• Title/Summary/Keyword: Vacuum Consolidation

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Thermoelectric Properties of Half-Heusler TiCoSb Synthesized by Mechanical Alloying Process

  • Ur, Soon-Chul
    • Korean Journal of Materials Research
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    • v.21 no.10
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    • pp.542-545
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    • 2011
  • Half-Heusler alloys are a potential thermoelectric material for use in high-temperature applications. In an attempt to produce half-Heusler thermoelectric materials with fine microstructures, TiCoSb was synthesized by the mechanical alloying of stoichiometric elemental powder compositions and then consolidated by vacuum hot pressing. The phase transformations during the mechanical alloying and hot consolidation process were investigated using XRD and SEM. A single-phase, half- Heusler allow was successfully produced by the mechanical alloying process, but a minor portion of the second phase of the CoSb formation was observed after the vacuum hot pressing. The thermoelectric properties as a function of the temperature were evaluated for the hot-pressed specimens. The Seebeck coefficients in the test range showed negative values, representing n-type conductivity, and the absolute value was found to be relatively low due to the existence of the second phase. It is shown that the electrical conductivity is relatively high and that the thermal conductivities are compatibly low in MA TiCoSb. The maximum ZT value was found to be relatively low in the test temperature range, possibly due to the lower Seebeck coefficient. The Hall mobility value appeared to be quite low, leading to the lower value of Seebeck coefficient. Thus, it is likely that the single phase produced by mechanical alloying process will show much higher ZT values after an excess Ti addition. It is also believed that further property enhancement can be obtained if appropriate dopants are selectively introduced into this MA TiCoSb System.

Research for a cases of overseas constructions and domestic tentative execution about high vacuum dewatering and consolidation/dehydration by Super Well point method (슈퍼웰포인트공법에 의한 고진공배수 압밀탈수에 대한 시공사례)

  • Shin, Chang-Beom;Kim, Dae-Hwal;Takahashi, Shigeyoshi;Lee, Kwang-Yeol
    • Proceedings of the Korean Geotechical Society Conference
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    • 2008.10a
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    • pp.581-590
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    • 2008
  • A SWP method is a revolutionary dewatering method. The conventional dewatering method, deep-well method, had ever occurred a civil appeal caused by the well depletion in compliance with the reduction of the groundwater level over a wider area considerably by the deep-well pumping from homogeneous sand-layer ground for a dry-work, while pump groung excavation working in Sendai city, Japan 10 years ago. it'd developed with the problematic proposal to find the new method which can lower the groundwater level only within the sheet pile without any reduction of groundwater outside of the sheet pile and until currently steady improvement came. It's been confirmed with plenty of executional results that there was almost no decreasing of water-level from surroundings, over so many construction-sites including vertical shafts which completely does not enter into non-water permeable layer and pumping ground etc. The SWP method in this time has been introducing initially and carried into a the execution tentatively at a construction-site and made a various result get through the execution.

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Binderless Consolidation of Fine Poly-Si Powders for the Application as Photovoltaic Feedstock (태양전지(太陽電池) 원재료(原材料)로 사용(使用)하기 위한 폴리실리콘 미세분말(微細粉末)의 무점결제(無粘結劑) 성형(成形))

  • Shin, Je-Sik;Kim, Dae-Suk;Kim, Ki-Young;Shon, In-Jin;Moon, Byung-Moon
    • Resources Recycling
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    • v.18 no.1
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    • pp.38-43
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    • 2009
  • In this study, binderless consolidation processes of ultra foe Si powder, by-products of making high purity poly-Si in the current method, were systematically investigated for use as economical solar-grade feedstock. The average diameter of the silicon powder was $7.8{\mu}m$. The main contaminants of the fine silicon powder were $SiO_2$ type oxide and humidity. The chemical pretreatment using the HF solution was observed to be effective for the improvement of the compactability of the silicon powder and the density ratio and the strength of the silicon powder compacts. The yield of the binder-free consolidation process increased by 20% under a vacuum condition. In as-received state, the silicon powder were not pure enough to be used as solar grade feed-stock material. After the dry chemical treatments, a sufficiently high purity above solar-grade was able to be achieved.

A Study on the Performance of Vacuum Preloading with Vertical Drains (수직배수를 병행한 진공압밀공법 적용시의 연약지반 거동 예측 연구)

  • Park, Jung-Bae;Kim, Seung-U;Kim, Yu-Seok
    • Geotechnical Engineering
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    • v.12 no.5
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    • pp.79-88
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    • 1996
  • In this study, prediction of soil behavior under vacuum preloading with vertical drain is explored on the basis of numerical models and toe results were compared with field measurements. Reasonable prediction of the time rate of settlements and pore pressure dissipation under vacuum preloading is the maj or concern. The conventional method for vatsuum preloading is based on modeling vacuum preloading as surcharge loading for the consolidation analysis. However, this modeling may violate the real behavior of soils under vacuum loading since the total stress in the analysis varies due to the modeled surcharge loading whereas in'.situ total stress of soils under vacuum loading is constant. In this study a new method is suggested. Instead of modeling vacuum loading as surcharge loading, negative hydraulic head is applied at the surface drain boundary to simulate the vacuum preloading. Comparisons of predictions and field measurements of soil behavior under vatsuum preloading are presented and the usefulness of the new modeling technique is demonstrated.

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Mechanical Alloying and the Consolidation Behavior of Nanocrystalline $Ll_2$ A$1_3$Hf Intermetallic Compounds (Cu 첨가에 따른 nanocrystalline ${Ll_2}{Al_3}Hf$ 금속간 화합물의 기계적 합금화 거동 및 진공열간 압축성형거동)

  • Kim, Jae-Il;O, Yeong-Min;Kim, Seon-Jin
    • Korean Journal of Materials Research
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    • v.11 no.8
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    • pp.629-635
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    • 2001
  • To improve the ductility of $A1_3Hf$ intermetallics, which are the potential high temperature structural materials, the mechanical alloying behavior. the effect of Cu addition on the $Ll_2$ phase formation and the behavior of vacuum hot-pressed consolidation were investigated. During the mechanical alloying by SPEX mill, the $Ll_2 A1_3Hf$ intermetallics with the grain size of 7~8nm was formed after 6 hours of milling in Al-25at.%Hf system. The $Ll_2$ Phase of Al_3Hf$ intermetallics with the addition of 12.5at.%Cu, similar to that of the binary Al-25at.% Hf, was formed, but the milling time necessary for the formationof the $Ll_2$ phase was delayed form 6 hours to 10 hours. The lattice parameter of ternary $Ll_2(Al+Cu)_3Hf$ intermetallics decreased with the increase of Cu content. The onset temperature of $Ll_2$ to $D0_{23}$ phase in $Al_3Hf$ intermetallics was around 38$0^{\circ}C$, the temperature upon completion varied from 48$0^{\circ}C$ to 5$50^{\circ}C$ as the annealing time. The onset temperature of $Ll_2$ to $D0_{23}$ phase transformation in $(Al+ Cu)_3Hf$ intermetallics increased with the amount of Cu and the highest onset temperature of $700^{\circ}C$ was achieved by the Cu addition of 10at.%. The relative density increased from 89% to 90% with the Cu addition of 10at.% in $Al_3Hf$ intermetallics hot-pressed in vacuum under 750MPa at 40$0^{\circ}C$ for 3 hours. The relative density of 92.5% was achieved without the phase transformation and the grain growth as the consolidation temperature increased from 40$0^{\circ}C$ to 50$0^{\circ}C$ in $(Al+Cu)_3Hf$ intermetallics hot-pressed in vacuum under 750MPa for 3 hours.

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A Study of Cleaning Method of Excavated Gold Brocade (출토 직금직물의 세척방법에 관한 연구)

  • Hong, Moon-Kyung;Lee, Mee-Sik
    • Journal of the Korean Society of Clothing and Textiles
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    • v.34 no.7
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    • pp.1162-1174
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    • 2010
  • Excavated gold brocade, often shows signs of serious damage and contamination from environmental factors such as exposure to soil or human remains. Therefore, most of the conservation procedures are focused on the consolidation of the gold thread and on cleaning with water or organic solvents. Indiscreet cleaning using solvents could damage the gold leaf, which identifies the features of fabric. There is a need to develop cleaning protocols appropriate for relics through the careful analysis of the condition of the relics. This study finds the appropriate cleaning method for the excavated gold brocade. Four different cleaning methods, vacuum cleaning, kneaded rubber eraser cleaning, immersion wet cleaning, and absorption wet cleaning were applied to the excavated gold brocade. The degree of cleaning and damage were examined depending on the cleaning methods, changes to the physical condition (before and after cleaning) were also analyzed through the surface observation. Although immersion cleaning showed the best cleaning result, this method had a risk of damage to the gold thread. Absorption wet cleaning safely eliminated the various soluble contaminants and the rotten smell of relics. Kneaded rubber eraser was suitable for the excavated gold brocade fabric because it can be applied to selective parts, intentionally excluding some sensitive parts such as the gold thread. The vacuum cleaning method required special attention because of a possibility of suctioning off loosely attached gold leaf. Dual cleaning, the kneaded rubber eraser cleaning, followed by the absorption cleaning was the most effective method to preserve and clean excavated gold brocade.

A Case Study of Vacuum Consolidation Method on Reclaimed Ground (준설매립지반에서의 진공압밀공법 적용사례)

  • Yang, Kee-Sok;Ahn, Chang-Yol;Son, Su-Won;Kang, Myeong-Chan;Kim, Byeong-Gyu;Lee, Song
    • 기술발표회
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    • s.2006
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    • pp.248-260
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    • 2006
  • 광양항 3단계 1차 컨테이너터미널 부지 연약지반개량의 경우 광양지역의 특성상 재하용 토사확보 곤란, 시공기간 단축 및 환경훼손 최소화를 위해 진공압밀공법이 적용되었다. 본 사례연구에서는 진공압밀공법의 시공에 따른 문제점 및 개선사항을 제시하였고, 현장계측 및 진공 압밀완료 후에 실시된 지반조사 결과 등을 분석하여 준설매립지반에서의 진공압밀공법의 적용성을 평가하였다.

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Experinces with Soft Clay Improvement in the Bangkok plain

  • O, P-R
    • Proceedings of the Korean Geotechical Society Conference
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    • 1997.06c
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    • pp.1.1-16
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    • 1997
  • This lecture summarizes the progress of the development of the different ground improvement techniques in Bangkok Plain and is reviewed in relation to the extensive deep wen pumping and the resulting piezometric drawdown at deeper depths. Case records of test embankments with sand drains, sand wicks and PVD are presented to inustrate the effectiveness of different types of vertical drains with surcharge. The use of prefsbicated drain seems more superior than the other types of sand drain. Construction of test embaxlkment, criteria for PVD selection and relevant laboratory testing techniques are discussed for formulating the specif'ication. Alternative teckuuque, such in, the use of deep chemical mixing is reviewed in terms of the efficiency of cement, lime and flyash as additive. Vacuum pre-loading with surcharge and elctro- osmotic consolidation are also explored as possible tectmiques to improve the engineering properties of soft Bangkok clay.

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Development of Al-SiC Metal Matrix Composites by using Hot Press Forming Technologies (열간가압성형기술을 이용한 Ai-SiC 금속기 복합재료 개발)

  • Jeon, Ho-Jin;Kim, Tae-Won
    • Composites Research
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    • v.20 no.4
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    • pp.9-17
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    • 2007
  • Powder metallurgy has been employed for the development of SiC particle reinforced aluminum metal matrix composites by means of hot isotropic pressing and vacuum hot pressing. A material model based on micro-mechanical approach then has been presented for the processes. Densification occurs by the inelastic flow of matrix materials during the consolidation, and consequently it depends on many process conditions such as applied pressure, temperature and volume fraction of reinforcement. The model is implemented into finite element software so that the process simulation can be performed enabling the predicted relative density to be compared with experimental data. In order to determine the performance of finished products, further tensile test has been conducted using the developed specimens. The effect of internal void of the materials on mechanical properties therefore can be investigated.

Consolidation Characteristics of Soft Ground in Suction Drain Method (석션드레인공법이 적용된 연약지반의 압밀특성에 관한 사례 분석)

  • Kim, Byung Il;Kim, Do Hyung;Kim, Soo Sam;Han, Sang Jae
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.29 no.6C
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    • pp.287-294
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    • 2009
  • Suction Drain Method is a relatively new technique to improve soft ground using vacuum pressure which can be directly applied to the soft ground through drains that the pore water pressure around them are decreased without changing total stress. This can accelerate volume changes and increase strength of the ground. This paper shows the results of field test of the suction drain method applied at dredged and reclaimed clay. To evaluate the improvement effects of soft ground by the suction drain method, this paper analyzed real-time field measurements to the results of the laboratory tests and numerical analysis. The comparisons of the settlement and shear strength between suction drain method and surcharge preloading method show possibilities for replacement of the preloading methods. The settlements by suction drain method were 2.3 times larger and undrained shear strength were 300%~400% higher than surcharge method. Moreover, the water content is decreased about 30% and the preconsolidation pressure is increased about $0.52kgf/cm^2$.