• 한국세라믹학회지
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• 제52권6호
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• pp.403-409
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• 2015

Porous alumina ceramics are involved in many industrial applications due to the exceptional properties of these products. This study addresses the preparation of porous alumina ceramics using hollow microspheres as a pore-forming agent and slip casting as a green-body-forming technique. A uniform distribution of pores is a basic requirement of a porous material. This study investigates three different slurry systems, i.e., as-prepared alumina slurry, alumina slurry electrostatically dispersed by hydrochloric acid (HCl), and slurry dispersed by the commercial dispersant 'Darvan C-N'. At a low viscosity, the hollow microspheres in the slurry tend to float, which causes a non-uniform pore distribution. To avoid this phenomenon, the viscosity of the slurry was increased to the extent that the movement of hollow microspheres ceased in the slurry. As a result, a uniform pore distribution was achieved.

• 공업화학
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• 제10권5호
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• pp.707-710
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• 1999

제전성 폴리에틸렌테레프탈레이트(PET)에 열안정제를 첨가하여 수분율과 고유점도의 거동변화를 연구하였다. 제전 PET의 최종 수분율은 건조시간보다는 건조온도의 함수로 나타났다. 용융방사후 제전 PET의 고유점도 강하는 수분율이 증가함에 따라 증가했다. 용융방사후 제전 PET의 고유점도가 감소했는데 이것은 제전제 성분중 폴리옥시알킬렌글리콜(POAG) 성분의 열화 열분해에 의한 것이다. 열안정제로서 trimethylphosphate(TMP)를 사용하는 것보다 triphenylphosphate(TPP)를 사용한 것이 더 효과적이었다. 열안정제로서 TPP를 300ppm 사용한 것이 용융방사후 고유점도의 저하가 적었다.

• Elastomers and Composites
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• 제25권4호
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• pp.280-290
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• 1990

The effect of surface treatment of kaolinite with silane coupling agent on the reinforcement of SBR was investigated. The possibility of the practical use of kaolinite as an organic filler was also scrutinized and it was found that the reinforcement of SBR was improved by modifying surface of the cheap inactive inorganic filler with organic silane coupling agents. 3-Chloropropyltrimethoxysilane(C-series), 3-mercaptopropyltrimethoxysilane(M-series) and 3-aminopropyltriethoxysilane(A-series) were used as coupling agents. To test the material properties of vulcanized and unvulcanized SBR, Mooney viscosity, modulus, elongation and fractured surface measurements by SEM were carried out by changing the amount of silane coupling agents. Torqe of the unvulcanized SBR following the measurement of the degree of vulcanization was to be increased as the amount of silane was increasing, and Mooney viscosity of M-series and A-series was also increased.

• Macromolecular Research
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• 제14권2호
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• pp.187-193
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• 2006

Organoclay, was applied as a filler, in place of carbon black and silica, to a natural rubber (NR)/butadiene rubber (BR) blend. A compounding method was used to disperse and separate the layered silicates. The effect of a coupling agent on the vulcanizates was evaluated using both the silica and organoclay filled compounds. After the compounding processes were completed, the XRD diffraction peaks disappeared, but then reappeared after vulcanization. The scorch times for the organoclay-filled compounds were very short compared to those for carbon black and silica-filled compounds. The organoclay-filled compounds showed high values of tensile strength, modulus, tear energy, and elongation at the break. When ranked by viscosity, the compounds appeared in the following order: silica > silica (Si-69) > organoclay > organoclay (Si-69) > carbon black. Fractional hysteresis, tensile set, and wear rates were very consistent with the viscosity of the vulcanizates. The Si 69 coupling agent increased reversion resistance, the maximum torque values in the ODR, modulus, and wear resistance, but decreased elongation at the break, fractional hysteresis, and tension set of the vulcanizates.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 1996년도 봄 학술발표회 논문집
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• pp.117-122
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• 1996

The purpose of this study is to investigate the properties of underwater concrete using three kinds of cellulose ether which has viscosity and water retention. The result is that water retention in underwater concrete shows in inverse proportion to PH value and the compressive strength is almostly effected by water retention. It can be certificated by the zeta electro potential value of an undispersed underwater concrete.

• 한국구조물진단유지관리공학회 논문집
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• 제23권6호
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• pp.99-104
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• 2019

본 연구의 목적은 시멘트계 복합재료의 적층을 위해 증점제를 적용하여 개발한 출력배합의 수축 특성을 평가하고, 프린팅 기법을 이용해 제작한 적층시험체와의 수축 특성을 비교하는 데 있다. 증점제 적용 시 수축이 기준배합과 비교하여 평균 25% 저감(56일 기준)되는 것을 확인하였다. 수축이 저감되는 긍정적인 효과에 반해 압축강도는 약 15% 감소(28일 기준)되는 부정적인 효과도 확인되었다. 출력배합을 이용해 제작한 적층시험체와 몰드시험체를 이용하여 수축을 평가한 결과, 적층시험체의 수축변형률이 약 25% 감소(28일 기준)되는 것을 확인하였다. 본 연구결과를 통해 3D 프린팅을 이용한 시멘트계 복합재료의 출력 시 수축의 진전속도와 수축으로 인한 균열의 발생시점을 예측할 수 있을 것으로 판단된다.

• 한국염색가공학회지
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• 제17권6호
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• pp.20-26
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• 2005

For developing digital printing textiles, special pretreatment processes are necessary. These processes include developing formulation of coating agent and coating processes. The pretreatment were investigated with the variation concentration of anti-migration agent, fixation chemical etc.. The printing qualities according to pretreatment conditions were studied with color yield, printed capital letter sharpness and washing fastness. It was observed that the concentration of anti-migration agent, fixation agent(alkali) was closely related to printing qualities. For developing industrial technology of cellulosic digital printing textiles, optimum viscosity of pretreatment coating formulation is very important factor.

• 한국방재학회 논문집
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• 제10권4호
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• pp.25-32
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• 2010

최근 고강도 및 고내구성에 대한 인식이 높아지면서 고성능 숏크리트에 대한 연구가 일부 진행되기도 하였으나, 국외 선진국에 비하면 아직 초보 단계에 그치고 있다. 즉 강도와 내구성 평가만 일부 이루어졌고, 시공성을 대변하는 펌핑성능(Pumpability)과 뿜칠성능(Shootability)에 대한 평가가 전혀 이루어지지 않았다. 따라서 본 논문의 목표는 국내 습식 숏크리트의 고성능화에서 고시공성에 대한 연구로, 이를 위해 실리카 흄(0.0, 4.5, 9%), AE제(0.0, 0.005%)를 주요 변수로 하여 시공성 평가를 위해서 레오미터를 사용한 레올로지를 측정하였을 뿐만 아니라, 펌프압, 리바운드율, 붙임두께 등을 측정하여 비교고찰 하였다. AE제와 고성능 감수제가 레올로지 특성에 미치는 영향을 고찰한 결과 AE제는 흐름저항(Flow Resistance, G)과 토크점성(Torque Viscosity, H)이 모두 일정하게 감소되었고, 실리카 흄은 흐름저항(G)은 증가 토크점성(H)은 감소한 결과가 나타났다. 펌핑성능과 레올로지 관계에서 토크점도(H)가 증가함에 따라 필요 펌핑 압송력이 상승하는 결과를 얻었고, 뿜칠성능과 레올로지 관계에서는 흐름저항(G)가 증가할수록 최대 붙임두께는 증대 리바운드율은 감소하는 경향을 얻었다.

• 한국윤활학회:학술대회논문집
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• 한국윤활학회 1997년도 제26회 추계학술대회
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• pp.86-92
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• 1997

When Lubricants is used under severe running condition, tribological characteristics is very important. I have studied the lubricating oil viscosity, kinds of additives and lubricating oil temperatures were changed. In order to study the effect of oil temperature on the wear of the surface, the temperature of the oil was changed for the same sample. Moreover, the temperatures of three kinds of oils which have very different viscosities at room temperature, were varied while the oil viscosity was unchanged. It was shown from the test results that wear is not greatly affected by the amount of ZnDTP antiwear agent, but E-P additives are less effective against wear than ZnDTP additives. The viscosity of lubricating oil and its tempea-ature greatly affect the wear of the surface. Combining all the wear data with those of the surface strength, it was observed that the higher the load, the lower the scratch of wear, and also in the case of the same running load, the lower the wear, the longer the life of the surface strength.

• 콘크리트학회논문집
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• 제11권3호
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• pp.153-160
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• 1999

Water soluble hydroxyalkyl methycellulose ethers are used in a variety of applications incluing building industry as a supplementary agent used for incresing adhesives, water retention capacity, workability and viscosity modify. Water retention capacity(WRC) is the capability to contain water in the ploymer chain under condition of being mixed with cement. In general, the WRC is affected by the viscosity, the adding amount, the particle size, the rate of dissolving and the amount of substituted chemical in cellulose ethers. In the other words, WRC is increased as higher the viscosity, more adding amount, finer the particle size and longer the dissolving time of cellulose ethers. This thesis investigated each factor that effect the WRC, particularly the relation between degree of substitution(DS), molar of substitution(MS) and WRC. It is observed that WRC is not nearly affected by DS of cellulose ethers, but is changes proportionally as MS increases in the narrow range(0.10~2.25)