• Title/Summary/Keyword: Two-phase extraction

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The Phase Separation of Low Alkali Borosilicate Glass by Substituting $Li_2O$ for $Na_2O$ (산화리튬의 치환에 따른 붕규산 유리의 분상에 관한 연구)

  • 양중식
    • Journal of the Korean Ceramic Society
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    • v.18 no.1
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    • pp.27-34
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    • 1981
  • The phase separation of low-alkali borosilicate glass with the composition of $6.25Na_2O$.$18.75B_2O_3$.$75.00SiO_2$(mole%) substituting $Li_2O$ for $Na_2O$ was studied. The phase separation in the temperature range of transformation was examined with various heating temperatures and soaking times. Durability to water, thermal expansion and specific density of the specimen were investigated and the microstructure of the separated phase was also observed by transmission electron micrograph techniques. The maximum alkali extraction result with the best phase separation effect was obtained when $Na_2O$ of the base glass was replaced with $1.88Li_2O$ (mole %) and electron micrograph of carbon film replica of $1.88Li_2O$$4.37Na_2O$.$18.75B_2O_3$.$75.00SiO_2$ (mole %) glass showed that the glass consisted of homogeneous two phases. The minimum specific density was shown with the specimen treated at 57$0^{\circ}C$ and it was also shown that the longer the treating time the lower the specific density. The apparent activation energies of approximately 45 kcal/mole by the alkali extraction and 43kcal/mole by the thermal expansion method were derived from the Arrhenius plots, respectively.

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Analgesic Effects of Taxus cuspidata Pharmacopuncture Using Different Extraction Methods on the Formalin-Induced Pain Model (추출 방식의 차이에 따른 주목약침이 Formalin 유도 통증 모델의 진통에 미치는 영향)

  • Shin, You Bin;Lee, Hyun Jong;Kim, Jae Soo;Lee, Yun Kyu
    • Journal of Acupuncture Research
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    • v.33 no.3
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    • pp.17-28
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    • 2016
  • Objectives : This study was designed to investigate the analgesic effects of Taxus cuspidata pharmacopuncture(TCP) at KI03 on formalin-induced pain in rats and to evaluate the efficiency of different extraction methods of Taxus cuspidata(TC). Methods : 30 rats were divided into 5 groups, each consisting of 6 rats. Each of the groups was treated two times. The first treatment for its right KI03 was as follows: rats were treated with normal saline(NOR), normal saline(CON), hot-water extraction of TC(W), ethanol extraction of TC(E), and ultrasonification extraction of TC(U). The second treatment was given 35 mins after the first one. Rats in NOR were treated with normal saline at their hind-paw. All groups, except NOR, were treated with formalin(5 %, $40{\mu}{\ell}$) at their hind-paw. To evaluate pain behavior, Ultrasonic vocalization(USV) was examined to be around 18~30 kHz. After analysis of USV, blood samples were taken from the rats for analysis of Substance P, aspartate aminotransferase(AST) and alanine aminotransferase(ALT). Results : In the experimental groups, USV was significantly decreased compared with CON and similar to that of NOR in the early phase. But there were no significant differences among the three extraction methods of TC. In addition, Substance P of W was significantly decreased. AST and ALT activation showed no significant differences among the 5 groups. Conclusion : These results show that regardless of extraction methods of TC, TCP at KI03 has analgesic effects in the early phase on formalin-induced pain in rats. In particular, hot-water extraction of TC significantly reduces Substance P activation.

Partitioning of Lactobacillus helveticus Cells and Lactic Acid in Aqueous PEI/HEC Two-Phase Systems. (수용성 이상계에서의 젖산과 Lactobacillus helveticus세포의 분배특성)

  • 안한군;권윤중
    • Microbiology and Biotechnology Letters
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    • v.26 no.1
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    • pp.55-60
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    • 1998
  • For an ideal extractive bioconversion in aqueous two-phase systems, the product has to be preferentially partitioned into the phase opposite to the one in which the biocatalyst is located. Partitioning behaviors of Lactobacillus helveticus IAM 11090 and lactic acid in aqueous two-phase systems composed a polycation, poly(ethylenimine) (PEI), and an uncharged polymer (hydroxyethyl)cellulose (HEC) were investigated. L. helveticus cells were preferentially partitioned to the HEC-rich top phase while about 85% of lactic acid was partitioned to the PEI-rich bottom phase. These results indicate that extraction of charged, low molecular weight products in an aqueous two-phase systems can be promoted by using an oppositely charged polymer as one of the phase-forming polymer. By the ideal partitioning of the cells and lactic acid, an aqueous PEI/HEC two-phase system can be used as a potential system for the extractive lactic acid fermentation of cheese whey.

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Novel-1,3-Alternate Calix[4]thiacrown Ethers

  • Sim, Won-Bo;Lee, Jai-Young;Kwon, Jong-Chul;Kim, Moon-Jib;Kim, Jong-Seung
    • Bulletin of the Korean Chemical Society
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    • v.23 no.6
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    • pp.879-884
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    • 2002
  • A series of novel 1,3-alternate calix[4]-mono-thiacrown and -bis-thiacrowns were synhesized within good yields. The three dimensional 1,3-alternate conformation was confimed by X-ray crystal structure. From the results of two phase extraction and NMR studies on the ligand-metal complex, one can conclude that the calix[4]thiacrown ethers showed the very high selectivity for silver ion over other metal ions by an electrostatic interaction between sulfur atom and silver ion and by a $\pi-metal$ complexation.

3D Object Extraction Algorithm Based on Hierarchical Phase Using Fast Fourier Transform (고속 푸리에 변환을 이용한 계층적 위상기반 3차원 객체 추출 기법)

  • 한규필;이채수;박양우;엄태억
    • Proceedings of the IEEK Conference
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    • 2001.06c
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    • pp.145-148
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    • 2001
  • This paper presents a phase-based stereo matching algorithm in order to efficiently extract 3-dimensional objects from two 2D images. Conventional phase-based methods, especially using windowed Fourier phases, inherit good properties in the cage of hierarchical approaches, because they basically use a multi-resolution phase map. On the contrary, their computational cost is too heavy. Therefore, a fast hierarchical approach, using multi-resolution phase-based strategy and reducing redundancies of phase calculations based on FFT concept is proposed in this paper. In addition, a structural matching algorithm on the phase domain is presented to improve the matching quality. In experimental results. it is shown that the computation loads are considerably reduced about 8 times and stable outputs are obtained from various images.

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Liquid Chromatography-Solid Phase Extraction-NMR (LC-SPE-NMR) Analysis of Liquid Crystalline Mixtures

  • Park, Gregory Hyung-Jin;Park, Ae-Na;Rho, Kyung-Rae;Shin, Jong-Ho;Kim, Yeong-Jeon;Jo, Sung-Chan;Oh, Weon-Sik
    • Journal of the Korean Magnetic Resonance Society
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    • v.15 no.1
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    • pp.14-24
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    • 2011
  • We have performed Liquid Chromatography-Solid Phase Extraction-NMR (LC-SPE-NMR) analysis for liquid crystalline mixture and elucidated the structures of selected components by NMR spectra. Combining the results of one-dimensional 1H experiments as well as homonuclear and heteronuclear two-dimensional experiments, we could analyze the molecular structure of the liquid crystal singles whose structure had not been interpretable by mass spectrometry alone.

Design of QR Decomposition Processor for GDFE (GDFE를 위한 QR분해 프로세서 설계)

  • Cho, Kyung-Ju
    • The Journal of the Korea institute of electronic communication sciences
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    • v.6 no.2
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    • pp.199-205
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    • 2011
  • This paper presents a QR decomposition processor by exploiting Givens rotation for the GDFE (Generalized Decision Feedback Equalizer). A Givens rotation consists of phase extraction, sine/cosine generation and angle rotation parts. Combining two-stage method (coarse and fine stage) and the fixed-width modified-Booth multiplier, we design an efficient QR decomposition processor. By simulations, it is shown that the proposed QR decomposition processor can be a feasible solution for GDFE.

Characterization of Natural Organic Matter in Spring Water

  • Yoo, Hee-Jin;Choi, Yoon-Ji;Cho, Kun
    • Mass Spectrometry Letters
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    • v.11 no.4
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    • pp.90-94
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    • 2020
  • Interest in aspects of industrialization relating to human health has increased. Accordingly, the use of labels such as 'natural foods' and 'organic ingredients' has become more widespread, and greater emphasis is being placed on improving quality of life. Water is an essential element for human life, and water quality has a significant impact on human health. However, technology that can precisely determine the substances present in water is still lacking. This study was conducted to establish a complete mass spectrometry process, from pretreatment to analysis, to measure and characterize natural organic matter (NOM) in Korean spring water samples. Salts and other matrices were removed from the samples using solid-phase extraction (SPE) with two different columns (PPL and C18). After establishing an accurate analysis method, the experimental results were evaluated based on Van Krevelen diagrams and analysis of molar O/C and H/C ratios. The method for characterizing NOM introduced herein should facilitate evaluation of water quality.

Feature Extraction for Fault Signals of High Voltage Motor Stator Windings (고압전동기 결함신호의 특징추출에 관한 연구)

  • Park, Jae-Jun;Kim, Hee-Dong
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2004.07b
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    • pp.1154-1157
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    • 2004
  • During normal machine operation, partial discharge(PD) measurements were performed with turbine generator analyzer(TGA) in imitation stator winding of high voltage motors. The motor was energized to 4.47kV, 6.67, respectively. Applied voltage to Imitation winding was used two voltage level, 4.47[KV]and 6.67[KV]. Motors having imitation stator winding were installed with 80pF capacitive couplers at the terminal box Case of PD Pattern regarding applied voltage phase angel, the PD patterns were displayed two dimensional and three dimensional. TGA summarizes each plot with two quantities such as the normalized quantity number(NQN) and the peak PD magnitude(Qm). As the result, we could discrimidate using TGA the difference of internal and surface discharge for imitation stator winding. We have used the other technique, in order to feature extraction of faulty signals on stator winding, Daubechies Discrete wavelet transform and Harmonics analysis(FFT) about faulty signals.

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Two Unresolved Target Angle Estimation in Phase Comparison Monopulse Radar (위상비교모노펄스를 이용한 근접한 두 표적 분리에 관한 연구)

  • Lee, Seung-Phil;Cho, Byung-Lae;Kim, Young-Soo
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.27 no.6
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    • pp.539-544
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    • 2016
  • This paper improves Sherman's two-pulse method for angle estimation of two unresolved targets in phase comparison monopulse radar. The proposed method provides the angle information with only a single-pulse measurement instead of two pulses. The proposed method can estimate a single-target angle by single-target indicator, in contrast with previous techniques. The accuracy of angle estimation for proposed method is demonstrated by simulations.