• Title/Summary/Keyword: Tumbling

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A Study on the Preparation of Granules by Mixer Granulation

  • Lee, Kang-Choon;Shin, Hong-Min;Rhee, Shang-hi;Kim, Yong-Bae
    • Archives of Pharmacal Research
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    • v.2 no.1
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    • pp.17-24
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    • 1979
  • A first systematic approach on new and simple preparation method of spherical granules in the system using organic granulating solution was carried out. Mixer granulation required narrow range of moisture content but gentle action of tumbling in the mixer and capilary forces were adequate to compact the porous mass and also were highly effective to produce granules close to sphere. Where the granules by massing and screening provided the more open structure, its pore distribution lied between 71 and 16 .mu.m by above 50% and on the contrary, that of the mixer granulated granules showed only below 25%. Increase in retention time in the mixer decreased the intragranular porosity of granules produced, and in comparison with granular particles produced by conventional wet granulation, those from the mixer granulation had the advantages of flow properties, packing characteristics and definite spherocity. They also had extremely low friability resulting in few fines.

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An NMR Study on Complexation of Ethylammonium Ion by Alkyl p-tert-Butylcalix[6]aryl Ester Derivatives

  • 안상두;문철순;정기주;이조웅;오원석;장석규
    • Bulletin of the Korean Chemical Society
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    • v.19 no.1
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    • pp.68-74
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    • 1998
  • The complexation of ethylammonium ion by alkyl p-tert-butylcalix[6]aryl ester derivatives was studied via measurements of proton and carbon spin-lattice relaxation times $(T_1)$ and chemical shift changes in solution state $(CDCl_3)$. The results indicate that the endo-type complexes are formed and that the overall tumbling rates of these complexes are more rapid than those of the corresponding free hosts. The association constants for these complexes in $THF-d_8$ were determined by $^1H$ NMR titration at several different temperatures to estimate the relevant thermodynamic parameters. The logK's for ethylammonium complexes of methyl, ethyl, and propyl esters at 313 K, for example, were found to be 1.56, 3.41, and 3.08, respectively. The complexes formed may be thought of as being kinetically stable in view of their $^1H$ NMR behavior in 2 : 1 host/guest solution.

The Effect of Piston Configuration on Combustion and Flame Propagation (피스톤 형상이 연소와 화염전파에 미치는 영향)

  • Jie, Myoung-Seok;Kang, Ki-Young
    • Journal of the Korean Society of Industry Convergence
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    • v.22 no.5
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    • pp.511-517
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    • 2019
  • Two type pistons which had different configuration were made to find out the effects on combustion and flame propagation. Flame propagation speed was obtained by use of the cylinder head gasket ionization probe. Ionization Probe voltage output and flame propagation speed were increased according to the air fuel mixture ratio increase. Exhaust direction flame propagation speed was fastest in combustion chamber and next was front direction, rear direction and intake direction cause of tumbling motion in cylinder. In case of remove the valve pocket in piston, average flame propagation speed changed slowly and spark timing was advanced. Also emission was decreased.

A Real-time Motion Adaptation Method using Spatial Relationships between a Virtual Character and Its Surrounding Environment

  • Jo, Dongsik;Choi, Myung Geol
    • Journal of the Korea Society of Computer and Information
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    • v.24 no.4
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    • pp.45-50
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    • 2019
  • Recently, character motion have been used extensively in the entertainment business, and researchers have investigated algorithms of reproducing, editing, and simulating mimic human movements. Also, many recent researches have suggested how a character interacts with its surrounding environment in terms of motion. Specially, spatial relationships of the environment have been introduced for adapting and preserving character motion. In this paper, we propose a motion adaptation technique preserving a spatial property between a virtual character and the configuration of its surrounding space. Additionally, we report on experimental results of smoothly adapted motions in various environmental structures with original motions such as walk, jump, and tumbling.

A Study on Relationship between Point Load Strength Index and Abrasion Rate of Sediment Particle (퇴적물 입자의 점하중강도지수와 마식율의 관계에 대한 연구)

  • Kim, Jong-Yeon
    • Journal of the Korean Geographical Society
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    • v.43 no.6
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    • pp.808-823
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    • 2008
  • Sediment abrasion in rivers is caused by the interaction between bedrock channel bed and sediment particles transported through the river. Abrasion rate of sediment particles in rivers is controlled by two major factors; Sediment transport conditions including hydraulic conditions form the erosive forces and physical and chemical strengths of the particles form a resistance force against abrasion and other erosional processes. Physical experiments were performed to find the role of each variable on sediment abrasion process. Total 266 sediment particles were used in this experiment. All sediment particles were divided into 11 independent sediment groups with sediment particle size and sediment loads. Each sediment groups were abraded in tumbling mill for up to 8 hours. Changes in weight were recorded by run and total: 2,128 cases of abrasion rate were recoded. Physical strength of rock particles was measured with point load strength index. It is found that sediment abrasion rate has a negative functional relationship point load strength index ($I_{a(50)}$) ($R^2=0.22$). It was suggested that physical strength of sediment particles set the "maximum possible abrasion rate'. As sediment flux increases, abrasion rates of sediment particles with similar point load strength index were changed. It could be concluded that not only physical characteristics of sediment particles, but also sediment transport conditions control sediment abrasion rates.

Scaling Up Fabrication of UO2 Porous Pellet With a Simulated Spent Fuel Composition (모의 사용후핵연료 조성의 UO2 다공성펠렛 제조 스케일 업)

  • Jeon, Sang-Chae;Lee, Jae-Won;Yoon, Joo-Young;Cho, Yung-Zun
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.15 no.4
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    • pp.343-353
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    • 2017
  • Processing and equipment were tailored for engineering scale fabrication of $UO_2$ porous pellets, a feed material for the electrolytic reduction process in the PRIDE (PyRoprocessing Integrated DEmonstration) facility at KAERI (Korea Atomic Energy Research Institute). The starting materials, $UO_2$ powder and pre-milled surrogate oxide powders, were proportioned to simulate the chemical composition of spent fuel (so-called Simfuel). The Simfuel powders were homogenized by mixing, compacted into a pellet shape, and finally heat treated using a tumbling mixer, rotary press, and sintering furnace. After sintering at $1450^{\circ}C$ for 24 h in $4%\;H_2-Ar$, the average bulk density of the $UO_2$ Simfuel pellets was $6.89g{\cdot}cm^{-3}$, which meets the standard of the following electrolytic reduction process. In addition, the results of a microstructural analysis demonstrated that the sintered Simfuel $UO_2$ porous pellets accurately simulate the properties of spent fuel in terms of the formation of second phases. These results provide essential information for the massive fabrication of $UO_2$ porous pellets for engineering scale pyroprocessing research.

Structural Studies of Membrane Protein by Solid-state NMR Spectroscopy (고체상 핵자기공명 분광법을 이용한 막단백질의 구조연구)

  • Kim, Yongae
    • Analytical Science and Technology
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    • v.17 no.5
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    • pp.388-392
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    • 2004
  • Structural studies of membrane proteins, importantly involving interpretation of genomics information, many signaling pathway and major drug target for drug discovery, are having difficulty in characterizing the function using conventional solution nmr spectroscopy and x-ray crystallography because phospholipid bilayers hindered fast tumbling and crystallization. Here, we studied the structure of the pf1 coat protein in oriented phospholipid bilayers by home-built solid-state NMR probe. Bacteriophage pf1 was purified from Paeudomonas Aeruginosa and coat protein of bacteriophage pf1 was isolated from DNA and other proteins.

Conformational Studies of Macrocyclic Corrin-Ring of Coenzyme B12 by NMR methods

  • Kim, Daesung;Park, Jung-Rae;Hoshik Won
    • Journal of the Korean Magnetic Resonance Society
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    • v.3 no.1
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    • pp.44-51
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    • 1999
  • An enzyme derived conformational changes of cobalamine is thought to be important in the homolytic cleavage of Co-C bond which is the first step of catalytic Cl-cycle of coenzyme B12-dependent enzymes. Modern 2D-NMR and NMR-based distance geometric studies were carried out to determine the 3D structure of corrin ring. Homonuclear and heteronuclear correlation NMR experiments were performed for complete 1H-NMR signal assignments. Distances between numerous proton pairs were deduced based on the NOE cross peak intensities and subsequently used as input into the distance geometry program for the 3D structure determination. The detailed 3D structure from the present NMR-based analysis was compared with the result from X-ray crystallographic study, which revealed greater conformational changes occur in benzimidazole group and sugar ring than in macrocyclic corrin and tetrapyrrole. In addition, the distance geometry used in this study was found to be quite useful for NMR-based structure determination of medium-sized molecules that give poor NOE effects arising from their intermediate tumbling rate ($\omega$$\tau$c 1.0).

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CAR DETECTION IN COLOR AERIAL IMAGE USING IMAGE OBJECT SEGMENTATION APPROACH

  • Lee, Jung-Bin;Kim, Jong-Hong;Kim, Jin-Woo;Heo, Joon
    • Proceedings of the KSRS Conference
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    • v.1
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    • pp.260-262
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    • 2006
  • One of future remote sensing techniques for transportation application is vehicle detection from the space, which could be the basis of measuring traffic volume and recognizing traffic condition in the future. This paper introduces an approach to vehicle detection using image object segmentation approach. The object-oriented image processing is particularly beneficial to high-resolution image classification of urban area, which suffers from noisy components in general. The project site was Dae-Jeon metropolitan area and a set of true color aerial images at 10cm resolution was used for the test. Authors investigated a variety of parameters such as scale, color, and shape and produced a customized solution for vehicle detection, which is based on a knowledge-based hierarchical model in the environment of eCognition. The highest tumbling block of the vehicle detection in the given data sets was to discriminate vehicles in dark color from new black asphalt pavement. Except for the cases, the overall accuracy was over 90%.

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Study of Molecular Reorientation in Liquid with Raman Spectroscopy (I). Anisotropic Rotation of CDC$l_3$ in Neat Liquid (용액 중에서의 분자의 재배치 운동에 관한 라만 분광법적 연구 (제1보). 순수 액체상태의 $CDCl_3$에 관한 비등방성 회전)

  • Myung Soo Kim;Kook Joe Shin
    • Journal of the Korean Chemical Society
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    • v.26 no.4
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    • pp.205-209
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    • 1982
  • Anisotropic rotation of $CDCl_3$ in neat liquid is investigated by the analysis of ${\nu}_1$ band of Raman spectrum and the diffusion constant($D_{\perp}$) for the tumbling motion is obtained. The diffusion constant ($D_{II}$) for the spinning motion is obtained from the above $D_{\perp}$ value and the chlorine-35 nuclear quadrupole relaxation time. The diffusion constants thus obtained seem to agree very well with the ones obtained from $^2H$ and $^35C$l in NQR results within experimental errors. The data suggest fairly anisotropic character of reorientational motions in neat $CDCl_3$.

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