• Title/Summary/Keyword: Vacuum Hot Pressing

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The Compressive Deformation Behavior of Nanocrystalline Al-5at.%Ti Alloy Prepared by Mechanical Alloying at Low Temperature (저온 기계적 합금화한 nanocrystalline Al-5at.%Ti 합금의 압축변형거동)

  • 정경화;오영민;김선진
    • Journal of Powder Materials
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    • v.6 no.4
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    • pp.277-285
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    • 1999
  • Mechanical properties of nanocrystalline Al-5at.%Ti alloy were investigated through high temperature compression test. Al-5at.%Ti nanocrystalline metal powders, which had finer and more equiaxed shape than those produced at room temperature, were produced by mechanical alloying at low temperature. The powders were successfully consolidated to 99fo of theoretical density by vacuum hot pressing. XRD and TEM analysis revealed that $Al_3Ti$ intermetallic compounds formed inside powders and pure Al region with coarse grains formed between powders, especially at triple junction. Mechanical properties in terms of hardness and strength were improved by grain size refinement, but ductility decreased presumably due to the formation of the weak interfaces between Al pool and powders.

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Elevated Temperature Compressive Properties of Al-Ti Alloys Prepared by Mechanical Alloying (기계적 합금화에 의해 제조된 AS-Ti합금의 고온압축성질)

  • 이광민
    • Journal of Powder Materials
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    • v.5 no.2
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    • pp.129-132
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    • 1998
  • The elevated temperature compressive tests were carried out in order to investigate the deformation behavior and microstructural characteristics of Al-8%Ti, Al-12%Ti and Al-16%Ti (wt%) alloys, which were mechanically alloyed and consolidated by vacuum hot pressing, A13Ti intermetallic phases were formed with sizes of few hundred nanometers in the mechanically alloyed Al-Ti alloys. The compressive strength of mechanically alloyed AA-Ti alloys increased with decroasing the temperature and with increasing the strain rate. The strain rate sensitivities of Al-8%Ti, Al-12%Ti and Al-16%Ti alloys were measured 0.02,0.03, and 0.14, respectively, at 35$0^{\circ}C$.

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Toughening of Ni Bonded $Cr_3C_2$ by Mo Particulates (Mo 입자에 의한 Ni 결합 $Cr_3C_2$의 고인성화)

  • 한동빈;장철우;백성기;박병학
    • Journal of the Korean Ceramic Society
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    • v.30 no.6
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    • pp.429-432
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    • 1993
  • Cr3C2 material is characterized by high chemical stability and poor sinterability with low strength [50~150MPa]. In his study, low melting temperature nickel powder was used to improve sinterability as well as strength. In addition, molydenum particles were added to the Ni-bonded Cr3C2 cermet pseudomatrix to increase resistance to fracture. The specimens made by hot-pressing under vacuum and strength was measured by 4-point bending. Indentation cracking and fractographic examination were conducted to study the interaction of the indentation cracks with the reinforcing particles. Toughening mechanisms and failure will be discussed in terms of crack/particle interactions and compared with previous works.

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Properties on Hysteresis and Aging phenomenon of 9.5/65/35 PLZT (9.5/65/35 PLZT의 HYSTERESIS와 AGING현상에 관한 연구)

  • Lee, H.G.;Kim, S.Y.;Song, J.T.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1993.05a
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    • pp.88-91
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    • 1993
  • In this study 9.5/65/35 PLZT was selected which has the excellent quadratic electro-optic property and slim-loop. It was fabricated by the methods of vacuum hot-pressing and sintering. The electrode of color filter was evaporated using the interdigital type masks. Hysteresis and transmission characteristics were measured. The coercive field and the nontransmited field were correlative. Aging effect was measured according to time at same temperature. Wavelengths of RGB were chosen 700[nm] for red, 545[nm] for green and 435[nm] for blue by the standard of the Commission Internationale del Eclaiage.

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A Study on Synthesis and Characterization of $Ti_xZr_{1-x}C$ Solid-Solution by Self-propagation High Temperature Synthesis Method (SHS법에 의한 $Ti_xZr_{1-x}C$ 고용체의 합성 및 특성 연구)

  • 이형복;오유근;이성민
    • Journal of the Korean Ceramic Society
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    • v.34 no.7
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    • pp.731-737
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    • 1997
  • TixZr1-xC(0$0^{\circ}C$, 5.1 mm/sec respectively. The relative density, three point flexural strength, and the hardness of composites, which was sintered at 190$0^{\circ}C$ for 60 min by using hot-pressing under a pressure of 30 MPa, were 99%, 525 MPa and 24 GPa respectively.

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A study on properties optical transparency effect and Hysteresis of transparent PLZT (투광성 PLZT의 HYSTERESIS와 광투과 효과에 과한 연구)

  • Lee, H.G.;Kim, S.Y.;Song, J.T.
    • Proceedings of the KIEE Conference
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    • 1993.07a
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    • pp.21-23
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    • 1993
  • In this study PLZT was selected which has the excellent quadratic electro-optic property and slim-loop. It was fabricated by the methods of vacuum hot-pressing and sintering. The electrode of color filter was evaporated using the interdigital type masks. Through XRD have we investigated the molecular structure composition formular. Hysteresis and transmission characteristics were measured, The transmission of RGB was envestigated. We are going to study the correlation of coercive field and the nontransmited field.

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Factors Affecting Longitudinal Tensile Strength of SiC/Ti-Al-V Composites Manufactured by Plasma Spraying

  • Baik, Kyeong-Ho
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.514-515
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    • 2006
  • In this study, multi-ply SiC fiber reinforced Ti-6Al-4V composites have been manufactured by plasma spraying and subsequent vacuum hot pressing. Two different sizes of Ti-6Al-4V feedstock powders were used for plasma spraying to form matrix. A considerable amount of oxygen was incorporated into as-sprayed Ti matrix during plasma spraying, and consequently caused matrix embrittlement. The use of coarse-sized feedstock powder reduced oxygen contamination, but tended to increase fiber spacing irregularity and fiber strength degradation. Longitudinal tensile strength and ductility of the composites were mainly affected by the matrix oxygen content.

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A study on properties optical transparency effect and Hysteresis of transparent PLZT (투광성 PLZT의 HYSTERESIS와 광투과 효과에 관한 연구)

  • Lee, H.G.;Kim, S.Y.;Song, J.T.
    • Proceedings of the KIEE Conference
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    • 1993.07b
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    • pp.555-557
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    • 1993
  • In this study PLZT was selected which has the excel lent quadratic electro-optic property and slim-loop. It was fabricated by the methods of vacuum hot-pressing and sintering. The electrode of color filter was evaporated using the interdigital type masks. Through XRD have we investigated the molecular structure composition formular. Hysteresis and transmission characteristics were measured. The transmission of RGB was envestigated. We are going to study the correlation of coercive field and the nontransmited field.

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Tribological Properties of the Aluminum Short fiber and glass fiber Reinforced Tin-Bronze Matrix Composites (알루미나 단섬유 및 유리섬유 보강 청동기지 복합재의 마모특성 연구)

  • 황순홍;안병길;이범주;최웅수;허무영
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 1996.04b
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    • pp.13-19
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    • 1996
  • The tribological properties of the aluminum short fiber and glass fiber reinforced tin-bronze matrix composites manufactured by vacuum hot pressing was studied. The effect of the composition and the relative density on the wear properties was examined by a reciprocal type tribo-test machine. The results were discussed by the observation of the microstructure of sintered specimen and worn surface observation using SEM and EDS. Addition of the fibers led to the wear resistance since the metal matrix was reinforced by the fibers. The reinforcement of the fiber seemed to be stronger as the distribution of the fibers was more uniform. Graphite also reduce the wear loss. The pores in the sintered composites seemed to play an important role to improve the wear resistance since the pores provide the places where the solid lubricants locate.

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Phase Transformation and Thermoelectric Properties of N-tyre β Processed by Mechanical Alloying (기계적 합금화로 제조한 N형 β의 상변화 및 열전 특성)

  • Eo, Sun-Cheol
    • Korean Journal of Materials Research
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    • v.12 no.5
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    • pp.375-381
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    • 2002
  • N-type ${\beta}-FeSi_2$ with a nominal composition of $Fe_{0.98}Co_{0.02}Si_2$ powders has been produced by mechanical alloying process and consolidated by vacuum hot pressing. As-milled powders were of metastable state and fully transformed to ${\beta}-FeSi_2$ phase by subsequent isothermal annealing. However, as-consolidated $Fe_{0.98}Co_{0.02}Si_2$ consisted of untransformed mixture of ${\alpha}-Fe_2Si_ 5$ and $\varepsilon$-FeSi phases. Isothermal annealing has been carried out to induce the transformation to a thermoelectric semiconducting ${\beta}-FeSi_2$ phase. The transformation behavior of ${\beta}-FeSi_2$ was investigated by utilizing DTA, a modified TGA under magnetic field, SEM, and XRD analyses. Isothermal annealing at $830^{\circ}C$ in vacuum led to the thermoelectric semiconducting ${\beta}-FeSi_2$ phase transformation, but some residual metallic $\alpha$ and $\varepsilon$ phases were unavoidable even after prolonged annealing. Thermoelectric properties were remarkably improved by isothermal annealing due to the transformation from metallic $\alpha$ and $\varepsilon$ phases to semiconducting phases.