• Journal of the Korean Society of Propulsion Engineers
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• v.8 no.1
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• pp.1-7
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• 2004

The precipitation of ultra fine ammonium perchlorate(UFAP) crystals from the N-methyl pyrrolidone(NMP) solutions of ammonium perchlorate(AP) was studied. The characteristics of the precipitated crystals were investigated by means of scanning electron micrograph(SEM), X-ray diffraction(XRD), and thermogravimetric analysis(TGA). When chloroform, methylene chloride and toluene were the precipitants, the product crystals had a mean particle size less than 2$\mu\textrm{m}$. The crystallographical property and thermal decomposition behavior of the prepared UFAP were almost the same as those of the commercial AP.

• Journal of the Korean Society of Propulsion Engineers
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• v.12 no.4
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• pp.1-6
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• 2008

The burning characteristics of HTPB/AP solid propellants were measured by closed bomb of internal volume of 200 cc and 700 cc up to 30,000 psia. The burning rates of closed bomb method showed good agreement with those of strand burner method between 1,000 psia and 5,000 psia, and the sharp increment of pressure exponent(n) around 6,000 psia as a result of testing in accordance with loading densities. The burning rate measured in 200 cc and 700 cc of internal volume of closed bomb agreed well without the relation of internal volume size.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• v.y2005m4
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• pp.88-91
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• 2005

The combustion characteristics of high burning HTPB/AP solid propellants have been investigated by means of a closed bomb method of interval volume of 200 co and 700 cc at pressures from 1000 to 30,000 psi. The burning rate data measured by closed bomb are in good agreement with strand burner test results at pressure from 1000 to 5000 psi using disc sample of 1 mm thickness. The burning rate dat by using 200 cc closed bomb are in general agreement with that of 700 cc closed bomb. At pressure between $5,000\sim7,000$ psi, a market increase in pressure dependence of the linear burning rate occurs for HTPB/AP propellant.