• Title/Summary/Keyword: Ultrasonic Material

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In-vitro and In-vivo Biocompatibility Evaluation of Silica Based Bio-active Glass Prepared by Hydrothermal Method

  • Sarkar, Swapan Kumar;Nguyen, Phuong Thi;Lee, Byong-Taek
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2011.05a
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    • pp.53.1-53.1
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    • 2011
  • Bioactive glass powders were synthesized by hydrothermal chemical route by the use of ultrasonic energy irradiation. We used sodalime, calcium nitrate tetra hydrate and di ammonium hydrogen phosphate as the precursor material to synthesize $SiO_2$ rich bio-active glass materials. The $SiO_2$ content was varied in the precursor mixture to 60, 52 and 45 mole%. Dense compacts were obtained by microwave sintering at $1,100^{\circ}C$. Mechanical properties were characterized for the fabricated dense bioactive glasses and were found to be comparable with conventional CaO-$SiO_2$-$Na_2O$-$P_2O_5$ bioactive glass. Detailed biocompatibility evaluation of the glass composition was investigated by in-vitro culture of MG-63 cell and mesenchyme stem cell. Cell adhesion behavior was investigated for both of the cell by one cell morphology for 30, 60 and 90 minutes. Cell proliferation behavior was investigated by culturing both of the cells for 1, 3 and 7 days and was found to be excellent. Both SEM and confocal laser scanning microscopy were used for the investigation. Western blot analysis was performed to evaluate the bimolecular level interaction and extent and rate of specific protein expression. The ability to form biological apatite in physiological condition was observed with simulated body fluid (SBF). In-vivo bone formation behavior was investigated after implanting the materials inside rabbit femur for 1 and 3 month. The bone formation behavior was excellent in all the bioglass compositions, specially the composition with 60% $SiO_2$ content showed most promising trend.

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Joining Technology of Flat Panel Photobioreactor Case (평판형 광생물반응기 케이스 접합 기술)

  • Ahn, Dong-Gyu;Lee, Ho Jin;Ahn, Yeong-Su
    • Journal of the Korean Society for Precision Engineering
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    • v.30 no.2
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    • pp.154-163
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    • 2013
  • Adhesive bonding and plastic welding have been widely used to join two plastic materials together. The goal of this paper is to determine a proper joining technology of a pair of flat panel (FP) photobioreactor (PBR) case. The material of the FP PBR case is polycarbonate (PC) plate. Two types of adhesion, including acryl adhesive and two-part epoxy adhesive, as well as two types of plastic welding technology, including ultrasonic welding and thermal welding, are employed for joining of PC plates. In order to influence of the adhesion and welding conditions on the joining characteristics of the PC plates in operational conditions of the FP PBR case, the morphology in the vicinity of the joined region as well as the water and pressure resistance characteristic are investigated. In addition, the variation of the bonding strength of the joined region and deformation behaviors in the vicinity of the joined region according to the adhesion and welding conditions is examined via the lap-shear test. From the results of basic experiments, proper joining technologies are chosen. Using the chosen joining technologies, the FP PBR case are fabricated to perform full-scale durability experiment. The results of the full-scale durability experiment have been shown that the chosen joining technologies can be applicable to fabricate the FP PBR case.

Measurement of Elastic Constants of Thin Metallic Foil by Guided Wave Dispersion Characteristics (유도초음파 분산 특성을 이용한 박판의 탄성계수 측정)

  • Lee, Dong-Jin;Cho, Youn-Ho;Jang, Kang-Won;Cho, Seung-Hyun;Ahn, Bong-Young
    • Journal of the Korean Society for Nondestructive Testing
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    • v.32 no.1
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    • pp.41-46
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    • 2012
  • As the development of MEMS/NEMS structure and application technology the demand for an assessment of the mechanical properties have increased. The mechanical properties are mainly evaluated by using tensile test or ultrasonic wave measurement. However, the new technology have been developed such as nano-indentation, guided wave method because they have a limitation in case of a thin plate and thin film. In the study, the guided wave velocities are measured by electromagnetic-acoustic transducer(EMAT), the material properties of thin metallic foils are obtained using optimization process of the theoretical and experimental group velocity of guided wave. The Young's modulus obtained by the optimization process(201.6 GPa), nano-indentation(207.0 GPa) and literature value(203.7 GPa) of a $50{\mu}m$ thick nickel thin plate shows good agreement within 3%.

Determination of Impact Source Location Using a Single Transducer and Time Reversal Technique (단일센서와 시간역전법을 이용한 판에서의 충격위치 결정에 관한 연구)

  • Jeong, Hyun-Jo;Cho, Sung-Jong
    • Journal of the Korean Society for Nondestructive Testing
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    • v.32 no.1
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    • pp.47-55
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    • 2012
  • A structural health monitoring technique for locating impact position in a plate structure is presented in this paper. The method employs a single sensor and spatial focusing of time reversal (TR) acoustics. We first examine the TR focusing effect at the impact position and its surroundings through simulation and experiment. The imaging results of impact points show that the impact source location can be accurately estimated in any position of the plate. Compared to existing techniques for locating impact or acoustic emission source, the proposed method has the benefits of using a single sensor and not requiring material properties and geometry of structures. Furthermore, it does not depend on a particular mode of dispersive Lamb waves that is frequently used in other ultrasonic testings of plate-like structures.

Microstructural Characterization for Structural Health Monitoring of Heat-Resisting Rotor Steels (로터용 내열강의 구조 건전성 모니터링을 위한 미세 조직 평가)

  • Kim, C.S.;Byeon, Jae-Won;Park, Ik-Keun
    • Journal of the Korean Society for Nondestructive Testing
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    • v.28 no.2
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    • pp.177-183
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    • 2008
  • The typical heat-resisting rotor steels such as 2.25CrMo, 9CrMo and 12CrW steel were experimentally studied in order to understand their materials degradation under high temperature and pressure during the long-term service, and then use the basic studies for the structural health monitoring. In order to monitor the materials degradation, it was conducted by the isothermal aging for 2.25CrMo steel, creep-fatigue for 9CrMo steel and creep for 12Cr steel with the incremental step test. The ultrasonic wave properties, electrical resistivity and coercivity were interpreted in relation to microstructural changes at each material and showed strong sensitivity to the specific microstructural evolution.

A study on mechanical properties of concrete including activated recycled plastic waste

  • Ashok, M.;Jayabalan, P.;Saraswathy, V.;Muralidharan, S.
    • Advances in concrete construction
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    • v.9 no.2
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    • pp.207-215
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    • 2020
  • This paper describes the experimental studies carried out to determine the properties of fresh and hardened concrete with Recycled Plastic Waste (RPW) as a partial replacement material for fine aggregates. In the experimental study, RPW was used for replacing river sand and manufactured sand (M sand) aggregates in concrete. The replacement level of fine aggregates was ranging from 5% to 20% by volume with an increment of 5%. M40 grade of concrete with water cement ratio of 0.40 was used in this study. Two different types of RPW were used, and they are (i) un-activated RPW and (ii) activated RPW. The activated RPW was obtained by alkali activation of un-activated RPW using NaOH solution. The hardened properties of the concrete determined were dry density, compressive strength, split tensile strength, flexural strength and ultrasonic pulse velocity (UPV). The properties of the concrete with river sand, M sand, activated RPW and un-activated RPW were compared and inferences were drawn. The effect of activation using NaOH solution was investigated using FT-IR study. The micro structural examination of hardened concrete was carried out using Scanning Electron Microscopy (SEM). The test results show that the strength of concrete with activated RPW was more than that of un-activated RPW. From the results, it is evident that it is feasible to use 5% un-activated RPW and 15% activated RPW as fine aggregates for making concrete without affecting the strength properties.

Detection of Micro-Crack Using a Nonlinear Ultrasonic Resonance Parameters (비선형 초음파공명 특성을 이용한 미세균열 탐지)

  • Cheong, Yong-Moo;Lee, Deok-Hyun
    • Journal of the Korean Society for Nondestructive Testing
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    • v.32 no.4
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    • pp.369-375
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    • 2012
  • In order to overcome the detection limit by the current nondestructive evaluation technology, a nonlinear resonant ultrasound spectroscopy(NRUS) technique was applied for detection of micro-scale cracks in a material. A down-shift of the resonance frequency and a variation of normalized amplitude of the resonance pattern were suggested as the nonlinear parameter for detection of micro-scale cracks in a materials. A natural-like crack were produced in a standard compact tension(CT) specimen by a low cycle fatigue test and the resonance patterns were acquired in each fatigue step. As the exciting voltage increases, a down-shift of resonance frequency were increases as well as the normalized amplitude decrease. This nonlinear effects were significant and even greater in the cracked specimen, but not observed in a intact specimen.

Scanning Acoustic Microsope System Using 200MHZ ZnO Transducer (ZnO를 이용한 초음파 현미경의 제작과 평가)

  • Jang, Ji-Won;Do, Si-Hong;Lee, Jong-Gyu
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.25 no.4
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    • pp.200-208
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    • 1989
  • To the purpose of preparation for investigating aspect of material that not revealed by the light microscope and extending our knowledge in applicable field, a scanning acoustic microscope system of 200MHz was organized and appraised its performance with experiments. Professor N.CHUBACHI in Tohoku University in Sendai, Japan provided the ZnO transducer with lens. The system for transmitting and receiving ultrasonic pulses of 200nsec was organized with a rectangular audio wave generator for modulation of 200MHz carrier wave, gating system for transmitting and receiving, mixer for converting intermediate frequency, a directional coupler, ZnO transducer, radio frequency amplifiers. detecter and personal computer. The Scanning system was driven in micro steps with three stepping motors in the direction of x, y and z axes. The system was a reflecting type scanning acoustic microscope and the operation program processed graphics data from receiving echo intensities. Photograph of fish scale obtained by optical microscope was compared with its image by the scanning acoustic microscope organized here. The result was satisfiable.

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The Effect of Fiber Stacking Angle on the Relationship Between Fatigue Crack and Delamination Behavior in a Hybrid Composite Materials (하이브리드 복합재료의 섬유배향각이 피로균열 및 층간분리 거동의 관계에 미치는 영향)

  • Song, Sam-Hong;Kim, Cheol-Woong
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.28 no.3
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    • pp.281-288
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    • 2004
  • The hybrid composite material (Al/GFRP laminates) are applied to the fuselage and wing in a aircraft. Therefore, Al/GFRP laminates suffer from the cyclic bending moments. This study was to evaluate the effect of fiber stacking angle on the fatigue crack propagation and delamination behavior using the relationship between crack growth rate (da/dN) and stress intensity factor range (ΔK) in Al/GFRP laminates under cyclic bending moment. The variable delamination growth behavior in case of three different type of fiber orientations, i.e., [Al/O$_2$/Al], [Al/+45$_2$/Al] and [Al/90$_2$/Al] at the interface of Al layer and glass fiber layer was measured by ultrasonic C-scan images. As results of this study, It represent that the delamination shape should turns out to have more effective characteristics on the fiber stacking angle. The extension of the delamination zone in case of [Al/+45$_2$/Al] and [Al/90$_2$/Al] were not formed along the fatigue crack profile. The shape of delamination zone depend on fiber stacking angle and the variable type with the delamination contour decreased non-linearly toward the crack tip at the Al layer.

Consolidation Efficiency of In-situ Application Considering Weathering Grade and Rock Properties for Stone Cultural Heritage in Yeongyang Area, Gyeongsangbuk-do (경북 영양일대 석조문화재의 구성암석과 풍화도를 고려한 표면강화제의 현장적용 효과)

  • Lee, Myeong-Seong;Kim, Jae-Hwan;Lee, Jae-Man;Lee, Jang-Jon
    • Journal of Conservation Science
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    • v.27 no.3
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    • pp.277-290
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    • 2011
  • The aim of this study is to examine the efficiency of ethylsilicate consolidants on sandstone according to its weathering state for an appropriate application to stone cultural heritage in Yeongyang area. Yeongyang area had sandstone and conglomeratic sandstone cultural heritages which needed conservation intervention due to granular disintegration and scaling on their surface. Hyeonri Three-storied Pagoda having typical stone materials in this area was investigated for the analyses of the material and deterioration. And both in-situ and laboratory applications of consolidants were conducted to the outcrop which had the same characteristics of rock type and weathering grade. As a result of the application, it was concluded that Wacker OH 100 and Remmers 300 showed the most appropriate consolidating effect, and Remmers 300 was the most effective to strengthen the loosen and granular-disintegrated surface of the sandstone.