• Title/Summary/Keyword: Treatment phase

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Study on commercialization process of Bi-B223 HTS tape (Bi-2223 고온초전도 선의 상용화 공정 연구)

  • 하동우;김상철;오상수;하홍수;이동훈;양주생;황선역
    • Progress in Superconductivity and Cryogenics
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    • v.6 no.1
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    • pp.1-5
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    • 2004
  • Long length of Bi-2223/Ag superconducting wives were fabricated by stacking and drawing process with advanced heat-treatment schedules. Intermediate annealing was carried out to increase the homogeneity and uniformity of the superconducting filaments embedded in the silver matrix. Phase modification from tetragonal to orthorhombic Bi-2212 by pre heat treatment(PHT) was executed to improve the texture and phase transformation of Bi-2223. Drawing stress was measured to predict the sausaging and stress limit. Rolling Parameters such as thickness. width and winding tension were investigated to roll the tape with uniformity. 1 km length of Bi-2223/Ag superconducting wires were fabricated without any breakage. Critical current (Je) of 270 m length of superconducting tapes was measured over than $70 A/cm^2$ continuously after final sintering.

Treatment of Wastewater from Purified Terephtalic Acid (PTA) Production in a Two-stage Anaerobic Expanded Granular Sludge Bed System

  • Lee, Young-Shin;Han, Gee-Bong
    • Environmental Engineering Research
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    • v.19 no.4
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    • pp.355-361
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    • 2014
  • The wastewater treatment with a two-phase expanded granular sludge bed (EGSB) system for anaerobic degradation of acetate, benzoate, terephtalate and p-toluate from purified terephtalic acid (PTA) production was studied. The feasibility and effectiveness of the system was evaluated in terms of organic oxidation by chemical oxygen demand (COD), gas production, bacterial adaptability and stability in the granular sludge. Average removal efficiencies 93.5% and 72.7% were achieved in the EGSB reactors under volumetric loading rates of $1.0-15kg-COD/m^3/day$ and terephtalate and p-toluate of 351-526 mg/L, respectively. Gas production reached total methane production rate of 0.30 L/g-COD under these conditions in the sequential EGSB reactor system. Higher strength influent COD concentration above 4.8 g-COD/L related to field conditions was fed to observe the disturbance of the EGSB reactors.

Effect of heat treatment condition on optical properties of ZnS:Mn,Cu,Cl phosphor

  • Lee, Hak-Soo;Cho, Tai-Yeon;Gwak, Ji-Hye;Han, Sang-Do;Han, Chi-Hwan;Park, Sang-Hyun;Chun, Il-Su
    • 한국정보디스플레이학회:학술대회논문집
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    • 2007.08b
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    • pp.1534-1536
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    • 2007
  • ZnS-based orange-emitting phosphors were synthesized by two-step firing process: above $1000^{\circ}C$ to obtain hexagonal phase, and at $750^{\circ}C$ for cubic phase. The effect of heat treatment condition on the optical properties was investigated to fine an optimum condition for high-performance ZnS:Mn,Cu,Cl phosphor.

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Characterization of Solid Phase Crystallization in Sputtered and LFCVD Amorphous Silicon Thin Film (스퍼터링 및 저압화학기상증착 비정질 실리곤 박막의 고상 결정화 특성)

  • 김형택
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1995.11a
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    • pp.89-93
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    • 1995
  • Effects of hydrogenation in amorphous silicon rile growths on Solid Phase Crystallization (SPC) was investigated using x-ray diffractometry, energy dispersive Spectroscopy, and Raman spectrum. Interdiffusion of barium(Ba) and aluminum(Al) compounds of corning substrate was observed in both of rf sputtering and LFCVD films under the low temperature(580$^{\circ}C$) annealing. Low degree of crystallinity resulted from the interdiffusion was obtained. Highly applicable degree of crystallinity was obtained through the mechanical damage induced surface activation on amorphous silicon films. X-ray diffraction intensity of (111) orientation was used to characterize the degree of crystallinity of SPC. Nucleation and growth rate in SPC could be controllable through the employed surface treatment. IIydrogenated LPCVD films showed the superior crystallinity to non-hydrogenated sputtering films. Insignificant effects of activation treatment in sputtered film was of activation treatment in sputtered film was observed on SPC.

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The Effects of CPAP Therapy Program on Hypernasality in Preschool Children with Cleft Lips and Palates (CPAP(Continuous Positive Airway Pressure) 치료 프로그램이 취학 전 구순.구개열 아동의 과대비성 개선에 미치는 효과)

  • Jo, Sung-Mi;Jeong, Ok-Ran;Han, Ki-Hwan
    • Speech Sciences
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    • v.14 no.4
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    • pp.261-271
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    • 2007
  • The purpose of this study was to determine the effectiveness of CPAP (Continuous Positive Airway Pressure) therapy on the treatment of hypernasality in patients with cleft lips and palates. 7 preschool children with severe hypernasality participated in the study. Acoustic measurements of nasality were done by using the NasalView (version 1.31). Results showed that the nasalance values were reduced linearly in both vowels according to the treatment period. The sharp treatment effect was observed at the beginning stage. The nasality values of the vowel /i/ showed a sharp decrease at the Evaluation Phase 1 and 2 and a small increase at the Phase 4 followed by a drop in the end. Further studies would be desirable for various patients with different disorder types.

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Sintering and Heat Treatment Characteristics of Al-Cu-Mg Powder Metallurgy Alloy for Lightweight Automotive Parts (자동차 경량 부품 제조를 위한 Al-Cu-Mg 분말 합금의 소결 및 열처리 특성)

  • Ahn, Byungmin
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.23 no.2
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    • pp.152-156
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    • 2014
  • Lightweight materials such as aluminum and magnesium have recently received much attention in the automotive industries because of environmental and fuel-efficiency concerns. Using the powder metallurgy (PM) process for these materials creates significant opportunities for the cost-effective manufacture of lightweight automotive parts. In the present study, an Al-Cu-Mg alloy was fabricated using conventional PM processes. Primarily, the effects of the alloying elements on the sintering characteristics and mechanical behavior after heat treatment were investigated. A microstructural analysis was performed using an optical microscope and a scanning electron microscope to investigate the behavior of liquid phase sintering, including the formation of precipitates. The dependence of the mechanical behavior on the alloying elements was evaluated based on the transverse rupture strength.

Effect of CaO Addition on Age Hardening Behavior of AZ91 Alloy (AZ91 합금의 시효경화 거동에 미치는 CaO 첨가의 영향)

  • Jun, Joong-Hwan
    • Journal of the Korean Society for Heat Treatment
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    • v.24 no.4
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    • pp.193-198
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    • 2011
  • Effect of CaO addition on age hardening response has been studied by using optical microscopy, scanning electron microscopy and differential thermal analysis in AZ91 and CaO-containing ECO-AZ91 alloys. After solution treatment, the ${\beta}$($Mg_{17}Al_{12}$) phase formed during solidification mostly disappeared in the microstructure in the AZ91 alloy, whereas numerous ${\beta}$ precipitates containing Ca were still observed in the ECO-AZ91 alloy due to its enhanced thermal stability. The ECO-AZ91 alloy showed the delayed peak aging time and higher peak hardness compared with those of the AZ91 alloy. The activation energies for ${\beta}$ precipitation calculated by means of Kissinger method increased from 71.4 to 85.6 kJ/mole by the addition of CaO, which implies that CaO plays a role in reducing ${\beta}$ precipitation rate in the AZ91 alloy.

Phase Transformation Behavior on Aging Treatment in CuAINi Shape Memory Alloy (CuAINi 형상기억합금의 시효처리에 따른 상변태 거동)

  • Yang, G.S.;Kang, J.W.
    • Journal of the Korean Society for Heat Treatment
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    • v.6 no.4
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    • pp.213-222
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    • 1993
  • This research was performed to investigate the transformation behavior and shape memory effect of Cu-13.5Al-4.5Ni(wt%) alloy with various aging temperature and time. The results obtained in this study are as follows: Transformation temperature was very increased when aging temperature is at $250^{\circ}C$. The variation of transformation temperature in first reverse transformation cycle and second was very significant, but there was little difference in case of 2nd and 3rd. Transformation temperature at various aging temperature was increased with increasing of aging temperature and time. Microvickers hardness was increased with increasing of aging temperature and time. It was found that ${\alpha}$ and ${\gamma}_2$ phase were created by aging of long time at high temperature.

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Embrittlement Behavior of Zirconium Alloy in Quenching Heat Treatment (급랭 열처리시 지르코늄 합금의 취성 거동)

  • Kim, Jun Hwan;Lee, Jong Hyuk;Choi, Byoung Kwon;Jeong, Yong Hwan
    • Journal of the Korean Society for Heat Treatment
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    • v.17 no.4
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    • pp.216-222
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    • 2004
  • Study was focused on the quenching embrittlement property of Zircaloy-4 cladding simulated Loss Of Coolant Accident (LOCA) environment in terms of high temperature oxidation and phase transformation. Property in LOCA condition of advanced cladding that contained Nb element was also investigated. Claddings were oxidized at given temperature and given time followed by water quenching. The results showed that ${\beta}$ phase which formed at quenching stage has an influence on cladding property. In case of advanced cladding, Nb retards cladding oxidation, thus enhances quenching resistance.

Solution-based fabrication of germanium sulphide doped with or without Li ions for solid electrolyte applications

  • Jin, Byeong Kyou;Cho, Yun Gu;Shin, Dong Wook;Choi, Yong Gyu
    • Journal of Ceramic Processing Research
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    • v.13 no.spc1
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    • pp.110-113
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    • 2012
  • Ge-S and Li-Ge-S powders were synthesized via solution-based process in order to employ chalcogenide-based solid electrolyte for use in Li secondary batteries. GeCl4 and thioacetamide in combination result in Ge-S powders of which major crystalline phase becomes GeS2 where the tetragonal and orthorhombic phases coexist after heat treatment. A chemical treatment using NaOH brings about the reduction of chlorine in the powders obtained. However, the heat treatment at 300 ℃ is more effective in minimizing the chlorine content. When lithium chloride is used as the precursor of Li ions, the LiCl powders are agglomerated with an inhomogeneous distribution. When Li2S is used, the Li-Ge-S powders are distributed more uniformly and the orthorhombic GeS2 phase dominates in the powders.