• Title/Summary/Keyword: Uniformity of temperature

Search Result 669, Processing Time 0.034 seconds

Gas sensing properties of CuO nanowalls synthesized via oxidation of Cu foil in aqueous NH4OH (NH4OH 수용액 하에서 Cu 호일의 산화를 통해 합성한 CuO 나노벽의 가스센싱 특성)

  • ;;;Lee, Si-Hong;Lee, Sang-Uk;Lee, Jun-Hyeong;Kim, Jeong-Ju;Heo, Yeong-U
    • Proceedings of the Korean Institute of Surface Engineering Conference
    • /
    • 2018.06a
    • /
    • pp.141-141
    • /
    • 2018
  • Copper is one of the most abundant metals on earth. Its oxide (CuO) is an intrinsically p-type metal-oxide semiconductor with a bandgap ($E_g$) of 1.2-2.0 eV 1. Copper oxide nanomaterials are considered as promising materials for a wide range of applications e.g., lithium ion batteries, dye-sensitized solar cells, photocatalytic hydrogen production, photodetectors, and biogas sensors 2-7. Recently, high-density and uniform CuO nanostructures have been grown on Cu foils in alkaline solutions 3. In 2011, T. Soejima et al. proposed a facile process for the oxidation synthesis of CuO nanobelt arrays using $NH_3-H_2O_2$ aqueous solution 8. In 2017, G. Kaur et al. synthesized CuO nanostructures by treating Cu foils in $NH_4OH$ at room temperature for different treatment times 9. The surface treatment of Cu in alkaline aqueous solutions is a potential method for the mass fabrication of CuO nanostructures with high uniformity and density. It is interesting to compare the gas sensing properties among CuO nanomaterials synthesized by this approach and by others. Nevertheless, none of above studies investigated the gas sensing properties of as-synthesized CuO nanomaterials. In this study, CuO nanowalls versus nanoparticles were synthesized via the oxidation process of Cu foil in NH4OH solution at $50-70^{\circ}C$. The gas sensing properties of the as-prepared CuO nanoplates were examined with $C_2H_5OH$, $CH_3COCH_3$, and $NH_3$ at $200-360^{\circ}C$.

  • PDF

Fine Dispensing Process of High Viscosity Phosphor for Repairing Application of White LED (백색 LED 보정 공정 적용을 위한 고점도 형광체 미세 정량토출 공정)

  • Yang, Bong Su;Yang, Young Jin;Kim, Hyung Chan;Ko, Jeong Beom;Cho, Kyung Ho;Doh, Yang Hoi
    • Journal of the Korean Society of Manufacturing Technology Engineers
    • /
    • v.25 no.2
    • /
    • pp.124-131
    • /
    • 2016
  • Several research works for finding and optimizing the methods of dispensing high viscosity phosphor used in the fabrication of white LED's are currently in progress. High viscosity phosphor dispensing with a high accuracy is crucial because the dispensing rate and uniformity directly affect parameters such as the CIE chromaticity diagram, color temperature and luminous flux of white LED's. This study presents a novel method of dispensing high viscosity phosphor using electrohydrodynamic printing. The dispensing rate was optimized less than 0.01 mg phosphor using experiments and optimizing the process parameters including the standoff distance from the nozzle to the substrate, ink supply pressure, and multi-step pulsed waveform magnitude ratio. The dispensing rate was measured by dispensing 20 dots using drop-on-demand with the optimized parameters, and the experiments were repeated 10 times to maximize the data accuracy. The average dispensing rate that can be reliably used for high viscosity phosphor dispensing was 0.0052 mg.

Study on Ni-Cr Electro Plating Process for Staged Combustion Cycle Engine (다단연소사이클 엔진 적용을 위한 Ni-Cr 코팅에 관한 연구)

  • Bae, Byung-Hyun;Hwang, Yang-Jin;Lee, Kyu-Hwan;Rhee, Byong-ho;Han, Yeoung-Min;Kim, Young-June;Noh, Yong-Oh;Cho, Hwang-Rae;Hyun, Seong-Yoon;Bang, Jeong-Suk
    • Proceedings of the Korean Society of Propulsion Engineers Conference
    • /
    • 2017.05a
    • /
    • pp.857-863
    • /
    • 2017
  • In this paper, the process of electro Ni and electro Cr plating is studied for the purpose of thermal barrier to protect the inner wall combustion chamber. The chamber is under the environment of very high temperature and high pressure when propellants burn in there. As one of the thermal barrier coatings, Zr-based thermal spray coating has been applied to the chamber. However, peeling of coating layer can occur under such a hard condition because of the difference of thermal expansion coefficients between the ceramic and the metallic wall. We study the characteristics of Ni-Cr coating and establish its process. It is found that the thickness of over $100{\mu}m$ of Ni and Cr coating layers with the uniformity of ${\pm}10%$ can be obtained with the used of as-developed plating bath.

  • PDF

Gibberellic Acid and Cold Stratification Promotes Seed Germination and Seedling Growth in Kadsura coccinea (GA3처리와 저온습윤처리에 의한 흑노호(Kadsura coccinea)의 종자발아 및 유묘생장 촉진)

  • Byoung Il Je;Joonng Suk Jeon;Jum-Soon Kang;Young Whan choi
    • Journal of Environmental Science International
    • /
    • v.32 no.1
    • /
    • pp.77-88
    • /
    • 2023
  • Kadsura coccinea (Lem.) A.C. Smith is used as a medicinal plant and cosmetic material in China and Southeast Asia. To mass-produce Kadsura coccinea seedlings, the effects of gibberellic acid (GA3) and cold stratification treatments on seed germination were investigated. Seed germination rate with GA3 treatment was most effective at concentrations of 250 or 500 mg/L. With respect to mean germination time (MGT), mean daily germination, and T50 (days to reach 50% seed germination), the germination-promoting effect was improved as the concentration of GA3 increased. Stem growth of seedlings was the highest following GA3 treatments of 250 and 500 mg/L, and the growth promoting effect gradually decreased as the concentration of GA3 decreased. Root growth was stimulated at GA3 concentrations of 250-1,000 mg/L. Examination of the effect of stratification treatment for 15, 30 and 60 days at temperatures of 0, 5 and 10℃ on the germination rate revealed that the most stratification treatment temperature was 10℃, and the results improved with longer treatment periods. Altogether, GA3 and stratification treatments improved the seed germination rate, shortened the MGT, improved germination uniformity, and produced healthy seedlings.

Validation of a Rodent Nose-only Exposure System for Inhalation Toxicity Evaluation of Cigarette Smoke (담배 흡입독성 평가를 위한 설치류 담배연기노출시스템의 유효화)

  • Sohn, Hyung-Ok;Lee, Hyeong-Seok;Shin, Han-Jae;Park, Chul-Hoon;Yoo, Ji-Hye;Jang, Mi;Hyun, Hak-Chul
    • Journal of the Korean Society of Tobacco Science
    • /
    • v.36 no.1
    • /
    • pp.20-25
    • /
    • 2014
  • As part of a balanced testing battery, subchronic inhalation studies on rats are performed to ensure that proposed cigarette modifications do not increase the toxicity of smoke and to demonstrate any instances where a modification may actually contribute to harm reduction. For subchronic inhalation studies with aerosols, the OECD suggests an exposure regimen of 6 hours/day (OECD Guideline 413, 1981), but alternative regimens have also been published: 1 hour/day and $2{\times}1$ hour/day. The aim of this study was to validate a rodent nose-only exposure system for the assessment of inhalation toxicity of cigarette smoke. In this study, cigarette smoke exposure system is consisted of cigarette smoke generator, smoke concentration adjusting system, and 20-port nose-only exposure system. Male SD rats were exposed for 35 days ($2{\times}1$ hour/day) to 3R4F Reference cigarette smoke and analysed major monitoring items of OECD Gudeline 413. WTPM, was measured in the test atmosphere, respiratory function (Buxco Biosystems) during exposure, postexposure urinary exposure biomarkers and alveolar neutrophiles in BAL fluid (Day 35) were evaluated. Validation demonstrated steady WTPM ($257{\pm}20ug/L$, $502{\pm}27ug/L$) and spatial uniformity (<10%). Nose port temperature ($22{\sim}26^{\circ}C$ and RH (45~75%) were acceptable over 35 days. Reductions in respiratory rate and minute volume and increase in the neutrophiles in BALF and the urinary exposure biomarkers were observed cigarette smoke dose dependently. This validation and 35-day inhalation study has shown that the rodent nose-only exposure system may be useful in the inhalation toxicity assessment of cigarette smoke.

Red-emitting α-SrO·3B2O3:Sm2+ Phosphor for WLED Lamps: Novel Lighting Properties with Two-layer Remote Phosphor Package

  • Tin, Phu Tran;Nguyen, Nhan K.H.;Tran, Minh Q.H.;Lee, Hsiao-Yi
    • Current Optics and Photonics
    • /
    • v.1 no.4
    • /
    • pp.389-395
    • /
    • 2017
  • This paper investigates a method to improve the lighting performance of white light-emitting diodes (WLEDs), which are packaged using two separate remote phosphor layers, a yellow-emitting YAG:Ce phosphor layer and a red-emitting ${\alpha}-SrO{\cdot}3B_2O_3:Sm^{2+}$ phosphor layer. The thicknesses of these two layers are $800{\mu}m$ and $200{\mu}m$, respectively. Both of them are examined in conditions where the average correlated color temperatures (CCT) are 7700 K and 8500 K. For this two-layer model, the concentration of red phosphor is varied from 2% to 30% in the upper layer, while in the lower layer the yellow phosphor concentration is kept at 15%. It was found interestingly that the lighting properties such as color rendering index (CRI) and luminous flux are enhanced significantly, while the color uniformity is maintained in a relatively close range to the one of one-layer configuration (measured at the same correlated color temperature). Besides, the transmitted and reflected light of each phosphor layer are revised by combining Kubelka-Munk and Mie-Lorenz theories. Through analysis, it is demonstrated that the packaging configuration of two-layer remote phosphor that employs red-emitting ${\alpha}-SrO{\cdot}3B_2O_3:Sm^{2+}$ phosphor particles provides a practical solution for general WLEDs lighting.

Study on the OLED Thin Film Encapsulation of the Al2O3 Thin Layer Formed by Atomic Layer Deposition Method (원자층 증착방법에 의한 Al2O3 박막의 OLED Thin Film Encapsulation에 관한 연구)

  • Kim, Ki Rak;Cho, Eou Sik;Kwon, Sang Jik
    • Journal of the Semiconductor & Display Technology
    • /
    • v.21 no.1
    • /
    • pp.67-70
    • /
    • 2022
  • In order to prevent water vapor and oxygen permeation in the organic light emitting diodes (OLED), Al2O3 thin-film encapsulation (TFE) technology were investigated. Atomic layer deposition (ALD) method was used for making the Al2O3 TFE layer because it has superior barrier performance with advantages of excellent uniformity over large scales at relatively low deposition temperatures. In this study, the thickness of the Al2O3 layer was varied by controlling the numbers of the unit pulse cycle including Tri Methyl Aluminum(Al(CH3)3) injection, Ar purge, and H2O injection. In this case, several process parameters such as injection pulse times, Ar flow rate, precursor temperature, and substrate temperatures were fixed for analysis of the effect only on the thickness of the Al2O3 layer. As results, at least the thickness of 39 nm was required in order to obtain the minimum WVTR of 9.04 mg/m2day per one Al2O3 layer and a good transmittance of 90.94 % at 550 nm wavelength.

Self-Assembled InAs/AlAs Quantum Dots Characterization Using Photoreflectance Spectroscopy (자연 성장된 InAs/AlAs 양자점의 Photoreflectance 특성)

  • Kim, Ki-Hong;Sim, Jun-Hyoung;Bae, In-Ho
    • Journal of the Korean Vacuum Society
    • /
    • v.18 no.3
    • /
    • pp.208-212
    • /
    • 2009
  • The optical characterization of self-assembled InAs/AlAs quantum dots(QD) grown by MBE were investigated using photoreflectance spectroscopy. The intensities of the signals of the GaAs buffer and wetting layer(WL) changed with the width of the WL layer. The PR spectrum for the sample, in which QDs layer were etched off at room temperature, indicated that the broadened signal ranging $1.1{\sim}1.4\;eV$ was originated from InAs QDs and WL. The intensities of signals of GaAs buffer and the WL changed with the WL width. A red shift of the PR peak of WL are observed when the annealing temperatures range from $450^{\circ}C$ to $750^{\circ}C$, which indicates that the interdiffusion between dots and capping layer is caused by improvement in size uniformity of QDs.

SCR facility design for the selective catalyst performance of mixed gas

  • Woohyeon, Hwang;Kyung-Ok, Lee
    • Journal of the Korea Society of Computer and Information
    • /
    • v.28 no.1
    • /
    • pp.121-127
    • /
    • 2023
  • In this study, the design conditions and CFD analysis results are compared and reviewed in SCR that can optimally reduce nitrogen compounds. To this end, it was analyzed and compared using CFD to see if the design criteria were satisfied for the shell and tube areas of the boiler. In the SCR system, the analysis area is the gas/air heat exchanger on the shell side, and eight tubes of the gas/air heat exchanger on the tube side. Through CFD analysis, the gas velocity distribution on the primary catalyst side of the SCR system was designed to be 2.4%, and the NH3/NOx molar ratio distribution was 3.7%, which satisfied the design criteria. In addition, the uniformity of the temperature distribution was confirmed and the required condition of 260℃ or higher was satisfied. The angle of the gas entering the catalyst met the design conditions at 2.9 degrees, and the pressure loss that occurred also satisfied the design requirements. Through this CFD analysis, it was confirmed that it was designed and operated by satisfying the design conditions required for each area.

Study on the Soil Compaction (흙의 다짐에 관한 연구(I))

  • 강문묵
    • Magazine of the Korean Society of Agricultural Engineers
    • /
    • v.11 no.4
    • /
    • pp.1783-1790
    • /
    • 1969
  • It is one of the most economical method of soil stabilization works to compact soil, which increases soil density artificially. Compaction effort is to lessen void of soils, and consequently its aim is to enlarge friction and cohesion force, and reduce permeability of soil. Factors in compaction effort are moisture content, grain size, grain size distribution, physical properties, compaction method and temperature of soils etc. The results obtained in this study on the effects that grain size, gradation and physical properties influence upon compaction effort for 20 samples under the constant compaction method, are summarized as follows: 1. The bigger the maximum dry density is, the smaller the optimum moisture content is, on the other hand, the smaller the maximum dry densityis, the bigger the optimum moisture content is, ingeneral. 2. The coarser the grain size is, the bigger the maximum dry density is, and the optimum moisture content becomes small, and dry density-moisture content curve has the sharp peak, generally. Also, the finer the grain size is the smaller the maximum dry density is, and the optimum moisture content shows the big value, and dry density-moisture content curve has the dull peak. 3. The maximum dry density shows the biggest value on the sample to be about 15% of particles finer than No. 200 sieve. The more the percent passing of No. 10 sieve increase, the smaller the maximum dry density is. Soils which have uniformity coefficient less than 5 in particles larger than 0.074mm hardly show dry density-moisture content curve. 4. There is a relation which is ramax=2.3948-0.0376 Wopt between the maximum dry density and the optimum moisture content, namely, the maximum dry density is increased in proportion to decrease of the optimum moisture content. 5. There are relations to be the straight lines which the maximum dry density decrease, on the other hand, the optimum moisture content increase in accordance with enlargement of Atterberg Limit(LL, PL, PL) in compacted soils.

  • PDF