• 제목/요약/키워드: Total solid

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Gadolinium-doped Ceria/Magnesia (CGO/MgO) 복합체 전해질의 전기적 특성 분석 (Electrical Properties of Gadolinium-doped Ceria/Magnesia (CGO/MgO) Composite Electrolytes)

  • 조승환;;김도경
    • 한국재료학회지
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    • 제18권9호
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    • pp.470-474
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    • 2008
  • Composites of gadolinium-doped ceria/magnesia(CGO/MgO) were synthesized and characterized for the electrolytes of intermediate temperature solid oxide fuel cells. XRD and SEM results revealed that composite electrolytes consisted of their own phases after sintering at $1400^{\circ}C$ without noticeable solid solution of Mg into CGO. As the MgO content increased, the total electrical conductivity decreased, which might be attributed to the decrease of grain boundary conductivity, possibly due to the lowering of the continuity of the CGO grains and blocking effects of the insulating MgO phase. The space charge effect may not be a significant factor to affect the electrical conductivity of the CGO/MgO composites.

앨터네이터 로터폴의 단조가공에서 공전개선과 금형제작에 관한 연구 (A Study on the Manufacturing of Die and Improvement of Process in Fiorging Work of Alternator Rotor Pole)

  • 김세환
    • 한국공작기계학회:학술대회논문집
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    • 한국공작기계학회 1997년도 춘계학술대회 논문집
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    • pp.54-61
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    • 1997
  • Furthermore the rothor pole, with a solid type, manufactured by cold forging process at present should dmploy 3 press lines which consist of total 7 processes. Since A.S.B. treatment is prerequisite for the press line, the 3 times of A.S.B. treatment requires a long lead time, with little contribution to the reduction in cost. The author has investigated, through this researach, the possibility of a new forging method for a rotor pole production with (1) 2 pass instead of 3 press lines (2) only one A.S.B. treatment instead of 3 ones (3) solid type instead of sectional type, and (4) improvment of material property during process using a modified forging process and a specially designed die.

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시판된장의 리올로지(Rheology) 특성에 관한 연구 (Flow Properties of Doenjang)

  • 양신철;김선화
    • 한국관광식음료학회지:관광식음료경영연구
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    • 제13권1호
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    • pp.55-68
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    • 2002
  • Flow properties of doenjang samples at various total solid contents (30, 32, 34, 36, 38, 40%) were evaluated in this study. Flow properties of doenjang samples was determined by using Haake concentric cylinderical viscometer and Instron testing machine with capillary extrusion viscometer, and consistency index(K), and flow behavior index(n) was also determined from power models, and yield stress was derived form Casson models and vanes methods. Doenjang samples showed shear-thinning (pseudoplastic) fluid with small magnitude of flow behavior index(n) (n=0.30-0.55). Casson yield stress was from 2.11 to 64.02(Pa). Vane yield stress was more effective than casson yield stress in property of reactivation. Apparent viscosity was decreased with the increase in temperature and activation energy was in the range of 6.58 to 10.70 kJ/mole. From the capillary extrusion method, K and n was increased with the increase in solid content with good correlation with. The result revealed that capillary extrusion method is useful for measuring the flow properties of doenjang.

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Partial Conductivities, Nonstoichiometry and Defect Structure of a New Cathode Candidate $Y_{1-x}Ca_xFeO_{3-\delta}$

  • Kim, Chan-Soo;Yoo, Han-Ill
    • The Korean Journal of Ceramics
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    • 제4권2호
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    • pp.151-155
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    • 1998
  • The total electrical conductivity, ionic conductivity, and nonstoichimetry of a new cathode material $Y_{1-x}Ca_xFeO_{3-\delta}$ (x=0.1) were measured as functions of temperature ($900\leqT/^{\circ}C\leq1100$) and oxygen partial pressure $(10^{-6}\leqPo_2/atm\leq0.21$). Isothermal variations of these properties with $Po_2$ support that the majority type of ionic defects are anti-Frenkel disorder which, however, has seldom been considered for perovskite-based oxides. The results are discussed in comparison with those reported on similar oxides.

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Effect of Fermentation on the Antioxidant Activity of Rice Bran by Monascus pilosus KCCM60084

  • Cheng, Jinhua;Choi, Bong-Keun;Yang, Seung Hwan;Suh, Joo-Won
    • Journal of Applied Biological Chemistry
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    • 제59권1호
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    • pp.57-62
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    • 2016
  • In this study, we optimized fermentation conditions for the solid state fermentation of rice bran with Monascus pilosus KCCM60084, and the antioxidant activities were investigated. Optimal fermentation conditions were determined by the production of Monacolin K, a functional secondary metabolites with cholesterol lowering activity. The highest Monacolin K production were 2.88 mg/g observed on day 10 with 45% moisture content in the substrate when inoculated with 5% inoculum (w/w). Reducing power, iron chelating activity and $ABTS^+$ radical scavenging activity were significantly enhanced after fermentation by 60, 80, and 38% respectively. Furthermore, the content of total flavonoid were found to be increased by 4.58 fold. Based on these results, Monascus-fermented rice bran showed strong possibility to be used as a natural antioxidant agent due to its enhanced antioxidant activity.

표면 증발을 고려한 고체추진제의 연소율 해석 (Analysis of the Burning Rate of Solid Propellant Accounting for the Evaporation on the Surface)

  • 이창진
    • 한국추진공학회지
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    • 제3권1호
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    • pp.41-47
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    • 1999
  • 고체 추진제의 연소율(burning rate)은 연소의 동적 거동과 추진제의 성능을 판단할 수 있는 중요한 변수이다. 특히 AP계의 고체추진제 표면에서는 발열반응인 분해반응(decomposition) 이외에도 기체로 증발되는 증발반응(evaporation or sublimation)이 존재하므로 이를 고려한 연소 반응율의 해석은 매우 중요한 의미를 갖는다. 본 연구에서는 분해반응과 증발반응이 존재하며 외부로부터 고체추진제 표면으로 입사하는 복사열전달이 있는 경우, 응축영역에서 에너지 방정식과 화학 종 보존식을 사용하여 정상상태의 연소반응율에 관한 이론 해석을 수행하였다.

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MEMS 고체 추진제 추력기의 추진제실 설계와 구조체 가공 방법 (Design and Fabrication method of combustor for micro solid propellant thruster)

  • 이종광;권세진
    • 한국추진공학회:학술대회논문집
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    • 한국추진공학회 2006년도 제27회 추계학술대회논문집
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    • pp.251-254
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    • 2006
  • 마이크로 추력기는 마이크로/나노 위성체의 구현을 위한 핵심 기술이며 다양한 다이크로 추력기 중 마이크로 고체 추진제 추력기는 각광받고 있는 추력기중 하나이다. 마이크로 고체 추진제 추력기는 노즐, 점화기, 추진제실 그리고 추진제로 구성되어 있다. 본 논문에서는 다양한 마이크로 고체 추진제 추력기들을 조사하고, 1mNs의 임펄스를 구현할 수 있는 추력기 모델을 제시하고 연소실의 설계 및 제작 방법에 대한 결과를 보고하겠다.

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$Fe^{2+}$$Fe^{3+}$ 수산화물을 이용한 마그네타이트 합성 (Formation of Magnetite Using $Fe^{2+}$ and $Fe^{3+}$ Hydroxide)

  • 오재현;홍영호;박정훈;김만
    • 한국세라믹학회지
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    • 제31권11호
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    • pp.1346-1354
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    • 1994
  • In this study, the formation of magnetite using Fe(II) and Fe(III) hydroxides was investigated; The effects of hydroxide synthesizing pH and temperature, reaction temperature, and total water volume of hydroxide suspensions on the magnetite formation were studied. And the basic reaction behaviors of magnetite formation was discussed in the view of hydroxide formation reaction of Fe(II) and Fe(III) by titration. The characteristics of products were examined by TEM, VSM, XRD. From these experimental data, solid-solid reaction between Fe(II) and Fe(III) hydroxides is proposed as a new ferrite formation mechanism.

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S-자형 플랩을 이용한 충격파와 경계층 간섭현상 제어에 관한 연구 (Control of Shock Wave/Boundary-Layer Interactions Using S-Shaped Mesoflaps)

  • 이열
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2002년도 학술대회지
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    • pp.159-160
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    • 2002
  • New S-shaped aeroelastic mesoflaps are utilized to control normal shock/boundary-layer interactions. New generation of the mesoflaps is designed f3r a better rigidness and a good flow uniformity across the ulteractions. ,Major advantages of the mesoflap system can be a better total pressure recovery downstream of the interactions due to the lambda shock structure over the flap system, and a rehabilitation of the thickened boundary layer due to bleeding through a cavity underneath the flap system. Skin friction has been measured downstream of the interactions, using the laser interferometer skin friction (LISF) meter, which optically detects the rate of thinning of an oil film applied to the test surface. Various flap-thicknesses of the S-shaped mesoflap arrays are tested, and the results are compared to the solid-wall reference case. Overall, not much difference in the level of skin friction is noticed for the S-shaped flap arrays of various thicknesses, and its level is lower than the skin friction downstream of the solid-wall interaction

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Honeycomb Monolith Coated with Mo(VI)/ZrO2 as a Versatile Catalyst System for Liquid Phase Transesterification

  • Thimmaraju, N.;Pratap, S.R.;Senthilkumar, M.;Mohamed Shamshuddin, S.Z.
    • 대한화학회지
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    • 제56권5호
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    • pp.563-570
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    • 2012
  • Solid acid Mo(VI)/$ZrO_2$ with 2-10% Mo(VI) was coated on honeycomb monoliths by impregnation method. These catalytic materials were characterized by BET, $NH_3$-TPD/n-butylamine back titration, PXRD and SEM techniques. Phenyl salicylate (Salol) was synthesized via transesterification of methyl salicylate and phenol over these catalytic materials. An excellent yield (91.0%) of salol was obtained under specific reaction conditions. The effect of poisoning of acid sites of the catalytic material by adsorbing different bases and its effect on total surface acidity, powder XRD phases and catalytic activity was studied. A triangular correlation between the surface acidity, powder XRD phases and catalytic activity of Mo(VI)/$ZrO_2$ was observed. The thermally regenerated catalytic material was reused repeatedly with a consistent high yield of salol.