• Journal of the korean academy of Pediatric Dentistry
• /
• v.23 no.2
• /
• pp.327-346
• /
• 1996

The purpose of this study was to evaluate the shear bond strengths, microhardness, compressive strength and contraction gap at the resin-tooth interface of two types of composite resins polymerized with visible light and argon laser sourse. The results from the present study can be summarized as follows ; 1. Resin samples polymerized either by argon laser or visible light did not show significant difference in their physical properties tested(p>.05). 2. The contraction gap at the resin tooth interface was found to be present in all samples but any significant difference between groups could not be established due to their variability. Although the superiority of argon laser over visible light in enhancing the physical properties of resin could not be elucidated in the present study, continous efforts are deemed to be worthwhile to investigate this area using different conditions and materials of experiment.

• Journal of Technologic Dentistry
• /
• v.23 no.2
• /
• pp.49-59
• /
• 2002

The photopolymerization efficiency and surface hardness of composite resin containing 1,2-phenylpropanedione (PD) and diacetyl (DA) as photoinitiators were studied by IR and Vickers hardness and the results were compared with that of camphorquinone (CQ). Relative photopolymerization efficiency of the photoinitiators increased in the order of DA < CQ < PD. Vickers hardness of composite resin containing the photoinitiators increased in the order of CQ < PD < DA. Thus, PD is a new visible light photoinitiator for dental composite resin with higher photopolymerization efficiency and surface hardness than that of CQ. Mechanical properties such as Vickers hardness, diametral tensile strength, and flexural strength of the experimental resin composite prepared by addition of the photosensitizer into a resin of bis-GMA improved with increasing the photosensitizer content and irradiation time. The resin composite of bis-GMA containing DA or PD shows better mechanical properties than that of CQ.

• Journal of Technologic Dentistry
• /
• v.33 no.4
• /
• pp.291-297
• /
• 2011

Purpose: The purpose of this study was to know the availability of three photosensitizers, CQ, PD, DA, as a photosensitizer of dental resin composite. We want to know abortion band around visible light region for the using potential possibility as a photosensitizer for visible light cured dental composite resin. And I studied to know the relative photodecomposition ratio of three photosensitizers with or without photoinitiator, DAEM. Methods: The photodecomposition of three photosensitizers were studied by UV absorption spectroscopy in ethanol and determined by same instrument with irradiation time for relative photodecomposition. In order to study the effect of amine on photodecomposition was added the DAEM in the photosensitizer solution and the relative rate was measured by the same procedure with aove mentioned. Results: The all of three photosensitizers are absorbed around visible light region. The relative rate of decrease in absorbance incereased in the order: CQ < BD < PD. The effect of DAEM on the photodecomposition of the photosensitizers was appeared different results without DAEM. The photodecomposition rate of PD and DA decreased somewhat with the addition of amine, while that of CQ increased. The rtealtive photodecomposition rate increased in the oprder: BD ${\leq}$ CQ < PD with the addition of amine, but the differnce was not significant. Conclusion: PD and DA like CQ gives to the possibility of use as a photosensitizer for visible light cured dental composite resin by absorption around visible light region and photodecomposition in the maximum absorption wavelength. And it is showed that PD and DA are not effective decomposed with amine initiator, DAEM but CQ decomposed with DAEM effectively. This result may be due to a different mechanism operating for the decomposition of photosensitizers in the presence of amine.

• The Journal of Korean Academy of Prosthodontics
• /
• v.31 no.1
• /
• pp.11-18
• /
• 1993

Autopolymerising and visible light cured resin are used to reline dentures. But relined surface are easily contaminated by water or saliva in the mouth during clinical procedure. This study was to find out the effect of surface contamination on the transverse strength of the relined denture base. To accomplish this, the specimens of $65\times10\times3mm$ were made with heat-cured(Lucitone 199), visible light-cured(Triad), and autopolymerizing resin(Kooliner). Measurements of transverse strength were taken for each specimen. Specimens made of heat-cured resins, sizing $65\times10\times1.5mm$, were relined with heat-cured, light-cured, and autopolymerizing resin, respectively. Specimens relined with autopolymerizing and light-cured resins were further classified into not-contaminated, water-contaminated and saliva-contaminated groups. Again, measurements of the transverse strength were taken for each group. The results were as follows 1. The transverse strength of heat-cured resin was superior to all the other resins. 2. The transverse strength of each specimen decreased after relining in the following order, heat-cured, visible light-cured, and autopolymerizing resin. 3. Surface contamination produced an decrease in transverse strength, especially in the saliva contaminated group. According to these results, water or saliva contamination should be avoided during intraoral relining procedures.

• Proceedings of the Korean Society of Precision Engineering Conference
• /
• 2013.05a
• /
• pp.649-650
• /
• 2013

• Restorative Dentistry and Endodontics
• /
• v.11 no.1
• /
• pp.43-52
• /
• 1985

The purpose of this study was to measure the Micro-Knoop Hardness of three commercial visible light-cured composite resins (Plurafil-super, He1iosit and Durafi) according to the difference of depth and shade. Specimens of the resin were prepapared in plastic tubes 5mm in diameter with height of 5mm, and the tubes were put into the columned holes in stone molds. The molds were exposed to the visible light through the hole 5mm in diameter in metal plate. Specimens were sectioned (longitudinally) with disk. Knoop Hardness measurements were made at the depth of surface, 0.5, 1.0, 1.5, 2.0, 2.5 and 3.0mm from the surface to the deep portion. Knoop Hardness numbers were taken on each depth under 20gm load for 10 seconds with Shimadzu Tester. The following results were: 1. The highest hardness value was measured at 0.5mm depth. Then the deeper the depth, the lesser the hardness was observed. 2. The value of hardness was directly propotional to the time of exposure to the light. 3. The hardness of light shade resin was higher than the that of the dark shade. 4. The pattern of hardness change at varying depth is similar to all the experimental materials with no relation to the shade nor exposure time.

• Journal of the Korean Society for Precision Engineering
• /
• v.30 no.8
• /
• pp.878-884
• /
• 2013

Stereolithography can be classified into two main categories according to the cross-sectional shape: scanning type and projection type. Projection stereolithography has significant advantages when making a layer using a single patterned beam, and results in improved speed and accuracy. To implement relatively low-cost projection stereolithography, we developed a system using a commercially available resin, which cures on exposure to visible light. The optimum photoinitiator was investigated, as well as the mixing ratio. The viscosity, shrinkage, curing depth and tensile strength were evaluated through several experiments on fabricated three-dimensional structures, and thus an optimal resin selection system was developed.

• Journal of the korean academy of Pediatric Dentistry
• /
• v.23 no.4
• /
• pp.899-905
• /
• 1996

For the purpose of evaluation of microleakage of class V resin restoration, 64 extracted bovine teeth were filled with two kinds of light curing composite resins(Z-100, Clearfil) and polymerized with 40 seconds of visible light and with 10 seconds of argon laser. After 1000 thermocycling($5^{\circ}C/55^{\circ}C$), specimens were placed in 1 % methylen blue dye solution for 72 hours in $37^{\circ}C$ water bath. The specimens were sectioned at center of filling body and the degree of dye penetration was observed with a stereomicroscope. The following results were obtained, 1. Differences of the microleakage of resin restorations polymerized with 10 seconds of argon laser and 40 seconds of visible light were statistically insignificant. 2. There was more microleakage in Z-100 than clearfil and there was a statistical significancy (p<0.05).

• Restorative Dentistry and Endodontics
• /
• v.19 no.2
• /
• pp.602-610
• /
• 1994

The purpose of this study was to measure the free flow of the unpolymerized resin by its weight for 10 minutes by one minute interval, and to measure the dimensional change of composite resins during the irradiation of visible light(Quich light VL-l Kuraray Japan) using visible leser displacement meter(LC-2210 Kerence Japan). The unpolymerized resin was cured by the visible light for 40 seconds, the dimensional change was measured at the begining of irradiation for 5 minutes. The results were as follows : 1. In free flow LFI was the largest, BLI was the smallest at $23^{\circ}C$ and CFP was the largest, and BL was the smallest at $37^{\circ}C$. 2. In dimensional change CFI, LFP, LEI and CFP was excessively contracted flow the begining of irradiation until 15 seconds but BLI and BL was excessively contracted until 30 seconds BL and BLI in dimensional change was much larger than LFI and CFP.

• The Journal of the Korean dental association
• /
• v.51 no.1
• /
• pp.12-17
• /
• 2013

Curing methods for denial resin-based materials are limited because of the need to polymerize quickly in the oral cavity at an ambient temperature. At present, most dental restorative composites use a camphorquinone-amine complex initiation, visible light-cure, one-component systems. Clinically, it is important to try to optimize the degree of conversion of res in composites using proper manipulation and adequate light-curing techniques to ensure the best outcome.