• Title/Summary/Keyword: Ultra high temperature

Search Result 542, Processing Time 0.033 seconds

Study on electrical property of self-assembled nitro molecule onto Au(111) by Using STM/STS (STM/STS에 의한 Au (111)에 자기조립된 니트로분자의 전기적 특성 측정)

  • Lee, Nam-Suk;Choi, Won-Suk;Shin, Hoon-Kyu;Chang, Jeong-Soo;Kwon, Young-Soo
    • Proceedings of the KIEE Conference
    • /
    • 2005.07c
    • /
    • pp.1844-1846
    • /
    • 2005
  • The characteristic of negative differential resistance(NDR) is decreased current when the applied voltage is increased. The NDR is potentially very useful in molecular electronics device schemes. Here, we investigated the NDR property of self-assembled 4,4- Di(ethynylphenyl)-2'-nitro-1-(thioacetyl)benzene, which has been well known as a conducting molecule. Self-assembly monolayers(SAMs) were prepared on Au(111), which had been thermally deposited onto pre-treatment$(H_2SO_4:H_2O_2=3:1)$ Si. The Au substrate was exposed to a 1mM/l solution of 1-dodecanethiol in ethanol for 24 hours to form a monolayer. After thorough rinsing the sample, it was exposed to a $0.1{\mu}M/l$ solution of 4,4-Di(ethynylphenyl)-2'-nitro-1-(thioacetyl)benzene in dimethylformamide(DMF) for 30 min and kept in the dark during immersion to avoid photo-oxidation. After the assembly, the samples were removed from the solutions, rinsed thoroughly with methanol, acetone, and $CH_2Cl_2$, and finally blown dry with $N_2$. Under these conditions, we measured electrical properties of self-assembly monolayers(SAMs) using ultra high vacuum scanning tunneling microscopy(UHV-STM). The applied voltages were from -2V to +2V with 299K temperature. The vacuum condition is $6{\times}10^{-8}$ Torr. As a result, we found the NDR voltage of the nitro-benzene is $-1.61{\pm}0.26$ V(negative region) and $1.84{\pm}0.33$ (positive region), respectively.

  • PDF

Single Carrier Spectroscopy of Bisolitons on Si(001) Surfaces

  • Lyo, In-Whan
    • Proceedings of the Korean Vacuum Society Conference
    • /
    • 2010.02a
    • /
    • pp.13-13
    • /
    • 2010
  • Switching an elementary excitation by injecting a single carrier would offer the exciting opportunity for the ultra-high data storage technologies. However, there has been no methodology available to investigate the interaction of low energy discrete carriers with nano-structures. In order to map out the spatial dependency of such single carrier level interactions, we developed a pulse-and-probe algorithm, combining with low temperature scanning tunneling microscopy. The new tool, which we call single carrier spectroscopy, allows us to track the interaction with the target macrostructure with tunneling carriers on a single carrier basis. Using this tool, we demonstrate that it is possible not only to locally write and erase individual bi-solitons, reliably and reversibly, but also to track of creation yields of single and multiple bi-solitons. Bi-solitons are pairs of solitons that are elementary out-of-phase excitations on anti-ferromagnetically ordered pseudo-spin system of Si dimers on Si(001)-c(42) surfaces. We found that at low energy tunneling the single bisoliton creation mechanism is not correlated with the number of carriers tunneling, but with the production of a potential hole under the tip. An electric field at the surface determines the density of the local charge density under the tip, and band-bending. However a rapid, dynamic change of a field produces a potential hole that can be filled by energetic carriers, and the amount of energy released during filling process is responsible for the creation of bi-solitons. Our model based on the field-induced local hole gives excellent explanation for bi-soliton yield behaviors. Scanning tunneling spectroscopy data supports the existence of such a potential hole. The mechanism also explains the site-dependency of bi-soliton yields, which is highest at the trough, not on the dimer rows. Our study demonstrates that we can manipulate not just single atoms and molecules, but also single pseudo-spin excitations as well.

  • PDF

Influence of the Solid Solution for Crystalline Phase on the Characterization of $Bi_2Sr_2Ca{_{n-1}}Cu_nO_x$(n=0,1,2) Thin Films (결정상에 대한 고용체가 $Bi_2Sr_2Ca{_{n-1}}Cu_nO_x$(n=0,1,2) 박막의 특성에 미치는 영향)

  • Yang, Seung-Ho;Lee, Ho-Shik;Park, Yong-Pil
    • Journal of the Korea Institute of Information and Communication Engineering
    • /
    • v.11 no.6
    • /
    • pp.1115-1121
    • /
    • 2007
  • [ $Bi_2Sr_2Ca{_{n-1}}Cu_nO_x$ ](n=0,1,2) thin fans have been fabricated by co-deposition at an ultra-low growth rate using ion beam sputtering(IBS) method. Bi 2212 phase appeared in the temperature range of 750 and $795^{\circ}C$ and single phase of Bi 2201 existed in the lower region than $785^{\circ}C$. Whereas, $PO_3$ dependance on structural formation was scarcely observed regardless of the pressure variation. And high quality of c-axis oriented Bi 2212 thin film with $T_c$(onset) of about 90 K and $T_c$(zero) of about 45 K is obtained. Only a small amount of CuO in some films was observed as impurity, and no impurity phase such as $CaCuO_2$ was observed in all of the obtained films.

Surface Characteristics, Antimicrobial and Photodegradation Effect of Cotton Fibers Coated with TiO2 Nanoparticles and 3-Mercaptopropyltrimethoxysilane(3-MPTMS) (TiO2 나노입자와 3-MPTMS로 코팅 처리한 면섬유의 표면 특성과 항균성 및 광분해효과)

  • Park, Sujin;Lee, Jaewoong;Kim, Sam Soo;Lee, Sang Oh
    • Textile Coloration and Finishing
    • /
    • v.30 no.4
    • /
    • pp.245-255
    • /
    • 2018
  • In this study, cotton fabrics were coated with $TiO_2$ nanoparticles using 3-mercaptopropyltrimethoxysilane(3-MPTMS), which is highly reactive to cotton fabrics, as a medium, and the characteristics, antimicrobial properties, and photodegradation properties of the fibers were measured. The manufacturing process is as follows. (1) 3-MPTMS was added to isopropanol, and $TiO_2$ colloid was added to the mixture to prepare a solution. (2) Cellulose fibers were immersed in the prepared $3-MPTMS/TiO_2$ solution, stirred for 90 minutes at $45^{\circ}C$ in a constant temperature water bath, and dried thereafter. In order to identify the morphology of the cellulose fibers coated with $TiO_2$ nanoparticles, the surface was observed with a scanning electron microscope(SEM), and SEM-EDS was measured to identify the adhesion of $TiO_2$ nanoparticles. The SEM images showed $TiO_2$ nanoparticle and 3-MPTMS coated layers on the fibers and it was identified that $TiO_2$ nanoparticles were attached to the cellulose fibers. The antimicrobial activity of $3-MPTMS/TiO_2$-treated cotton fabrics was measured using a bacterial reduction method. $3-MPTMS/TiO_2$ cellulose fibers which was irradiated by ultra violet light, showed antimicrobial activity against Escherichia coli(ATCC 43895) and Staphylococcus aureus(ATCCBAA-1707) unlike unirradiated fibers. The cellulose fibers were stained with methylene blue and the photodegradation performance of the stained fabrics was analyzed. The stained fabrics showed high degradation performance with photolytic reactions of $TiO_2$ nanoparticles.

Research to Minimize Endoscope and Objective-lens Sensitivity Using Multi-configurations (다중 구성을 이용한 내시경 및 대물렌즈 광학계 공차 민감도 최소화 설계 기술)

  • Jung, Mee-Suk
    • Korean Journal of Optics and Photonics
    • /
    • v.32 no.6
    • /
    • pp.259-265
    • /
    • 2021
  • Recently, lens manufacturing and assembly technology has greatly improved. However, tight requirements of manufacturing and assembly lead to an increase in cost and manufacturing time, and in some cases the performance of an optical system may deteriorate depending on the operating environment's conditions, such as temperature or vibration. In addition, the use of a compensator is an effective method to reduce sensitivity in an ultra-precision optical system, but in the case of a small lens, such as that in an endoscope, it is difficult to use a compensator due to the size limitation of the lens barrel. Therefore, minimizing lens sensitivity is the most important technology in lens design. For this reason, there have been various attempts to reduce the lens sensitivity, and there is a trend to add functions to reduce the sensitivity in the lens design S/W. In this paper, we introduce a design technology that minimizes lens sensitivity. We first design a lens with quite good performance, then analyze the sensitivity of this lens, make a multi-configuration with high-sensitivity element error, and then reoptimize it. We prove with an example that this design technique is very effective.

Effect of Heat Treatment on Mechanical Properties of Cross-Linked Ultra-High Molecular Weight Polyethylene Used for Artificial Joint Liner (인공관절 라이너용 가교된 초고분자량폴리에틸렌(UHMWPE)의 열처리 조건에 따른 기계적 특성 변화)

  • Kim, Hyun-Mook;Kim, Dong-Hoon;Gu, Ja-Uk;Choi, Nak-Sam;Kim, Sung-Kon
    • Composites Research
    • /
    • v.22 no.2
    • /
    • pp.1-6
    • /
    • 2009
  • The mechanical characteristics of gamma-ray irradiated UHMWPE specimens were investigated under various heat treatment conditions. The heat treatment was performed in the range of annealing and remelting temperatures. The annealing treatment below the temperature of $130^{\circ}C$ hardly induced changes in the tensile strength, the strain at the failure and the hardness. However the remelting treatment above $140^{\circ}C$ deteriorated those mechanical properties. It was shown in an FTIR analysis that the annealing treatment caused some oxidation of free radicals created by the pretreatment of the irradiation. These quantitative data represented by the behavior of mechanical properties might be used as basic informations for the design and analysis of various artificial joints.

A study on Shift Efficiency Characteristics of a 2-speed Transmission applying CVT Structure (CVT구조를 적용한 2단 변속기의 효율특성에 관한 연구)

  • Kwang-Wook Youm
    • Journal of the Korean Institute of Gas
    • /
    • v.28 no.1
    • /
    • pp.59-64
    • /
    • 2024
  • In this study, we conducted research on a miniaturized transmission system suitable for ultra-compact electric vehicles, such as electric arts or small electric cars. While conventional electric vehicles eliminate multi-gear transmissions and control motor output or secure initial driving force through reducers, in vehicles like electric karts or compact electric cars, which have relatively small battery capacities, the driving range can be reduced or the motor can be stressed epending on the loading state. Therefore, in this study, we developed a low stage ratio 0.625 and high stage ratio 1.6 a two-stage transmission system that can change gears as needed, considering factors such as slope conditions and loading status, by applying the continuously variable transmission (CVT) mechanism. Based on the selected gear ratios, we designed the transmission and created a test rig to verify the power transmission efficiency of the developed transmission. Using the test rig, we varied the rotational speed and load of the transmission to confirm its power transmission characteristics and also examined the heat generation characteristics during shifting and operation. As a result, developed a two-stage transmission with a CVT structure.

A study on CAE and injection molding of automotive thick-walled light guide with micro-optical patterns (마이크로 광학 패턴이 있는 차량용 후육 라이트 가이드의 CAE 및 사출성형에 관한 기초연구)

  • Dong-Won Lee;Jong-Su Kim;Hyeon-Hwa Lee;Sung-Hee Lee
    • Design & Manufacturing
    • /
    • v.17 no.3
    • /
    • pp.8-14
    • /
    • 2023
  • In this study, basic research was conducted on manufacturing technology of thick-walled light guide a component that controls the light source of automobile lamps. As a preliminary study for manufacturing the final injection molded parts, a model for analyzing the influence of micro patterns on light guides is presented. The optical characteristics of the light guide were analyzed according to the change of the curvature radius of the micro-optical pattern, and the injection molding characteristics of the light guide according to the change of injection molding conditions were analytically evaluated. It was confirmed that the luminance uniformity improves as the R value decreases for changes in the micro-pattern R value, but it was confirmed that there are technical limitations in actual injection mold core processing and high-replication injection molding. Injection molding analysis showed that cooling channel design is very important compared to general injection molding due to thick-wall characteristics and thickness variation. It was also confirmed that the cooling channel has a great influence on the cycle time and birefringence result due to residual stress. As a result of analyzing the influence of filling time, holding condition, and cooling on shrinkage, it was found that the cooling water temperature has a significant effect on the shrinkage of ultra-fine light guide parts, and the holding condition also has a significant effect.

Quality Changes during Storage of Low Salt Fermented Anchovy treated with High Hydrostatic Pressure (초고압 처리한 멸치젓의 저장 중 품질 변화)

  • Lim, Sang-Bin;Jwa, Mi-Kyung;Mok, Chul-Kyoon;Woo, Gun-Jo
    • Korean Journal of Food Science and Technology
    • /
    • v.32 no.2
    • /
    • pp.373-379
    • /
    • 2000
  • Low salt fermented anchovy was stored at $25^{\circ}C$ for a period of 20 days from the time of ultra-high pressure treatment under different operating conditions, such as magnitude of pressure($(200{\sim}500\;MPa)$, temperature$(20{\sim}50^{\circ}C)$ and treatment time$(5{\sim}20\;min)$ with viable cell count(VCC) and quality assessments conducted at regular intervals. VCC decreased logarithmically during storage. Lower values of VCC in the treated samples were observed compared to the untreated. A gradual increase in peroxide value was noticed during storage, compared to those of the untreated which showed a sudden rise. Thiobarbituric acid value decreased initially and remained at that level before rising almost exponentially between 12 and 20 days. Volatile basic nitrogen increased gradually during storage. Amino nitrogen remained almost constant up to 20 days, regardless of any conditions investigated. High pressure treatment maintained better quality during storage at $25^{\circ}C$ by reducing the viable cell count in low salt fermented anchovy.

  • PDF

Magnetic Tunnel Junctions with AlN and AlO Barriers

  • Yoon, Tae-Sick;Yoshimura, Satoru;Tsunoda, Masakiyo;Takahashi, Migaku;Park, Bum-Chan;Lee, Young-Woo;Li, Ying;Kim, Chong-Oh
    • Journal of Magnetics
    • /
    • v.9 no.1
    • /
    • pp.17-22
    • /
    • 2004
  • We studied the magnetotransport properties of tunnel junctions with AlO and AlN barriers fabricated using microwave-excited plasma. The plasma nitridation process provided wider controllability than the plasma oxidization for the formation of MTJs with ultra-thin insulating layer, because of the slow nitriding rate of metal Al layers, comparing with the oxidizing rate of them. High tunnel magnetoresistance (TMR) ratios of 49 and 44% with respective resistance-area product $(R{\times}A) of 3 {\times} 10^4 and 6 {\times} 10^3 {\Omega}{\mu}m^2$ were obtained in the Co-Fe/Al-N/Co-Fe MTJs. We conclude that AlN is a hopeful barrier material to realize MTJs with high TMR ratio and low $R{\times}A$ for high performance MRAM cells. In addition, in order to clarify the annealing temperature dependence of TMR, the local transport properties were measured for Ta $50{\AA} /Cu 200 {\AA}/Ta 50 {\AA}/Ni_{76}Fe_{24} 20 {\AA}/Cu 50 {\AA}/Mn_{75}Ir_{25} 100 {\AA}/Co_{71}Fe_{29} 40 {\AA}/Al-O$ junction with $d_{Al}= 8 {\AA} and P_{O2}{\times}t_{0X}/ = 8.4 {\times} 10^4$ at various temperatures. The current histogram statistically calculated from the electrical current image was well in accord with the fitting result considering the Gaussian distribution and Fowler-Nordheim equation. After annealing at $340^{\circ}C$, where the TMR ratio of the corresponding MTJ had the maximum value of 44%, the average barrier height increased to 1.12 eV and its standard deviation decreased to 0.1 eV. The increase of TMR ratio after annealing could be well explained by the enhancement of the average barrier height and the reduction of its fluctuation.