• 한국세라믹학회지
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• 제34권4호
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• pp.406-412
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• 1997

Al2O3/SiC hybrid-composite has been fabricated by the conventional powder process. The addition of $\alpha$-Al2O3 as seed particles in the transformation of ${\gamma}$-Al2O3 to $\alpha$-Al2O3 provided a homogeneity of the microstructure. The grain growth of Al2O3 are significantly surpressed by the addition of nano-size SiC particles. Dislocation were produced due to the difference of thermal expansion coefficient between Al2O3 and SiC and piled up on SiC particles in Al2O3 matrix, resulting in transgranular fracture. The high fracture strength of the composite was contributed to the grain refinement and the transgranular fracture mode. The addition of SiC platelets to Al2O3/SiC nano-composite decreased the fracture strength, but increased the fracture toughness. Coated SiC platelets with nitrides such as BN and Si3N4 enhanced fracture toughness much more than non-coated SiC platelets by enhancing crack deflection.

• 대한기계학회논문집
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• 제4권4호
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• pp.152-159
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• 1980

The temperature and the grain boundary precipitation have the great influence on the low-cycle fatigue behavior of austenite stainless steel at elevated temperature. For the purpose of investigating the mechanism concerning the change of fatigue micro crack mode in SUS 316 under various conditions low-cycle fatigue test was carried out at the elevated temperature 600.deg.C, plastic strain range 2% and constant strain rate .5c.p.m. A special attention is given to the observation of intergranular crack initiation. The results obtained are summarized as follows. The low-cycle fatigue behavior of SUS 316 at 600.deg.C is affected by transition of crack initiation mode from intergranular to transgranular. The transition is due to the aging effect, which is caused by grain boundary precipitations of Cr$\_$23/C$\_$6/. Since the intergranular crack initiation is brought about by the grain boundary sliding, the transgranular crack initiates in case that the strengthening of grain boundary due to the precipitation of Cr$\_$23/C$\_$6/ carbides takes place ahead of the intergranular crack initiation.

• 한국생산제조학회지
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• 제6권3호
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• pp.65-72
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• 1997

The horizontal corrosion fatigue tester has been developed for investigating environmental strength. Using this tester, we investigated about corrosion fatigue caracteristics for A106-Gr B steel weldments in 3.5% synthetic seawater and room temperature. Considered parameter is only frequency of 1, 3 and 5Hz.. and Corrosion fatigue crack length was measured by DC potential difference method. From the results, we could find that the horizontal corrosion fatigue tester could be well applied to estimation of fatigue strength. and, In case of 5Hz., corrosion fatigue crack growth pate of A106-Gr B steel weldment was transgranular, and of 1 and 3Hz. showed that transgranular and interfranular was mixed. Also, Material constants of corrosion fatigue crack growth estimated in each frequency were C=9.33$\times$$10^{-9}$ and m=2.93 in 1Hz., C=9.77$\times$$10^{-10}$ and m=3.47 in 3Hz., C=1.02$\times$$10^{-10}$ and m=4.05 in 5Hz

• 열처리공학회지
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• 제9권3호
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• pp.212-218
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• 1996

To clarify the influence of precipitation microstructure and inclusion on the monotonic tensile fracture behaviors in 2090 alloy aged at $180^{\circ}C$, the detailed measurement of hardness, tensile strength, elongation and the observation of scanning electron micrography, transmision electron micrography have been carried out. The transgranular shear ductile fracture has been observed in specimen quenched after solution treatment at $500^{\circ}C$ for 45min. While the under-aged specimen was fractured in both transgranular shear ductile and intergranular fracture mode, the fracture mode of peak-aged and over-aged alloy was predominantly intergranular fracture. The fracture behavior of each ageing condition was influenced by the change of precipitation microstructural features. In the case of peak-aged and over-aged alloys, the coarse and heterogeneous slip band caused by both shearable nature of the ${\delta}^{\prime}(Al_3Li)$ precipitates and PFZ along the high angle grain boundary aid the localization of deformation, resulting in low energy intergranular fracture. It was also estimated that the fractured T-type intermetallic phases (inclusion) and the equilibrium ${\delta}$(AlLi) phases which were formed at grain boundaries palyed an important role in promoting intergranular fracture mode.

• 연구논문집
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• 통권22호
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• pp.115-125
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• 1992

Mechanical properties and microstructure were investigated on vacuum induction melted $Fe_3A1$base alloys of $DO_3$ structure. Specal emphasis were put on the effect of alloy chemistry, grain size and process(rolling, directional solidification) on mechanical properties of Fe-22.5-39at.%Al at elevated temperature between room temperature and $800^{\circ}C$. grain size of as-cast alloys is refined by rolling from 1mm to $80\mum$. Tensile strength of Fe-24.lat.%AI was about 404MPa at the critical ordering temperature, and the fracture strain of the alloy was 1-2% at room temperature. An inverse temperature dependence of the strength is noticed as-cast $Fe_3A1$. The presence of Cr and Zr do not affect the room temperature ductility and high temperature strength. Fracture strain of directionally solidified(DS) $Fe_3A1$ is about 1%at room temperature, but is about 60%at. $T_C$(550^{\circ}C)$. Tensile strength of DS alloy is lower than that of as-cast alloy at $530^{\circ}C$ and $430^{\circ}C$. Failure mode at room temperature varies from transgranular fracture to intergranular fracture with the addition of Al. the failure mode also varies from mixed(transgranular+ intergranular) mode between room temperature and $500^{\circ}C$ to intergranular mode above $550^{\circ}C$

• Nuclear Engineering and Technology
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• 제17권3호
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• pp.193-199
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• 1985

지르칼로이-4 피복재의 요드에 의한 응력부식 균열 현상을 개량된 내부가압방법으로 조사하였다. 요드 응력부식 균열 현상을 일으키는 임계요드농도와 임계 응력이 존재하였으며, 603$^{\circ}$K의 시험 온도에서 임계요드 농도는 약 0.2mg/$\textrm{cm}^2$였고 임계 응력은 시험온도와 시편의 기계적 성질에 다라 변하였다. 파괴면을 주사전자 현미경으로 관찰한 결과, 초기 단계는 입내 파손 형태로 W-형의 균열을 포함하고 있었으며, 균열이 진행됨에 따라 입내 파손과 편성 파손이 혼합된 형태로 나타남을 알 수 있었다. 그리고 균열은 한 결정립에서 다른 결정립으로 단계적으로 전파되어 나갔다.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 1994년도 춘계학술대회 논문집
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• pp.167-174
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• 1994

The creep behavior and creep fracture of alumina at high temperature were investigated under four point flexural test. The steady-state creep behavior was observed at low bending stress and the primary creep until fracture was observed at high bending stress. The loading history of bending stress did not affect on the steady-stated creep rate. Intergranular fracture was dominant for fracture of alumina at room and high temperature. However, transgranular fracture was dominant on creep fracture of alumina under high temperature by nuclueation and growth of microcracks due to residual flaws or cavities in the material.

• 한국세라믹학회지
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• 제31권5호
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• pp.543-551
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• 1994

The creep behavior and creep fracture of sintered alumina at high temperature were investigated under four point flexural test. Steady-state creep behavior was observed at low bending stress and primary creep until fracture was observed at hish bending stress. The loading history of bending stress did not affect on steady-state creep rate. Intergranular fracture was dominant for fracture of alumina at room and high temperature. However, transgranular fracture was dominant on creep of alumina under high temperature by nucleation and growth of microcracks due to residual flaws or cavities in the material.

• 한국재료학회지
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• 제2권3호
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• pp.172-179
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• 1992

$Al_2O_3/ZrO_2$복합분말에 상릉분말을 침가하여 상압소결법으로 $Al_2O_3/ZrO_2$복합체를 제조한 후, 밀도, 강도, 경도 및 파괴인성등의 물성을 측정하였으며 미세구조 및 파괴단면도 관찰하였다. 상용분말의 침가량이 중량비로 50%이하인 경우에는 평균 꺽임 강도가 640 MPa정도로 거의 변화가 없었으며, 50%이상 첨가된 경우에는 강도가 저하되었는데, 이는 미세조직과 관계가 있는 것으로 생각된다. 또한 파괴인성(4.3-5.3 $Mpam^{1/2}$)값은 상용분말 첨가량에 비례하여 증가하였다. 파괴단면 관찰결과 파괴원인으로는 가공에서 생기는 표면 결함, $ZrO_2$ agglomeration에 의한 crack-like void 및 $Al_2O_3/ZrO_2$ nano복합체 분말과 상용분말간의 소결성 차이에서 생기는 계면 분리등이 관찰되었는데, nano 복합 분말만을 사용한 소결체에서는 가공에 의한 표면 결함만이 파괴원으로 작용하였다. 또한, 파괴형태는 주로 transgranular fracture이었다

• 한국세라믹학회지
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• 제44권4호
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• pp.208-213
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• 2007

Alumina/silver ($Al_2O_3/Ag$) nanocomposites with Ag content up to 9 vol% were prepared from nanopowder by soaking method using ${\gamma}-Al_2O_3$ of needle type and spark plasma sintering (SPS). The mechanical properties of specimens were investigated three-point flexural strength and toughness as a function of the Ag contents. The maximum flexural strength of the alumina/silver nanocomposite was 850 MPa for the 1 vol% composite, and also higher than monolith alumina as about 800 MPa at 3, 5, and 7 vol% Ag contents. Fracture toughness by single edged V-notch beam (SEVNB) was $4.05MPa{\cdot}m^{1/2}$ for the 3 vol% composite and maintained about $4.00MPa{\cdot}m^{1/2}$ at 5, and 7 vol% Ag content. Microstructure of fracture surface for each fracture specimens was observed. Due to the inhibition effect of alumina grain growth, the average grain size of nanocomposites depends on the content of Ag nano particles. The fracture morphology of nanocomposite with dislocation (sub-grain boundary) by silver nano-particles of second phases in the alumina matrix also showed transgranular fracture-mode compare with intergranular of monolith alumina. Thermal conductivity of specimens at room temperature was about 40 W/mK for the 1 vol% Ag content.