• Title/Summary/Keyword: Tolerance(공차)

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Preconcentration and Extraction of Copper on Activated Carbon Using 4-Amino-2, 3-dimethyl-1-phenyl-3-pyrazoline or 4-(4-methoxybenzylidenimin) thiophenole (4-Amino-2,3-dimethyl-1-phenyl-3-pyrazoline 또는 4-(4-Methoxybenzylidenimin)thiophenole을 이용한 활성탄에서의 구리의 예비 농축 및 추출)

  • Ghaedi, Mehrorang;Ahmadi, Farshid;Karimi, Hajir;Gharaghani, Shiva
    • Journal of the Korean Chemical Society
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    • v.50 no.1
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    • pp.23-31
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    • 2006
  • carbon modified methods were used for the preconcentration and determination of copper in some real samples using the flame atomic absorption spectrometry. The copper ions was adsorbed quantitatively on the activated carbon due to their complexation with 4- amino-2, 3-dimethyl-1-phenyl-3-pyrazoline (ADMPP) or 4-(4- methoxybenzylidenimin) thiophenole (MBITP). The adsorbed copper on solid phase was eluted quantitatively using small amount of nitric acid. The influence of important parameters including pH, amount of carrier, flow rate, amount of activated carbon and type and concentration of eluting agent for obtaining maximum recovery were investigated. The methods based on ADMPP and MBITP at optimum conditions is linear over concentration range of 0.05-1.5 g mL-1 and 0.05-1.2 g mL-1 of copper with correlation coefficient of 0.9997 and 0.9994 and both detection limit of 1.4 ng mL-1, respectively. The preconcentration leads to enrichment factor of 310 and break through volume of 1550 mL for both ligands. The method has a good tolerance limit of interfering ion and a selectivity that has been successfully applied for the determination of copper content in real sample such as tap, spring, river and waste water.

Optical Design of a Subminiature Catadioptric Omnidirectional Optical System with an LED Illumination System for a Capsule Endoscope (LED 조명계를 결합한 캡슐내시경용 초소형 반사굴절식 전방위 광학계의 설계)

  • Moon, Tae Sung;Jo, Jae Heung
    • Korean Journal of Optics and Photonics
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    • v.32 no.2
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    • pp.68-78
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    • 2021
  • A subminiature catadioptric omnidirectional optical system (SCOOS) with 2 mirrors, 6 plastic aspherical lenses, and an illumination system of 6 light emitting diodes, to observe the 360° panoramic image of the inner intestine, is optically designed and evaluated for a capsule endoscope. The total length, overall length, half field of view (HFOV), and F-number of the SCOOS are 14.3 mm, 8.93 mm, 51°~120°, and 3.5, respectively. The optical system has a complementary metal-oxide-semiconductor sensor with 0.1 megapixels, and an illumination system of 6 light-emitting diodes (LEDs) with 0.25 lm to illuminate on the 360° side view of the intestine along the optical axis. As a result, the spatial frequency at the modulation transfer function (MTF) of 0.3, the depth of focus, and the cumulative probability of tolerance at the Nyquist frequency of 44 lp/mm and MTF of 0.3 of the optimized optical system are obtained as 130 lp/mm, -0.097 mm to +0.076 mm, and 90.5%, respectively. Additionally, the simulated illuminance of the LED illumination system at the inner surface of the intestine within HFOV, at a distance of 15.0 mm from the optical axis, is from a minimum of 315 lx to a maximum of 725 lx, which is a sufficient illumination and visibility.

Optical Design of a Reflecting Omnidirectional Vision System for Long-wavelength Infrared Light (원적외선용 반사식 전방위 비전 시스템의 광학 설계)

  • Ju, Yun Jae;Jo, Jae Heung;Ryu, Jae Myung
    • Korean Journal of Optics and Photonics
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    • v.30 no.2
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    • pp.37-47
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    • 2019
  • A reflecting omnidirectional optical system with four spherical and aspherical mirrors, for use with long-wavelength infrared light (LWIR) for night surveillance, is proposed. It is designed to include a collecting pseudo-Cassegrain reflector and an imaging inverse pseudo-Cassegrain reflector, and the design process and performance analysis is reported in detail. The half-field of view (HFOV) and F-number of this optical system are $40-110^{\circ}$ and 1.56, respectively. To use the LWIR imaging, the size of the image must be similar to that of the microbolometer sensor for LWIR. As a result, the size of the image must be $5.9mm{\times}5.9mm$ if possible. The image size ratio for an HFOV range of $40^{\circ}$ to $110^{\circ}$ after optimizing the design is 48.86%. At a spatial frequency of 20 lp/mm when the HFOV is $110^{\circ}$, the modulation transfer function (MTF) for LWIR is 0.381. Additionally, the cumulative probability of tolerance for the LWIR at a spatial frequency of 20 lp/mm is 99.75%. As a result of athermalization analysis in the temperature range of $-32^{\circ}C$ to $+55^{\circ}C$, we find that the secondary mirror of the inverse pseudo-Cassegrain reflector can function as a compensator, to alleviate MTF degradation with rising temperature.

A Study on the Vibration Analysis of Spindle Housing with High Strength Aluminum of 2NC Head in Five-axis Cutting Machine Training (5축 절삭가공기 교육 중 2NC 헤드의 고강도 알루미늄을 적용한 스핀들 하우징의 극한 조건의 진동해석에 관한 연구)

  • Lee, Ji Woong
    • Journal of Practical Engineering Education
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    • v.14 no.1
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    • pp.119-125
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    • 2022
  • Materials used for education are materials such as SM20C, Al6061, and acrylic. SM20C materials are carbon steel and are often used in certification tests and functional competitions, but are also widely used in industrial sites. The Al6061 material is said to be a material that has lower hardness and stronger flexibility than carbon steel, so it is a material that generates a lot of compositional selection of tools. If students are taught practical training using acrylic materials, vibration occurs due to excessive cutting in some parts and damage to the tool occurs. In this process, we examine to what extent the impact on the 2NC head, which is a five-axis equipment, can affect precision control. The weakest part of the five-axis equipment can be said to be the weakest part of the head that controls the AC axis. When the accuracy and cumulative tolerance of this part occur, the accuracy of all products decreases. Therefore, the core part of the 2NC head, the spindle housing, was carried out using an Al7075 T6 (Alcoa, USA) material. In the process of vibration and cutting applied to this material, the analysis was conducted to find out the value applied to the finite element analysis under extreme conditions. It is hoped that this analysis data will help students see and understand the structure of 5-axis machining rather than 5-axis cutting.

Developing domestic flood resilience indicators and assessing applicability and significance (국내 홍수회복력 지표 개발과 적용성 및 중요도 평가)

  • Kim, Soohong;Jung, Kichul;Kang, Hyeongsik;Shin, Seoyoung;Kim, Jieun;Park, Daeryong
    • Journal of Korea Water Resources Association
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    • v.57 no.8
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    • pp.533-548
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    • 2024
  • Due to climate change with extreme weather events, occurrences of unprecedented heavy rainfall have become more frequent. Since it is difficult to perfectly predict and prevent flood damages, the limitation of traditional prevention-centered approaches has come a issue. The concept of "resilience" has therefore been developed which emphasizes the ability to swiftly recover from damages to previous states or to even better conditions. In this study, we 1) developed a total of 20 domestic flood resilience indicators based on the 4R principles (Redundancy, Robustness, Rapidity, Resourcefulness), 2) conducted applicability evaluations targeting specific disaster-prone areas, and 3) assessed the importance of each indicator through Analytic Hierarchy Process (AHP) analysis with flood-related experts. To confirm the suitability of the developed flood resilience indicators, multicollinearity analysis was performed, and the results indicated that all 20 indicators had tolerance limits above 0.1 and Variance Inflation Factors (VIF) below 10, demonstrating suitability as factors. Furthermore, evaluations of proposed indicators were carried out targeting disaster-prone areas in 2022(21 areas), and AHP analysis was utilized to determine the relative importance of each indicator. The analysis revealed that the importance of each indicator was as follows: Robustness 0.46, Rapidity 0.22, Redundancy 0.17, and Resourcefulness 0.16, with Robustness exhibiting the highest importance. Regarding the sub-indicators that had the greatest influence on each 4R component, river embankment maintenance emerged as the most influential for Robustness, healthcare services for Rapidity, fiscal autonomy of local governments for Resourcefulness, and drainage facilities for Redundancy.