55.75%. The L value of brightness was increased, but a and b values were decreased significantly by addition of rice flour. In all of items of texture, the control group was higher than those of the pound cakes prepared with various levels of rice flour. Sensory evaluation scores in terms of appearance, flavor, taste, texture and overall preference for pound cakes showed that 50% and 75% substituted sample groups were higher than those of the other groups. The results of this study suggest that addition of 50~75% rice flour is the best substitution ratio for Korean Angelica pound cakes.

• 한국식품영양학회지
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• 제31권1호
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• pp.195-201
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• 2018

This study was intended to investigate the characteristics of muffins prepared with allulose which is low-calorie and physiologically functional rare sugar. Volume and specific volume of muffins increased significantly with allulose addition, but not with its contents. Muffin heights also increased as allulose was added more. Baking loss rate and moisture contents were not significantly different among samples. Allulose seemed to have nearly same water holding capacity with sucrose. Lightness of muffin crust and crumb both decreased, but redness and yellowness increased according to allulose, the reducing sugar addition by Maillard reaction. In the texture profile analysis, Hardness of AL100 was higher significantly (p<0.05) and springiness, cohesiveness and fracturability increased according to the allulose contents. In the sensory evaluation, AL0 was the sweetest and AL0 and AL25 got higher overall acceptance score. Physical characteristics were not different (p<0.05) among AL0, Al25 and AL50. As a result, 25% sucrose substitution with allulose can provide low-calorie, anti-hyperglycemic and tasty muffin.

• 한국식품영양과학회지
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• 제40권10호
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• pp.1474-1481
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• 2011

부드러운 식감을 선호하는 소비자들의 기호에 맞는 맞춤형 우리밀 파스타 제조의 일환으로 durum wheat rimachinata에 우리밀가루 0, 15, 30, 45 및 60%를 대체하여 제조한 파스타의 물리 화학적 특성을 살펴보고자 하였다. 입도분포는 우리밀이 250 ${\mu}M$ 이하의 작은 입자가 전체의 87.03%를 차지하며, durum rimachinata는 250 ${\mu}M$ 이상이 68.70%를 나타내었다. 일반성분은 durum rimachinata에서 단백질과 회분이 각각 13.84${\pm}$0.03, 0.70${\pm}$0.02로 우리밀보다 높게 나타났다. 반죽의 farinograph 특성은 우리밀의 대체량이 증가할수록 수분흡수율은 증가하고 반죽형성시간은 높게 나타났고, 안정도와 연화도는 증가하였다. Amylograph 특성은 우리밀의 대체량이 증가할수록 호화개시온도는 상승하고, 최고점도는 감소하였으나 우리밀 30% 대체까지는 550 B.U. 이상으로 면류제품의 물성변화에 큰 영향을 미치지 않았다. 조리특성은 우리밀 대체량 15% 미만에서 중량, 부피, 수분흡수율, 탁도 및 조리손실율이 대조구와 유사하여 부드럽고, 탄력성이 있는 파스타 면을 만들 수 있었다. 색도는 우리밀 대체량이 증가할수록 L값과 a값은 증가하였고, b값은 감소하였다. 물성측정 결과 조리면의 경도 및 점착성은 우리밀 대체 30% 이상에서 낮은 값을 나타내었으며, 탄력성, 검성, 씹힘성은 높은 값을 나타내었다. 전반적인 기호도는 대조구가 가장 높게 나타났으나 우리밀 대체 45% 이상에서 높은 기호도를 나타내었다. 따라서 우리밀을 대체한 파스타의 제조시 반죽 및 조리특성에서는 우리밀 15% 대체수준이 적합하나 조리된 파스타의 기계적 물성측정 및 관능평가 결과에서는 30% 대체 이상에서 높게 나타났다.

• 한국식생활문화학회지
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• 제30권2호
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• pp.206-212
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• 2015

The purpose of this study was to investigate the quality characteristics of cookies containing Ligularia fischeri powder (0, 1, 2, 3, 4%) substituted for flour. This study measured the density, pH, spread ratio, volume, color values, hardness, and sensory properties of cookies. The pH of cookie dough significantly decreased in response to addition of Ligularia fischeri powder (LFP) at all levels. The spread factor of cookies also significantly increased with higher LFP content. In addition, Hunter's color L, a, and b values significantly decreased with increasing LFP content. According to hardness measurement, substitution of 1~4% LFP resulted in increased hardness compared to the control. In the sensory evaluation, sensory scores for color, flavor, and overall acceptability were highest in 2% Ligularia fischeri powder cookies. Thus, our results suggest that the optimum amount of Ligularia fischeri powder added to cookies was 2%. These results suggest that Ligularia fischeri powder can be applied to cookies to achieve high quality and functionality.

• 동아시아식생활학회지
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• 제25권3호
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• pp.502-512
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• 2015

This study was conducted to investigate the physical, textural and sensory properties of sponge cake prepared with different amounts of radish leaf powder. The specific gravity and viscosity of cake batter and cooking loss of cake increased with an increasing amount of radish leaf powder, whereas specific loaf volume and moisture content of cake decreased. Lightness, redness and yellowness of crust and crumb decreased with increasing radish leaf powder content. Measurements using a texture analyzer showed that hardness, chewiness, gumminess, adhesiveness and fracturability of sponge cake tended to increase in proportion to the amount of radish leaf powder in the formula. In the sensory evaluation, sponge cake prepared with 5% radish leaf powder was similar to the control in terms of moistness, softness, chewiness and springiness. These results suggest that adding 5% radish leaf powder is the best substitution ratio for sponge cake.

• BMB Reports
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• 제28권4호
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• pp.363-367
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• 1995

E. coli methionyl-tRNA synthetase is one of the class I tRNA synthetases. The Tryptophane residue at the position 461 located in the C-terminal domain of the enzyme is a key amino acid for the interaction with the anticodon of $tRNA^{Met}$. W461 was replaced with other amino acids to determine the chemical requirement for the interaction with the anticodon of $tRNA^{Met}$. Saturation mutagenesis at the position 461 generated a total of 12 substitution mutants of methionyl-tRNA synthetase. All the mutants showed the same in vivo stability as the wild-type enzyme, suggesting that the amino acid substitutions did not cause severe conformational change of the protein The mutants containing tyrosine, phenylalanine, histidine and cysteine substitutions showed in vivo activity while all the other mutants did not. The comparison of the in vitro aminoacylation activities of these mutants showed that aromatic ring structure, Van der Waals volume and hydrogen bond potential of the amino acid residue at the position 461 are the major determinants for the interaction with the anticodon of $tRNA^{Met}$.

• 한국산업정보학회:학술대회논문집
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• 한국산업정보학회 1999년도 추계공동학술대회 논문집:21세기지식경영과 정보기술
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• pp.595-599
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• 1999

본 논문에서는 카오스 현상을 나타내는 수식을 변형하여 암호시스템이나 PN(pseudo-noise)시퀸스에 적용하기 위하여 복잡한 카오스 신호를 발생시키는 하이퍼카오스 VP 사상(HVPM, Hyper chaos Volume Preserving Maps)과 이들간의 카오스 동기화를 제안한다. 단계별 모듈러(modulus) 함수를 이용하여 랜덤한 카오스 신호를 발생시키기 위하여 이산시간(discrete-time) HVPM 모델을 설정하고, 수치해석 실험으로 아날로그 카오틱시퀸스(CAS. chaotic analog sequence)의 특징을 분석한다. 그리고 HVPM의 신호를 기존의 단순한 PC(Pecora, Carroll)방법을 응용한 치환동기화 (synchronous substitution)를 이용하여 구동 및 응답시스템간의 카오스 동기화(chaos synchronization) 제어를 한다. 수치실험에서 카오스 신호가 갖는 특징들을 확인할 수 있었으며, 치환동기시스템에서 효과적인 카오스 동기화가 수행됨을 증명할 수 있었다.

• 한국식품영양학회지
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• 제16권4호
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• pp.321-327
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• 2003

The reaction rates of 4-ethyl pyridine with p-methyl benzylbromide have been measured by conductometry in acetonitrile, and the rate constants of these reactions are determined in accordance with various temperatures (20, 25, 30$^{\circ}C$) and pressures (1, 200, 500, 1000 bar). The rate constants increased with the higher pressure and temperature. The activation energies and activation parameter values of these reactions are calculated by determination of the rate constants the same. The activation volume, activation compressibility coefficient and the activation entropy are all negative. The result of kinetic studies for the pressure show that this reaction proceeds in typical bimolecular nucleophilic substitution reaction.

• 한국결정학회지
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• 제14권2호
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• pp.110-114
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• 2003

LiAl/sub 0.24/Mn/sub 1.76/O/sub 4-y/S/sub y/ (y=0, 0.02) were synthesized by the sol-gel method. Both structures were refined by Rietveld method, its structure refined as a cubic spinel, space group Fd-3m, a=8.17937(30) Å and 8.18331(19) Å respectively. Though it has been made a charge/discharge experiment above 20 times, there was no change of 3 V/4 V capacity degradation. It was considered that the volume change of MnO/sub 6/ octahedron induced by sulfur substitution plays a key role in keeping the 3 V/4 V capacity. The refined composition of the compound could be confirmed with the ICP analysis.