• Title/Summary/Keyword: Ultrasonic Extraction

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Immediate Autogenous Fresh Demineralized Tooth (Auto-FDT) Graft for Alveolar Bone Reconstruction (즉시 탈회 치아이식재를 사용한 치조골 재건술)

  • Lee, Eun-Young
    • The Journal of the Korean dental association
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    • v.54 no.5
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    • pp.348-355
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    • 2016
  • Ideal autogenous or allogenic bone graft materials should provide 1) stabilization of blood clot, 2) scaffolds for cellular proliferation and differentiation, 3) release of osteogenic growth factors, 4) appropriate resorption profile for remodeling of new bone. Teeth, especially dentin, mostly contain hydroxyapatite and type I collagen which are similar to bone, and could be valuable graft material. Clinically teeth are used as calcined or demineralized forms. Demineralized form of dentin can be more effective as a graft material. But a conventional decalcification method takes time and long treatment time may give negative effects to various osteogenic proteins in dentin. Author used a new clinical method to prepare autogenous teeth, which could be grafted into the removal defects immediately after extraction using vacuum ultrasonic system. The process could be finished within two hours regardless of the form (powder, chip or block). Teeth were processed to graft materials in block, chip, or powder types immediately after extraction. It took 120 minutes to prepare block types and 40 minutes to prepare powder. Clinical cases did not show any adverse response and the healing was favorable. Rapid preparation of autogenous teeth with the vacuum ultrasonic system could make the immediate one-day extraction and graft possible.

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Optimization of Polyphenol Extraction Process from Native Soybean using Ultrasound (자생 희귀콩인 납떼기콩으로부터 초음파를 이용한 폴리페놀 성분의 추출 공정 최적화)

  • Kang, Hye Jung;Park, Junseong
    • Journal of the Society of Cosmetic Scientists of Korea
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    • v.48 no.3
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    • pp.255-264
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    • 2022
  • The active ingredients of Napttegi Kong(GML, Glycine max landrace), a type of native rare soybeans, were identified, and an ultrasonic extraction method was introduced as an eco-friendly extraction method. Through the component analysis of the Napttegi Kong extract, the epicatechin, which was not found in conventional soybeans, was identified. For effective extraction using ultrasonic, the main extraction conditions were optimized using the response surface analysis method. Through the Box-Behnken design process, 15 experiments were conducted with the extraction temperature, the ratio of extraction solvent/solution, and extraction time as key independent variables. A quadratic regression equation for the two dependent variables, epicatechin content and total isoflavone content, was derived, and the coefficients of determination were found to be high as R2 = 0.9939 and R2 = 0.9844, respectively, confirming that the correlation showed high significance. The extraction conditions satisfying the maximum expectations of these two dependent variables were predicted. to be 40.4℃ of extraction temperature, 19.3 times of extraction solvent/solution, and 91 sec of extraction time. The expected value and the actual experimental value of the epikatechin content and the total isoflavone content were similar, so it was confirmed that this experimental method is a highly reliable optimization model.

Antioxidant, Black Hair, and Hair Growth Effect of Mixed Extracts of Nardostachys jatamansi, Ocimum basilicum and Crocus sativus

  • Mi Jeong Choi;Yu Ri Kim
    • Microbiology and Biotechnology Letters
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    • v.51 no.1
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    • pp.43-52
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    • 2023
  • The purpose of this study is to confirm the antioxidant, black hair, and hair growth effects of the N. jatamansi, O. basilicum, and C. sativus mixed extracts that pharmacological efficacy has been verified. Accordingly, four samples (NOC-1 to-4) produced under different extraction conditions were prepared and the results are as follows. First, all samples showed an increase in antioxidant content in a concentration-dependent manner from the results of antioxidant efficacy. In particular, NOC-4 extracted by steaming and ultrasonic methods showed the highest antioxidant effect among the four samples. As a result of analysis of the amount of melanin production in mouse melanoma cells, NOC-4 with concentration of 500 ㎍/ml showed higher melanin production compared to the control group, so the black hair efficacy was the best. Also, in the hair growth test results, it was found that the hair growth was the best at 0.94 ± 0.10 mm at experimental group orally administered with 500 mg/kg of NOC-4. In addition, as a result of cytotoxicity analysis in mouse melanoma cells, the safety of samples was demonstrated by maintaining cell viability of 95% or more at all concentrations. These results suggest that the steaming and ultrasonic extraction method increased the extraction yield of active ingredients for antioxidant, melanin, and hair generation, thereby affecting physiological activity. Based on these results, if the steaming and ultrasonic extraction methods are applied to the mixed extraction of N. jatamansi, O. basilicum, and C. sativus, it is judged that the practical potential as a natural material for black hair and hair growth agents will increase.

Construction of Attractor System by Integrity Evaluation of Polyethylene Piping Materials (폴리에틸렌 배관재의 건전성 평가를 위한 어트랙터 시스템의 구축)

  • Taik, Hwang-Yeong;Kyu, Oh-Seung;Won, Yi
    • Proceedings of the KSME Conference
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    • 2001.06a
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    • pp.609-615
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    • 2001
  • This study proposes analysis and evaluation method of time series ultrasonic signal using attractor analysis for fusion joint part of polyethylene piping. Quantitatively characteristics of fusion joint part is analysed features extracted from time series. Trajectory changes in the attractor indicated a substantial difference in fractal characteristics. These differences in characteristics of fusion joint part enables the evaluation of unique characteristics of fusion joint part. In quantitative fractal feature extraction, feature values of 4.291 in the case of debonding and 3.694 in the case of bonding were proposed on the basis of fractal dimensions. In quantitative quadrant feature extraction, 1,306 point in the case of bonding(one quadrant) and 1,209 point(one quadrant) in the case of debonding were proposed on the basis of fractal dimensions. Proposed attractor feature extraction can be used for integrity evaluation of polyethylene piping material which is in case of bonding or debonding.

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A Comparison of Sonication and Microwave-assisted Extraction Method for Speciation of Arsenic in Fish Tissue, DORM-2 (어류중 비소의 종분화 분석을 위한 초음파 추출법과 마이크로파 추출법의 비교)

  • Yoon, Cheol-Ho;Park, Yong-Chul;Hong, Jong-Ki
    • Analytical Science and Technology
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    • v.16 no.2
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    • pp.134-142
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    • 2003
  • Comparison of a microwave-assisted extraction with sonication extraction was performed for arsenic speciation in fish tissue with chromatographic separation and inductively coupled plasma mass spectrometry detection. The detection limits of arsenicals with ultrasonic nebulizerand cross-flow nebulizer were shown to be similar. The arsenicals investigated were arsenobetaine (AsB), arsenite [As(III)], dimethylarsine acid (DMA), monomethylarsonic acid (MMA), arsenate [As(v)], and phenylarsonic acid (PAA). Quantitative extraction of arsenicals from dogfish muscle, DORM-2, standard reference material of NRCC (National Research Council of Canada) was achieved using 50% (v/v) methanol-water in both extraction methods. Extraction efficiency of arsenobetaine in both methods is greater than 82% with RSDs on replicates of less than 5%. The concentrations of AsB determined in extract of microwave assisted extraction and sonication methods were $14.18{\pm}0.42mg\;kg^{-1}$ and $13.54 {\pm}0.84mg\;kg^{-1}$, respectively. And the concentrations of DMA were $0.45{\pm}0.06mg\;kg^{-1}$ and $0.44{\pm}0.06mg\;kg^{-1}$, respectively.

Ultrasound-Assisted Liquid-Liquid Extraction for Recovery of Paclitaxel from Plant Cell Cultures (식물세포배양으로부터 파클리탁셀 회수를 위한 초음파를 이용한 액-액 추출)

  • Ha, Geon-Soo;Kim, Jin-Hyun
    • Korean Chemical Engineering Research
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    • v.54 no.2
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    • pp.229-233
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    • 2016
  • In this study, an efficient ultrasound-assisted liquid-liquid extraction process was developed for recovering of paclitaxel from plant cell cultures. The optimal ultrasonic power and operating time were 250 W and 15 min at fixed ratio of bottom phase, methylene chloride to top phase, MeOH (25%, v/v). Under the optimal conditions developed in the present method, most of the paclitaxel (~92%) was recovered from crude extract by a single extraction step. Due to the synergistic effect of ultrasound by the addition of inorganic salt, an appropriate inorganic salt concentration and the ultrasonic power were found to be required for the effective recovery of paclitaxel using ultrasound-assisted liquid-liquid extraction.

Chaotic Evaluation of Slag Inclusion Welding Defect Time Series Signals Considering the Hyperspace (초공간을 고려한 슬래그 혼입 용접 결함 시계열 신호의 카오스성 평가)

  • Yi, Won;Yun, In-Sik
    • Journal of the Korean Society for Precision Engineering
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    • v.15 no.12
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    • pp.226-235
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    • 1998
  • This study proposes the analysis and evaluation of method of time series of ultrasonic signal using the chaotic feature extraction for ultrasonic pattern recognition. The features are extracted from time series data for analysis of weld defects quantitatively. For this purpose, analysis objectives in this study are fractal dimension, Lyapunov exponent, and strange attractor on hyperspace. The Lyapunov exponent is a measure of rate in which phase space diverges nearby trajectories. Chaotic trajectories have at least one positive Lyapunov exponent, and the fractal dimension appears as a metric space such as the phase space trajectory of a dynamical system. In experiment, fractal(correlation) dimensions and Lyapunov exponents show the mean value of 4.663, and 0.093 relatively in case of learning, while the mean value of 4.926, and 0.090 in case of testing in slag inclusion(weld defects) are shown. Therefore, the proposed chaotic feature extraction can be enhancement of precision rate for ultrasonic pattern recognition in defecting signals of weld zone, such as slag inclusion.

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Wavelet-based feature extraction for automatic defect classification in strands by ultrasonic structural monitoring

  • Rizzo, Piervincenzo;Lanza di Scalea, Francesco
    • Smart Structures and Systems
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    • v.2 no.3
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    • pp.253-274
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    • 2006
  • The structural monitoring of multi-wire strands is of importance to prestressed concrete structures and cable-stayed or suspension bridges. This paper addresses the monitoring of strands by ultrasonic guided waves with emphasis on the signal processing and automatic defect classification. The detection of notch-like defects in the strands is based on the reflections of guided waves that are excited and detected by magnetostrictive ultrasonic transducers. The Discrete Wavelet Transform was used to extract damage-sensitive features from the detected signals and to construct a multi-dimensional Damage Index vector. The Damage Index vector was then fed to an Artificial Neural Network to provide the automatic classification of (a) the size of the notch and (b) the location of the notch from the receiving sensor. Following an optimization study of the network, it was determined that five damage-sensitive features provided the best defect classification performance with an overall success rate of 90.8%. It was thus demonstrated that the wavelet-based multidimensional analysis can provide excellent classification performance for notch-type defects in strands.

Construction of Chaoral Post-Process System for Integrity Evaluation of Weld Zone (용접부 건전성 평가를 위한 카오럴 후처리 시스템의 구축)

  • Lee, Won;Yoon, In-Sik
    • Journal of the Korean Society for Precision Engineering
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    • v.15 no.11
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    • pp.152-165
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    • 1998
  • This study proposes the analysis and evaluation method of time series ultrasonic signal using the chaoral post-process system for precision rate enhancement of ultrasonic pattern recognition. Chaos features extracted from time series data for analysis quantitatively weld defects For this purpose, feature extraction objectives in this study are fractal dimension, Lyapunov exponent, shape of strange attrator. Trajectory changes in the strange attractor indicated that even same type of defects carried substantial difference in chaoticity resulting from distance shifts such as nearby 0.5, 1.0 skip distance. Such difference in chaoticity enables the evaluation of unique features of defects in the weld zone. In quantitative chaos fenture extraction, feature values of 0.835 and 0.823 in the case of slag inclusion and 0.609 and 0.573 in the case of crack were suggested on the basis of fractal dimension and Lyapunov exponent. Proposed chaoral post-process system in this study can enhances precision rate of ultrasonic pattern recognition results from defect signals of weld zone, such as slag inclusion and crack.

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Ultrasonic NDE Classifications with the Gradient Descent Method and Synthetic Aperture Focusing Technique

  • Kim, Dae-Won
    • Journal of the Korean Society for Nondestructive Testing
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    • v.25 no.3
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    • pp.189-200
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    • 2005
  • Ultrasonic inspection methods are widely used for detecting flaws in materials. One of the more popular methods involves the extraction of an appropriate set of features followed by the use of a neural network for the classification of the signals in the feature space. This paper describes an approach which uses LMS method to determine the coordinates of the ultrasonic probe followed by the use of SAFT to estimate the location of the ultrasonic reflector The method is employed for classifying NDE signals from the steam generator tubes in a nuclear power plant. The classification results using this scheme for the ultrasonic signals from cracks and deposits within steam generator tubes are presented.