• 제목/요약/키워드: Tungsten ethoxide

검색결과 1건 처리시간 0.016초

텅스텐 에톡사이드의 기상 반응을 이용한 초미립 WC 분말의 합성 (Synthesis of Nano-sized Tungsten Carbide Powders by Vapor Phase Reaction of Tungsten Ethoxide)

  • 가미다;하국현;김병기
    • 한국분말재료학회지
    • /
    • 제10권1호
    • /
    • pp.1-5
    • /
    • 2003
  • Nano-sized WC powders were synthesized by vapor phase reaction using the precusor of tungsten ethoxide under helium and hydrogen atmosphere. The phases of the powder were varied with reaction Bone and gas flow rate. The powder size was about 30nm in diameter, and the tungsten carbide powder was coated by carbon layer. The synthesis of nano-sized WC powders was promoted as the hydrogen gas flow rate became higher. Inversely, tungsten oxide was formed by increasing the flow rate of helium gas. The synthesized powders were analyzed by XRD, FE-SEM, carbon analyzer etc.