• Title/Summary/Keyword: Two-layer Beam

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Transmission Electron Microscopy Specimen Preparation for Two Dimensional Material Using Electron Beam Induced Deposition of a Protective Layer in the Focused Ion Beam Method

  • An, Byeong-Seon;Shin, Yeon Ju;Ju, Jae-Seon;Yang, Cheol-Woong
    • Applied Microscopy
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    • v.48 no.4
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    • pp.122-125
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    • 2018
  • The focused ion beam (FIB) method is widely used to prepare specimens for observation by transmission electron microscopy (TEM), which offers a wide variety of imaging and analytical techniques. TEM has played a significant role in material investigation. However, the FIB method induces amorphization due to bombardment with the high-energy gallium ($Ga^+$) ion beam. To solve this problem, electron beam induced deposition (EBID) is used to form a protective layer to prevent damage to the specimen surface. In this study, we introduce an optimized TEM specimen preparation procedure by comparing the EBID of carbon and tungsten as protective layers in FIB. The selection of appropriate EBID conditions for preparing specimens for TEM analysis is described in detail.

PDMS기판에 이온빔 처리에 따른 수평 액정의 배향 연구

  • Kim, Yeong-Hwan;O, Byeong-Yun;Kim, Byeong-Yong;Lee, Won-Gyu;Im, Ji-Hun;Na, Hyeon-Jae;Seo, Dae-Sik
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2009.11a
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    • pp.159-159
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    • 2009
  • We characterize a flexible self-assembled liquid crystal display (LCD) fabricated from a polyimide (PI) alignment layer with polydimethylsiloxane pixel walls. Ion beam (IB) irradiation aligned LC molecules in the PI layer and bonded two flexible plastic substrates in a one-step assembly of the pixel walls. X-ray photoelectron spectroscopic analysis, Fourier transform infrared spectroscopy, and scanning electron microscopy provided chemical and physical evidence for the formation of stable chemical bonds between the PI layer and the PDMS pixel walls in addition to the important maintenance of a uniform 6 um gap between the two substrates without the use of any epoxy resins or other polymers.

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Growth of Epitaxial AlN Thin Films on Sapphire Substrates by Plasma-Assisted Molecular Beam Epitaxy (플라즈마분자선에피탁시법을 이용한 사파이어 기판 위 질화알루미늄 박막의 에피탁시 성장)

  • Lee, Hyo-Sung;Han, Seok-Kyu;Lim, Dong-Seok;Shin, Eun-Jung;Lim, Se-Hwan;Hong, Soon-Ku;Jeong, Myoung-Ho;Lee, Jeong-Yong;Yao, Takafumi
    • Korean Journal of Materials Research
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    • v.21 no.11
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    • pp.634-638
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    • 2011
  • We report growth of epitaxial AlN thin films on c-plane sapphire substrates by plasma-assisted molecular beam epitaxy. To achieve two-dimensional growth the substrates were nitrided by nitrogen plasma prior to the AlN growth, which resulted in the formation of a two-dimensional single crystalline AlN layer. The formation of the two-dimensional AlN layer by the nitridation process was confirmed by the observation of streaky reflection high energy electron diffraction (RHEED) patterns. The growth of AlN thin films was performed on the nitrided AlN layer by changing the Al beam flux with the fixed nitrogen flux at 860$^{\circ}C$. The growth mode of AlN films was also affected by the beam flux. By increasing the Al beam flux, two-dimensional growth of AlN films was favored, and a very flat surface with a root mean square roughness of 0.196 nm (for the 2 ${\mu}m$ ${\times}$ 2 ${\mu}m$ area) was obtained. Interestingly, additional diffraction lines were observed for the two-dimensionally grown AlN films, which were probably caused by the Al adlayer, which was similar to a report of Ga adlayer in the two-dimensional growth of GaN. Al droplets were observed in the sample grown with a higher Al beam flux after cooling to room temperature, which resulted from the excessive Al flux.

Heterogeneity of hard skin layer in wrinkled PDMS surface fabricated by Ar ion beam irradiation (아르곤 이온빔 조사로 형성된 주름진 PDMS 표면 경화층의 이질성)

  • Lee, Seunghun;Byeon, Eunyeon;Kim, Do-Geun;Jung, Sunghoon
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2018.06a
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    • pp.43.1-43.1
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    • 2018
  • Spatial distribution of binding state in depth direction is investigated in a hard skin layer on soft polydimethylsiloxane (PDMS) fabricated by Ar ion beam irradiations. The hard skin layer known as a silica-like homogenous layer was composed of two layers. Impinging Ar ions transfer energy to PDMS as a function of collisional energy transfer rate, which is the maximum at surface and decreases gradually as an ion penetrates. This formed the heterogeneous hard skin layer that consists of a top-most layer and an intermediate layer. XPS depth profiling showed the existence of the top-most layer and intermediate layer. In the top-most layer, scission and cross-linking were occurred simultaneously and Si-O bond showed dissociated status, SiOx (x = 1.25 - 1.5). Under the top-most layer, there was the intermediate layer in which cross-linking is mainly occurred and Si-O bond showed silica-like binding status, SiOx (x = 1.75 - 2). And theoretical analysis which calculates the collisional energy transfer and a displacement per atom explained the thickness variation of top-most layer according to Ar ion energy from 360 eV to 840 eV.

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Enhancement of Crystallinity and Exchange Bias Field in NiFe/FeMn/NiFe Trilayer with Si Buffer Layer Fabricated by Ion-Beam Deposition (이온 빔 증착법으로 제작한 NiFe/FeMn/NiFe 3층박막의 버퍼층 Si에 따른 결정성 및 교환결합세기 향상)

  • Kim, Bo-Kyung;Kim, Ji-Hoon;Hwang, Do-Guwn;Lee, Sang-Suk
    • Journal of the Korean Magnetics Society
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    • v.12 no.4
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    • pp.132-136
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    • 2002
  • Enhancement of crystallinity and exchange bias characteristics for NiFe/FeMn/NiFe trilayer with Si buffer layer fabricated by ion-beam deposition were examined. A Si buffer layer promoted (111) texture of fcc crystallities in the initial growth region of NiFe layer deposited on it. FeMn layers deposited on Si/NiFe bilayer exhibited excellent (111) crystal texture. The antiferromagnetic FeMn layer between top and bottom NiFe films with the buffer Si 50 ${\AA}$-thick induced a large exchange coupling field Hex with a different dependence. It was found that H$\sub$ex/ of the bottom and top NiFe films with Si buffer layer revealed large value of about 110 Oe and 300 Oe, respectively. In the comparison of two Ta and Si buffer layers, the NiFe/FeMn/NiFe trilayer with Si could possess larger exchange coupling field and higher crystallinity.

Electro-magneto-elastic analysis of a three-layer curved beam

  • Arefi, Mohammad;Zenkour, Ashraf M.
    • Smart Structures and Systems
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    • v.19 no.6
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    • pp.695-703
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    • 2017
  • In this paper, based on first-order shear deformation theory, the governing equations of motion for a sandwich curved beam including an elastic core and two piezo-magnetic face-sheets are presented. The curved beam model is resting on Pasternak's foundation and subjected to applied electric and magnetic potentials on the piezo-magnetic face-sheets and transverse loading. The five equations of motion are analytically solved and the bending and vibration results are obtained. The influence of important parameters of the model such as direct and shear parameters of foundation and applied electric and magnetic potentials are studied on the electro-mechanical responses of the problem. A comparison with literatures was performed to validate our formulation and results.

Evaluation of the Effect of Asphalt and Geotextile Interlayer on Unbonded Concrete Overlay (비접착식 콘크리트 덧씌우기 포장에서의 아스팔트와 Geotextile 중간층에 대한 영향 평가)

  • Cho, Seong-Hwan;Im, Jeong Hyuk;Hwang, Sung-Do
    • International Journal of Highway Engineering
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    • v.16 no.2
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    • pp.91-98
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    • 2014
  • PURPOSES : The objective of this study is to investigate the effect of asphalt and geotextile interlayer on the fracture behavior of unbonded concrete overlay through a laboratory composite beam test. METHODS : In order to evaluate the effect of interlayer materials on the fracture behavior of unbonded concrete overlay, a laboratory test of composite beam was conducted with different types of interlayer. The test results of the composite beam using two types of geotextile interlayer with different thicknesses were compared to the test results of the composite beam using the tradition type of asphalt interlayer. The unbonded concrete overlay on the existing concrete pavement without interlayer was set for the control condition. RESULTS AND CONCLUSION : Overall, the laboratory composite beam test results did show the effect of asphalt and geotextile interlayer on the fracture behavior of composite concrete beams. The three-layer geotextile interlayer and HMA layer both increase the peak load when the first macrocrack occurs in the top concrete beam, while the HMA interlayer causes the smallest load drop percentage after the first macrocrack. The three-layer geotextile did show better performance than the single-layer geotextile through the greater peak load and smaller load drop percentage. It indicates that the thickness of geotextile interlayer will affect the fracture behavior of unbonded concrete overlay and the thicker geotextile interlayer is recommended.

Simulation and Design of Optimized Three-Layer Radiation Shielding to Protect Electronic Boards of Satellite Revolving in Geostationary Earth Orbit (GEO) Orbit against Proton Beams

  • Ali Alizadeh;Gohar Rastegarzadeh
    • Journal of Astronomy and Space Sciences
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    • v.41 no.1
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    • pp.17-23
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    • 2024
  • The safety of electronic components used in aerospace systems against cosmic rays is one of the most important requirements in their design and construction (especially satellites). In this work, by calculating the dose caused by proton beams in geostationary Earth orbit (GEO) orbit using the MCNPX Monte Carlo code and the MULLASSIS code, the effect of different structures in the protection of cosmic rays has been evaluated. A multi-layer radiation shield composed of aluminum, water and polyethylene was designed and its performance was compared with shielding made of aluminum alone. The results show that the absorbed dose by the simulated protective layers has increased by 35.3% and 44.1% for two-layer (aluminum, polyethylene) and three-layer (aluminum, water, polyethylene) protection respectively, and it is effective in the protection of electronic components. In addition to that, by replacing the multi-layer shield instead of the conventional aluminum shield, the mass reduction percentage will be 38.88 and 39.69, respectively, for the two-layer and three-layer shield compared to the aluminum shield.

Performance Analysis of Dual-layer Beamforming Technique for MIMO-OFDM System (MIMO-OFDM 시스템에서 이중계층 빔포밍 기법의 성능분석)

  • Li, Xun;Kim, Young-Ju;Park, Noe-Yoon
    • Journal of the Institute of Electronics Engineers of Korea TC
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    • v.47 no.5
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    • pp.18-24
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    • 2010
  • This paper propose a dual-layer beam-forming technique for MIMO-OFDM systems. Dual-layer beam-forming is a capacity enhancing technique to transmit two streams of source data with more than two transmit and receive antennas. Beamforming is a technique to enhance the link-level performances gain using antenna array with the small inter element distance. The proposed scheme can obtain both high capacity of spatial multiplexing and antenna array gain of beamforming for MIMO-OFDM systems. Therefore, it provides better BER performance than the traditional spatial multiplexing and beamforming techniques under the same simulation environment.

Analysis of Beam Hardening of Modulation Layers for Dual Energy Cone-beam CT (에너지 변조 필터로 구현한 이중 에너지 콘빔 CT의 에너지 스펙트럼 평가 연구)

  • Ahn, Sohyun;Cho, Sam Ju;Keum, Ki Chang;Choi, Sang Gyu;Lee, Rena
    • Progress in Medical Physics
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    • v.27 no.1
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    • pp.8-13
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    • 2016
  • Dual energy cone-beam CT can distinguish two materials with different atomic compositions. The principle of dual energy cone-beam CT based on modulation layer is that higher energy spectrum can be acquired at blocked x-ray window. To evaluate the possibility of modulation layer based dual energy cone-beam CT, we analyzed x-ray spectrum for various thicknesses of modulation layers by Monte Carlo simulation. To compare with the results of simulation, the experiment was performed on prototype cone-beam CT for 50~100 kVp with CdTe XR-100T detector. As the result of comparing, the mean energy of energy spectrum for 80 kVp are well matched with that of simulation. The mean energy of energy spectrum for 80 and 120 kVp were increased as 1.67 and 1.52 times by 2.0 mm modulation layer, respectively. We realized that the virtual dual energy x-ray source can be generated by modulation layer.