• Food Science and Biotechnology
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• v.18 no.2
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• pp.546-551
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• 2009

The objective of this study was to investigate Fourier transform infrared (FT-IR) spectrometry and the X-ray diffraction (XRD) characterization of melanoidins formed from glucose and fructose with amino acid enantiomers in the Maillard reaction. Before dialysis, FT-IR spectroscopy of all the samples showed that the characteristic absorption intensities appeared as a broad and intense band of the stretching vibration of the -OH group at 3,400/cm for a high pH. The absorption bands of the melanoidins sharply decreased in intensity after dialysis as compared to those before dialysis. In particular, the absorption bands at 992 and 575/cm disappeared. The XRD confirmed that the crystal structure of the melanoidins disappeared after dialysis and a new crystal structure was formed at 9 and $28^{\circ}$ ($2{\theta}$. In particular, broad diffraction peaks were formed in the $10-21^{\circ}$ ($2{\theta}$) range for a high pH, while other sharp diffraction peaks disappeared.

• Elastomers and Composites
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• v.54 no.1
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• pp.1-6
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• 2019

In this study, we measured the leakage current at $30{\sim}80^{\circ}C$ and $90{\sim}170^{\circ}C$ under a voltage of 200~980 V applied to samples (ordinary temperature) and polyamide film specimens degraded at $170^{\circ}C$ for 20 minute respectively. After the specimen was degraded at $130^{\circ}C$ and $50^{\circ}C$, a voltage of 200 to 800 V was applied for 10 to 60 minutes. The measurement of the leakage current resulted in the following conclusions. In the case of using Al and Cu as the main electrode, it was confirmed that the leakage current also increased in high temperatures as the voltage increased. Regardless of the type of main electrode, when the temperature was constant at $130^{\circ}C$ and $50^{\circ}C$, the leakage current increased as the voltage increased, and gradually decreased with time. As a result of the FTIR measurement, the main absorption of the infrared absorption spectrum was C=O at about $1650cm^{-1}$ and N-H diagonal vibration occurred at around $1550cm^{-1}$. There was no change in the material, so no effect of temperature was observed. By the results of SEM measurements, as the temperature of degradation increases, cracks in the specimen disappear. This may be because the amide bond (-CO-NH-) is absorbed by the material.

• Advances in concrete construction
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• v.11 no.1
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• pp.73-80
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• 2021

Rice Husk Ash (RHA) geopolymer paste activated by sodium aluminate were characterized by X-ray diffractogram (XRD), scanning electron microscope (SEM), energy dispersion X-Ray analysis (EDAX)and fourier transform infrared spectroscopy (FTIR). Five series of RHA geopolymer specimens were prepared by varying the Si/Al ratio as 1.5, 2.0, 2.5, 3.0 and 3.5. The paper focuses on the correlation of microstructure with hardened state parameters like bulk density, apparent porosity, sorptivity, water absorption and compressive strength. XRD analysis peaks indicates quartz, cristobalite and gibbsite for raw RHA and new peaks corresponding to Zeolite A in geopolymer specimens. In general, SEM micrographs show interconnected pores and loosely packed geopolymer matrix except for specimens made with Si/Al of 2.0 which exhibited comparatively better matrix. Incorporation of Al from sodium aluminate were confirmed with the stretching and bending vibration of Si-O-Si and O-Si-O observations from the FTIR analysis of geopolymer specimen. The dense microstructure of SA2.0 correlate into better performance in terms of 28 days maximum compressive strength of 16.96 MPa and minimum for porosity, absorption and sorptivity among the specimens. However, due to the higher water demand to make the paste workable, the value of porosity, absorption and sorptivity were reportedly higher as compared with other geopolymer systems. Correlation regression equations were proposed to validate the interrelation between physical parameters and mechanical strength. RHA geopolymer shows comparatively lower compressive strength as compared to Fly ash geopolymer.

• Journal of KSNVE
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• v.6 no.3
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• pp.333-339
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• 1996

The absorption coefficients of 3 largely reticulated urethan foams are measured by transfer function method which uses two microphones in an impedance tube. Based on the previously published data, the new modified empirical equations for predicting the characteristic impedance and propagation constant of the largely reticulated urethane foams are developed. Comparison is made between the measured data and the predicted data, based on the previously published equations and the new equation. Good agreement of the absorption coefficient between the measured and predicted data by the new modified empirical equation has been obtained.

• Journal of KSNVE
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• v.7 no.5
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• pp.781-787
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• 1997

A new method is presented to determine two fundamental acoustic quantities of sound-absorbing materials such as characteristic impedance and propagation constant. In this study, the surface acoustic impedances of sound-absorbing materials are measured using the impedance tube and the anechoic chamber to determine the above acoustic quantities. The measured results are given for two typical sound-absorbing materials(glass wool and urethane foam) int the frequency range between 150 and 1, 600 Hz. The results are verified by other two known methods, which are Smith & Parrott method and Utsuno et al. method. The absorption coefficients calculated from the empirical models(Miki model for glass wool and Jung model for urethane foam) and two quantities by present method are in good agreement with the measured values.

• Transactions of the Korean Society for Noise and Vibration Engineering
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• v.20 no.7
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• pp.651-657
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• 2010

Previous experimental results performed by many researchers for a couple of decades in South Korea have shown that an absorbing sheet inserted in a conventional floating slab system for thermal insulation or vibration absorption may amplify the vibration of the slab system at specific frequency ranges depending on the material properties of the sheet. The amplified vibration, consequently, results in the heavy weight floor impact noise exceeding the sound level limit for an apartment house, 50 dB. In this study, the amplification mechanism is examined through numerical analysis and a new slab system is proposed to reduce the amplification and control the noise. The new slab system consists of studs connecting the base slab and upper concrete finishing yielding the dramatically increased stiffness of the slab. The numerical simulation is performed to investigate the effect of the slab system with studs on the vibration and noise control. The results show that the performance of the slab is sensitive to the number and location of studs, and the heavy weight floor impact noise can be reduced up to 6~7 dB compared to the conventional slab system at the optimal stud location.

• Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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• 1991.04a
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• pp.65-69
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• 1991

소음제어대책 수립시, 흡음구조는 공조용소음기, 공업용소음기, Enclosure, 실 내 흡음판등에 폭넓게 이용되고 있다. 흡음구조의 재료중 글라스울은 뛰어난 흡음성능과 고온에서의 내구성 및 난연성등으로 인하여 여러 흡음재료중에 서 가장 많이 이용되고 있으나 글라스율 미립자의 비산 및 강도문제로 글라 스율에 글라스 클로스(Glass Cloth), P.E.Film등과 같은 글라스울 비산방지막 과 유공함석판을 붙인 흡음구조체로 제작하여 이용하는 것이 일반적이다. 국 내외적으로 글라스울만의 흡음율 데이타는 각종 문헌등에 많이 발표되어 있 으나 글라스울에 글라스울 비산방지막과 유공함석판을 붙인 흡음구조체의 흡음율데이타는 거의 없는 실정이다. 본 연구에서는 이러한 글라스울 흡음구 조체의 글라스울의 밀도, 글라스울 비산방지막의 종류, 유공함석판의 유공치 수 등에 따른 흡음특성을 잔향실법 흡음율측정방법에 의해 측정 평가하고 이들을 상호 비교검토하여 각종 소음 제어대책의 기초 설계자료로 제시하고 자 한다.

• Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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• 2007.11a
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• pp.824-828
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• 2007

In this paper Statistical Energy Analysis has been considered to predict middle, high frequency air borne interior noise. PIM method is used for verification. Damping loss factor and coupling loss factor have been derived from the response(SPL) of sub systems when the power is applied. The airborne SEA model of vehicle is modeled through AutoSea2. Insulation material's absorption coefficient and transmission loss are acquired from closed form solution and experiment.

• Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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• 2007.11a
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• pp.960-963
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• 2007

In this paper, development of the noise barrier analysis program is described. The upper part of barriers may have complicated shapes like "Y", "T", inverted L, and other shapes. The insertion loss of the barrier is predicted by summation of multiple diffractions occurring at top edge points. In addition, the program considers diffractions occurring at both vertical sides, while reflections from ground due to mirror images are also included. In case of two barriers at both sides of the road, reflections from the other side of barriers are considered, in which magnitudes are decreased by the ratio of absorption coefficient.

• Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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• 2008.11a
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• pp.152-157
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• 2008

Enclosure is widely used for the sound insulation in a ship. But it is very difficult to estimate the sound insertion loss for the enclosure because the sound field between the enclosure and the machine is so complex. Therefore, it is usually estimated experimentally. In this research, sound insertion loss of the enclosure is estimated by theory assuming that the sound field in the enclosure is reverberation field. And the results from the theory are compared to those from the experiment.