• 한국주조공학회지
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• 제21권1호
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• pp.24-32
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• 2001

Recently, iron aluminides based on Fe3Al and FeAl are ordered intermetallic alloys that offer good oxidation resistance, excellent sulfidation resistance, and potentially lower cost than many high-temperature structural materials. They have better strength, elasticity to weight ratio and high temperature strength, therefore, they can be cosidered as candidate heat resistance structural materials for automobiles, ships, airplanes and spaceships applications. The changes in the mechanical properties and fracture behavior were investigated for Fe-30at.%Al-5at.%Cr alloys when Ti, Hf and Zr were added respectively. For mechanical properties such as Rockwell hardness and yield strength at room temperature, those were decreased in the case of Fe-30at.%Al-5at.%Cr alloy then increased in the case of 5at.% and 10at.% addition of Ti alone. However, Rockwell hardness and yield strength decreased again at 15%Ti then increased dramatically due to the precipitation hardening of the second phase on the specimen at 20%Ti. For fracture modes, cleavage fracture showed in the case of Fe-30at.%Al and Fe-30at.%Al-5at.%Cr alloys. As the amount of Ti addition changed cleavage to transgranular fracture and to quasi-cleavage fracture at 20%Ti. When Hf, Zr and Hf+Zr were added respectively, transgranular, cleavage and quasi-cleavage fracture were coexisted.

• 대한기계학회논문집A
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• 제41권3호
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• pp.193-198
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• 2017

Alloy 617은 초고온가스로(VHTR)의 중간열교환기(IHX)의 유력한 후보 재료 중의 하나이다. $850^{\circ}C$의 고온에서 Alloy 617 용접재의 저사이클 피로 거동을 고찰하기 위하여, 완전 양진 변형률제어 피로시험이 0.6에서 1.5%의 전변형률범위에서 수행되었다. 용접재 시험편은 V-그루브 형상의 가스텅그스텐아크 용접한 용접 패드로부터 가공되었다. 피로수명은 전변형률범위가 증가할수록 감소하였다. 모든 실험조건에서 Alloy 617 용접재 시험편의 반복 응력 반응 거동은 초기 수 사이클에서 반복 변형률 경화현상을 나타내었다. 또한 모든 피로 균열의 발생과 전파는 입내파괴의 파손 모드를 보였다.

• 열처리공학회지
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• 제36권2호
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• pp.77-85
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• 2023

In this study, the mechanical properties of the Al-Mg-X (X=Cr, Si) alloy, which clearly showed the influence of the specimen and grain size, were investigated by changing the specimen size extensively. In addition, the effect on the specimen size, grain size and aging condition on the mechanical properties of the grain refining alloy according to the addition of Cr was clarified, and the relationship between these factors was studied. As the specimen size decreased, the yield stress decreased and the fracture elongation increased. This change was evident in alloys with coarse grain sizes. Through FEM analysis, it was confirmed that the plastic deformation was localized in the parallel part of specimen S2. Therefore, when designing a tensile specimen of plate material, the W/L balance should be considered along with the radius of curvature of the shoulder. In the case of under-aged materials of alloys with coarse grain size, the fracture pattern changed from intergranular fracture to transgranular fracture as W/d decreased, and δ increased. This is due to the decrease in the binding force between grains due to the decrease in W. In the specimen with W/d > 40 or more, intergranular fracture occurred, and local elongation did not appear. Under-aged materials of alloys with fine grain size always had transgranular fracture over a wide range of W/d = 70~400. As W/d decreased, δ increased, but the change was not as large as that of alloys with coarse grain sizes. Compared to the under-aged material, the peak-aged material did not show significant dependence on the specimen size of σ_0.2 and δ.

• 한국산업융합학회 논문집
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• 제26권6_2호
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• pp.1019-1024
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• 2023

Ceramic materials have excellent material properties such as stability at high temperatures, chemical stability, corrosion resistance, and wear resistance, so they are applicable even in extreme environments of high temperature and pressure. In particular, silicon carbide can be applied in the field of structural ceramics due to its characteristics of high strength, hardness, corrosion resistance, and heat resistance even at high temperatures. In this study, considering the application of silicon carbide materials to next-generation turbines, silicon carbide materials were manufactured using a liquid phase sintering method. When manufacturing liquid phase sintered silicon carbide, sintering additives were added to lower the sintering temperature and densify the material. In Al₂O₃-SiO₂, it was confirmed that the secondary product of the sintering additive was observed as a slightly dark area and was evenly distributed overall, and the fracture surface of Al₂O₃-SiO₂ was in the form of transgranular fracture in which cracks progressed along the crystal plane, and the flexural strength for Al₂O₃-SiO₂ was about 445.6 MPa.

• 한국재료학회지
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• 제14권1호
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• pp.35-40
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• 2004

In this study, dissolution characteristics of four types of commercial calcium phosphate ceramics were investigated in distilled water with respect to chemical composition and microstructure. For all samples, no significant damage was observed after 3 days of immersion. Following the 7 days of immersion, surface dissolution of the ceramics containing a crystalline phase susceptible to water such as TCP, even pure hydroxyapatite, was initiated at grain boundaries and the dissolution was extended interior to the material along the grain boundaries. In the considerably dissolved area, there was grain separation followed by the formation of 20 $\mu\textrm{m}$ of cavities. In at least one case, the residual pores on the surface appeared to initiate dissolution. In a dissolved area, a crack during the fracture propagates along the grain boundaries resulting in intergranular fracture, while transgranular fracture occurs in a dense area without significant dissolution.

• 한국결정성장학회:학술대회논문집
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• 한국결정성장학회 1997년도 Proceedings of the 12th KACG Technical Meeting and the 4th Korea-Japan EMGS (Electronic Materials Growth Symposium)
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• pp.19-22
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• 1997

The surface modificaion of alumina by $Al_2$O$_3$/SiC nanocomposite coating was studied in terms of processing and microstructure. A powder slurry of 5 vol% SiC composition was dipcoated onto presintered alumina bodies and pressurelessly sintered at 1$700^{\circ}C$ for 2 h in $N_2$. The used of organic binder and plasticizer in the slurry preparation, and the control of the density of presintered alumina body were found to be necessary to avoid cracking and warping during processing. The nanocomposite coating well bonded to the alumina body with thickness about 110 ${\mu}{\textrm}{m}$. The average grain size of coating (2 ${\mu}{\textrm}{m}$) was much finer than that of alumina body (13 ${\mu}{\textrm}{m}$). Fracture surface observations revealed mostly transgranular fracture for the coating, whereas intergranular fracture for the alumina body. Some pores (about 6%) were observed in the coating layer, although the alumina body showed fully dense microstructure.

• 한국안전학회지
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• 제14권2호
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• pp.3-10
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• 1999

Fatigue crack growth rates in commercial plate of high strength Al 7075-T651 were investigated for the T-L direction in air, water and sea water. In this paper the effect of cyclic load wave-form(trapezoid and triangle) on fatigue crack growth rates in air, water and sea water environments were investigated using standard LEFM testing procedures. It was founded that the fatigue crack growth behaviors were not affected by cyclic load wave-forms. In region II (stable crack growth region), the fatigue crack growth behaviors were insensitive to cyclic load wave-forms and were sensitive to environment i.e. fatigue crack growth behaviors were higher in sea water than in air for all cyclic load wave-form. The result of fractographical morphology in air, water and sea water by SEM showed obvious dimple rupture and typical striation in air, but transgranular fracture surface in water and sea water. The values m are not affected by corrosion environments but C are different values.

• 한국안전학회지
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• 제13권4호
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• pp.113-120
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• 1998

Fatigue crack growth rates(i.e. crack initiation and crack growth of short and long crack) are investigated using commercial plates of high strength Al alloy 7075-T651 for the transverse-longitudinal(T-L) direction in air, water and sea water. Also, the evaluation direct current potential drop(D.C.P.D) method and the fractographical analysis by SEM are carried out. Near threshold region, short crack growth rates were much faster than those of comparable long cracks, and these short crack growth rates actually decrease with increasing crack growth and eventually merge with long crack data. Fatigue crack propagation rates in aggressive media(i.e. sea water) increase noticeably over three times those in air. One of the most significant characters in this phenomenon as a corrosion-fatigue causes an acceleration in crack growth rates. Sea water environment, particularly Cl$^{[-10]}$ solution brings the most detrimental effects to aluminum alloy. The result of fractographical morphology in air, water and sea water by SEM shows obvious dimpled rupture and typical striation in air, but transgranular fracture surface in water and sea water.

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2002년도 Proceedings of the International Welding/Joining Conference-Korea
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• pp.273-275
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• 2002

The effect of post-weld heat treatment (PWHT) of marine structures steel was investigated at electrochemical viewpoint. In addition, slow strain rate test (SSRT) was carried out to investigate both electrochemical and mechanical properties by PWHT effect during impressed current cathodic protection. The optimum cathodic protection potential by SSRT was -770 mV(SCE). At the applied cathodic protection potential of -770 mV -850 mV(SCE), the fracture morphology was dimple pattern with ductile fracture, while it was transgranular pattern (Q.C: quasi cleavage) under -875 mV(SCE).

• Corrosion Science and Technology
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• 제6권3호
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• pp.140-146
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• 2007

In the paper, with corrosion velocity measurement and metallographic observation on specimens after sulfuric acid/ferric sulfate boiling experiment, intergranular corrosion tendency of the new type ultra low carbon stainless steel developed by ourselves which experienced solution treatment at different temperatures was evaluated. A VHX 500 super depth field tridimensional microscope was used to observe corrosion patterns on the sample surfaces. The depth and width of grain boundary corrosion groove were measured by the tridimensional microscope, which indicated that the corrosion degrees of the samples which received solution treatment at different temperatures are quite different. Transgranular corrosion at different degree occurred along with forged glide lines. After comparison it was proved that the stainless steel treated at $1100^{\circ}C$ performs very well against intergranular corrosion.