• 제목/요약/키워드: Vacuum Evaporation

검색결과 529건 처리시간 0.033초

LCD 식각폐액으로부터 질산과 초산의 분리 (Separation of Nitric Acid and Acetic Acid from the Waste Acid in LCD Etching Process)

  • 전희동;노유미;박성국;김주한;신창훈;김주엽;안재우
    • 청정기술
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    • 제14권2호
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    • pp.123-128
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    • 2008
  • LCD 제조공정에서 배출되는 폐에칭액으로부터 조(粗)인산 회수 후 잔류하는 질산, 초산 혼산폐액을 분리하여 자원화함으로써 고부가가치화하고 2차 폐수의 발생이 없는 친환경적인 청정 재활용기술을 개발하고자 진공증발을 이용하여 혼산폐액을 분리하였다. 진공도 -760 mmHg 조건에서 온도의 따른 진공증발 결과 $33^{\circ}C$ 이하에서는 초산만 증발되었으나 $33^{\circ}C$ 이상에서는 초산과 함께 질산이 미량 증발되었다. 초산 회수율을 높이고 질산 증발을 억제하기 위하여 -760 mmHg, $40^{\circ}C$ 조건으로 증발시간에 따른 증발거동을 조사하고 회수되는 증발량을 고려하여 추가로 물과 원액을 공급하였다. 또한 질산만 선택적으로 반응하도록 20 g/L NaOH를 소량씩 단계적으로 공급하였다. 질산 증발은 batch type 에서는 7%이었으나, 물 추가 시 0.78%, 원액 추가 시 0.25%까지 감소하였다. 20 g/L NaOH를 소량씩 단계적으로 공급한 결과 초산 회수율은 100%까지 증가하였으며, 질산은 6.22%까지 증발하였다.

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LNG 벙커링용 고효율 LNG 저장탱크 열해석 (Thermal analysis of LNG storage tank for LNG bunkering system)

  • 윤상국
    • Journal of Advanced Marine Engineering and Technology
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    • 제39권9호
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    • pp.876-880
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    • 2015
  • IMO의 규제인 신조 선박에 대한 NOx 80% 감축의 2016년 발효를 앞두고, 청정에너지인 LNG연료 선박 및 벙커링 선박의 보급이 유럽 선진국들을 중심으로 추진되고 있다. LNG 저장탱크는 LNG 벙커링의 필수 설비로 현재의 액체질소 등을 저장하는 극저온 액체 저장탱크와 동일한 구조이며, IMO의 "C"형 가압탱크인 내외 용기로 구성된 2중 탱크에 진공펄라이트 단열재가 충전되는 형식이다. 그러나 이 단열방식은 진공작업이 어렵고 일 LNG 기화량이 2.0 % 내외가 되어 보다 고효율의 탱크가 요구되어 진다. 본 연구에서는 진공과 단열재를 분리하여 내외탱크에 고진공을 적용하고 외부 탱크에 우레탄폼을 가설시킨 탱크 단열 방식을 새로이 고안하여 열해석을 수행하였다. 해석결과 본 개발 탱크는 진공도가 $10^{-3}Torr$ 이하일 때 일 기화량이 0.03 % 이하로 매우 적게 유지될 수 있고, $10^{-4}Torr$ 이하가 되면 일 기화량이 0.11 %가 되었다. 진공이 파괴되는 경우에도 현재 진공펄라이트 단열은 일 4.9 %의 증발이 발생하나, 새 고안 탱크는 일 증발율이 4.12 %가 되는 매우 효율이 높고 안전한 LNG 탱크 단열방식이 되었다.

진공고주파를 이용한 일체형 건조기개발에 관한 연구 (A Study on an Integrated Drying Machine with Microwave at Vacuum Conditions)

  • 김태형;고광수;박윤철
    • 설비공학논문집
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    • 제26권9호
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    • pp.441-446
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    • 2014
  • In Jeju province, the Citrus is widely spread crop which is the most popular fruit on the island. When the quality of a Citrus is not in a good condition or when its size exceeds or is lower than the set criteria, it is discarded as a waste. In this study, a drying machine for waste Citrus has been developed with 2.6 GHz microwave energy supply to the Citrus at vacuum environment. The vacuum environment of the drying chamber was maintained to reduce the energy supply to the Citrus by lowering the evaporating temperature of the water. The experiment was conducted with variation of the vacuum pressure, interior temperature of the drying chamber, and operating time of the microwave. As a result, the effect of the temperature was shown to be higher than the other two control methods, and it showed with 0.305 g/W evaporation efficiency.

Formation of Plasma Damage-Free ITO Thin Flims on the InGaN/GaN based LEDs by Using Advanced Sputtering

  • Park, Min Joo;Son, Kwang Jeong;Kwak, Joon Seop
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2013년도 제44회 동계 정기학술대회 초록집
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    • pp.312-312
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    • 2013
  • GaN based light emitting diodes (LEDs) are important devices that are being used extensively in our daily life. For example, these devices are used in traffic light lamps, outdoor full-color displays and backlight of liquid crystal display panels. To realize high-brightness GaN based LEDs for solid-state lighting applications, the development of p-type ohmic electrodes that have low contact resistivity, high optical transmittance and high refractive index is essential. To this effect, indiumtin oxide (ITO) have been investigated for LEDs. Among the transparent electrodes for LEDs, ITO has been one of the promising electrodes on p-GaN layers owing to its excellent properties in optical, electrical conductivity, substrate adhesion, hardness, and chemical inertness. Sputtering and e-beam evaporation techniques are the most commonly used deposition methods. Commonly, ITO films on p-GaN by sputtering have better transmittance and resistivity than ITO films on p-GaN by e-bam evaporation. However, ITO films on p-GaN by sputtering have higher specific contact resistance, it has been demonstrated that this is due to possible plasma damage on the p-GaN in the sputtering process. In this paper, we have investigated the advanced sputtering using plasma damage-free p-electrode. Prepared the ITO films on the GaN based LEDs by e-beam evaporation, normal sputtering and advanced sputtering. The ITO films on GaN based LEDs by sputtering showed better transmittance and sheets resistance than ITO films on the GaN based LEDs by e-beam evaporation. Finally, fabricated of GaN based LEDs by using advanced sputtering. And compared the electrical properties (measurement by using C-TLM) and structural properties (HR-TEM and FE-SEM) of ITO films on GaN based LEDs produced by e-beam evaporation, normal sputtering and advanced sputtering. As a result, It is expected to form plasma damage free-electrode, and better light output power and break down voltage than LEDs by e-beam evaporation and normal sputter.

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Numerical Analysis on the Flow Characteristics in Steam Ejector

  • Shin, You-Sik;Jin, Zhen-Hua;Chun, You-Sin;Lee, Sang-Chul;Jeong, Hyo-Min;Chung, Han-Shik
    • 대한설비공학회:학술대회논문집
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    • 대한설비공학회 2006년도 하계학술발표대회 논문집
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    • pp.749-754
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    • 2006
  • This study performed of a water cooling system by using a steam ejector and jet condenser to drop the temperature of the water in aquafarm by about $5^{\circ}C$ from $25^{\circ}C$ or higher in this research, to replace the present water cooling system, Ive focused on a water cooling system operated by latent heat of evaporation, thus this system needs a vacuum pressure to evaporate the water in enclosed tank. The water cooling effects are dependent on the vacuum pressure in the enclosed tank, and the cooling water is generated by evaporation. As the experimental results, the absolute vacuum pressure obtained was about $5{\sim}8mmHg$ using a steam driven ejector with jet condenser in experiments. The obtained results are respectively ${\Delta}T=7^{\circ}C$, ${\Delta}T=5^{\circ}C$ and ${\Delta}T=5.5^{\circ}C$ at heat exchanger flow rate 4L/M. The obtained results are respectively ${\Delta}T=5.5^{\circ}C$, ${\Delta}T=5.5^{\circ}C$ and ${\Delta}T=5.5^{\circ}C$ at heat exchanger flow rate 4.5L/M.

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