• Title/Summary/Keyword: Various temperature

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Radio iodination (II) Radio iodination of various aromatic derivatives in organic solvent at low temperature (放射性 요오드化 反應 (第 II 報) 有機容媒 中에서의 各種 芳香誘導體의 低溫 요오드化 反應)

  • Kim, You-Sun;Kim, Chong-Doo
    • Journal of the Korean Chemical Society
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    • v.12 no.1
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    • pp.35-38
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    • 1968
  • Radio iodination of various aromatic derivatives (aniline, toluene, iodobenzene, acetanilide, benzene, benzoic acid) were achieved at low temperature by a chloroamine-T procedures in presence of polar solvent(dioxane). Organic base (piperidine) was used as the catalyst. Iodine replacement reaction had occured on the aromatic or alicyclic ring by this reaction, and the kind and ratio of iodinated products were proved to be different from those of usual iodide reaction in organic solvent at low temperature. The reactivity of various aromatic or alicyclic compounds towards the present iodination system was evaluated and the scope and limitation of the present procedures in the preparation of radio pharmaceuticals were discussed.

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Analysis of MICC, ELA TFT performance transition according to substrate temperature and gate bias stress time variation (온도 변화 및 Gate bias stress time에 따른 MICC, ELA TFT성능 변화 비교 분석)

  • Yi, Seung-Ho;Lee, Won-Baek;Yi, Jun-Sin
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2010.06a
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    • pp.368-368
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    • 2010
  • Using TFTs crystallized by MICC and ELA, electron mobility and threshold voltage were measured according to various substrate temperature from $-40^{\circ}C$ to $100^{\circ}C$. Basic curve, $V_G-I_D$, is also measured under various stress time from 1s to 10000s. Consequently, due to the passivation effect and number of grains, mobility of MICC is varied in the range of -8% ~ 7.6%, while that of ELA is varied from -11.04% ~ 13.25%. Also, since $V_G-I_D$ curve is dominantly affected by grain size, active layer interface, the graph remained steady under the various gate bias stress time from 1s to 10000s. This proves the point that MICC can be alternative technic to ELA.

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Setting Properties of High Aluminate Composite According to Various Temperature and Components

  • Li, Mao;Kim, Jin-Man;Choi, Sun-Mi;Lee, Dong-Won
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2016.05a
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    • pp.36-37
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    • 2016
  • Among all the slags, ladle furnace slag (LFS) is reducing slag generated from electric arc furnace. After cooled rapidly by high-pressured air (atomizing technology), LFS has more amorphous phase than slow cooled slag. Therefore, it shows higher reactivity than another recycling slag. This material also is named by rapid cooling LFS (RC-LFS). Pulverized RC-LFS should be fully understood. This paper deal with the present some basic experimental properties and discussions about the setting time of pulverized RC-LFS with different gypsum under the various temperatures. According to the experimental results, the pulverized RC-LFS with gypsum can hydrate in a low-temperature environment, even though the initial and final setting time are delayed.

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Modeling for Frost Growth on a Cold Plate (냉각 평판에서 서리 성장 모델링)

  • Yang, Dong-Keun;Lee, Kwan-Soo
    • Proceedings of the KSME Conference
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    • 2004.04a
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    • pp.1546-1551
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    • 2004
  • This paper presents a mathematical model to predict the frost properties and heal and mass transfer within the frost layer formed on a cold plate. The laminar flow equations for the air-side are analyzed. and the empirical correlations of local frost properties are employed in order to predict the frost layer growth. The correlations of local frost density and effective thermal conductivity of frost layer, obtained from various experimental conditions, are derived as functions of various frosting parameters (Reynolds number, frost surface temperature, absolute humidity and temperature of moist air, cooling plate temperature, and frost density). The numerical results are compared with experimental data and the results of various models to validate the present model, and agree well with experimental data within a maximum error of 10%. The heat and mass transfer coefficients obtained from the numerical analyses are presented, as the results, it is found that the model for frost growth using the correlation of heat transfer coefficient without solving air flow have a limitation in its application.

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Influence of Substrate Temperature on the TiC Thin Films Prepared by Unbalanced Magnetron Sputtering Method (비대칭 마그네트론 스퍼터링 방법으로 제조된 TiC 박막의 기판온도 영향)

  • Park, Yong-Seob;Lee, Jae-Hyeong
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.62 no.2
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    • pp.284-287
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    • 2013
  • In this work, we have fabricated TiC films by using unbalanced magnetron sputtering method with graphite and Ti targets for contact strip application of electric railway. TiC films were deposited with various substrate temperatures. We investigated various properties of TiC films prepared with various substrate temperatures, such as the hardness, surface roughness, friction coefficient, resistivity, FESEM (Field Emission Scanning Electron Microscopy), HRTEM (High Resolution Transmission Electron Microscopy) and XPS (X-ray Photoelectron Spectroscopy). The hardness and friction coefficient properties of TiC films were improved with increasing substrate temperature. These results indicate that the improvement of hardness and resistivity is related to the increase of sp2 clusters in TiC films. And also, the resistivity value of TiC films were decreased with increasing substrate temperature.

A Study of Evaporation and Ignition Characteristics of Single Fuel Droplet (단일액적의 증발 및 착화특성에 관한 연구)

  • 백병준
    • Journal of Advanced Marine Engineering and Technology
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    • v.22 no.4
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    • pp.551-559
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    • 1998
  • Evaporation and ignition characteristics of fuel droplet have major influences on the efficiency and performance of engine. In the present study the experiment of evaporation and self-ignition of single fuel was performed under the various ambient conditions. An individually suspended droplet of n-heptane n-hexadecane ethyl-alcohol and light oil were employed as a liquid droplet. Evaporation and ignition characteristics were measured by using the video-camera and image processing technique under the various ambient temperatures (up to 1000310 OC)and partial pressure of oxigen(up to 60%) The evaporation curve shows that the droplet life time ignition delay time decreases as the ambient temperature and partial pressure of oxigen increase, The temperature variations of droplet were also reported for various fuel and ambient temperatures. The numerical simulations were carried out to predict droplet diameter and temperature with favorable agreement.

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Numerical Study on the Thermal Characteristics of the Various Cooling Methods in Electronic Equipment

  • Son, Young-Seok;Shin, Jee-Young
    • Journal of Advanced Marine Engineering and Technology
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    • v.28 no.1
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    • pp.46-55
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    • 2004
  • Thermal characteristics of the various cooling methods in electronic equipment are studied numerically. A common chip cooling system is modeled as a parallel channel with protruding heat sources. A two-dimensional model has been developed for the numerical analysis of compressible. viscous. laminar flow. and conjugate heat transfer between parallel plates with uniform block heat sources. The finite volume method is used to solve this problem. The assembly consists of two channels formed by two covers and one printed circuit board that is assumed to have three uniform heat source blocks. Various cooling methods are considered to find out the efficient cooling method in a given geometry and heat sources. The velocity and the temperature fields. the local temperature distribution along the surface of blocks. and the maximum temperature in each block are obtained. The results are compared to examine the thermal characteristics of the different cooling methods both quantitatively and qualitatively.

Redox Property of Vanadium Oxide and Its Behavior in Cataltic Oxidation

  • 김영호;이호인
    • Bulletin of the Korean Chemical Society
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    • v.20 no.12
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    • pp.1457-1463
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    • 1999
  • Structure and their redox property of the vanadium oxides prepared by decomposing NH₄VO₃ at various temperatures were studied by XRD, SEM, XPS, and temperature programmed reduction/temperature programmed oxidation (TPR/TPO) experiment. All TPR profiles have two sharp peaks in the temperature range 650-750℃, and the area ratio of the two sharp peaks changed from sample to sample. There were three redox steps in TPR/TPO profiles. The oxidation proceeded in the reverse order of the reduction process, and both the reactions proceeded via quite a stable intermediates. The changes of the morphological factor $(I_{(101)}/I_{(010)})$, the ratio of $O_{1S}$ peak area (O$_{1S}$( α)/O$_{1S}$( β)) in the XPS results, and the ratio of hydrogen consumption in TPR profiles with various vanadium oxides showed the distinct relationship between the structural property and their redox property of vanadium oxides. The change of the specific yield of phthalic anhydride with various vanadium oxides showed a very similar trend to those of the peak area ratio in TPR profiles, which meant that the first reduction step related to the partial oxidation of o-xylene on the vanadium oxide catalyst.

Investigation of Standard Error Range of Non-Contact Thermometer by Environment (외부 환경 변화에 의한 비 접촉 체온계의 오차 범위 측정)

  • Kim, Jeongeun;Park, Sangwoong;Choi, Heakyung
    • Journal of The Korean Society of Integrative Medicine
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    • v.8 no.4
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    • pp.307-321
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    • 2020
  • Purpose : A person infected by SARS-CoV2 may present various symptoms such as fever, pain in lower respiratory tract, and pneumonia. Measuring body temperature is a simple method to screen patients. However, changes in the surrounding environment may cause errors in infrared measurement. Hence, a non-contact thermometer controls this error by setting a correction value, but it is difficult to correct it for all environments. Therefore, we investigate device error values according to changes in the surrounding environment (temperature and humidity) and propose guidelines for reliable patient detection. Methods : For this study, the temperature was measured using three types of non-contact thermometers. For accurate temperature measurement, we used a water bath kept at a constant temperature. During temperature measurement, we ensured that the temperature and humidity were maintained using a thermo-hygrometer. The conditions of the surrounding environment were changed by an air conditioner, humidifier, warmer, and dehumidifier. Results : The temperature of the water bath was measured using a non-contact thermometer kept at various distances ranging from 3~10 cm. The value measured by the non-contact thermometer was then verified using a mercury thermometer, and the difference between the measured temperatures was compared. It was observed that at normal surrounding temperature (24 ℃), there was no difference between the values when the non-contact thermometer was kept at 3 cm. However, as the distance of the non-contact thermometer was increased from the water bath, the recorded temperature was significantly different compared with that of mercury thermometer. Moreover, temperature measurements were conducted at different surrounding temperatures and the results obtained significantly varied from when the thermometer was kept at 3 cm. Additionally, it was observed that the effect on temperature decreases with an increase in humidity Conclusion : In conclusion, non-contact thermometers are lower in lower temperature and dry weather in winter.

Influences of Various Electrolytes on the Low-Temperature Characteristics of Ni-MH Secondary Battery (Ni-MH 2차 전지의 저온특성에 미치는 전해액의 영향)

  • Park, Chae-Gyu;Shim, Jong-Su;Jang, Min-Ho;Park, Choong-Nyeon;Choi, Jeon
    • Journal of Hydrogen and New Energy
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    • v.18 no.3
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    • pp.284-291
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    • 2007
  • The Ni-MH batteries for HEV and industry are normally placed in outdoor, consequently causing an too weak discharge power problem due to a cold weather specially in winter time. In order to improve the low temperature performances of the Ni-MH battery for HEV and industrial uses, it has been investigated the low temperature discharge characteristics of Ni-MH battery with various electrolytes at $-18^{\circ}C$. The summary of experimental results are as follows. The low temperature characteristics depended strongly on the characteristics of electrolytes. When the concentration of the electrolytes were too high or too low the low temperature performance was poor. The best electrolyte was composed of KOH 6.2M+LiOH 1.2M. An addition of RbOH or CsOH to electrolyte improved the low temperature performance. The best total concentration of electrolyte composed of KOH, NaOH and LiOH was about 7M.