• Title/Summary/Keyword: To-Tc method

Search Result 1,083, Processing Time 0.032 seconds

Fabrication Technology of High Tc Superconductor (초전도 나노 합성 기술)

  • Lee, Sang-Heon;Kim, Chan-Jung
    • Proceedings of the KIEE Conference
    • /
    • 2006.07c
    • /
    • pp.1335-1336
    • /
    • 2006
  • A high Tc superconducting with a nominal composition of YBCO wasprpared by the citarte method. The solid precursor produced by the dehydration of the gel at $120^{\circ}C$ for 12h is not in the amorphous state as expected but in a crystalline state. X-ray diffraction peaks of nearly the same angular position as the peaks of high Tc phase were observed in the precursor. After pyrolysis at $400^{\circ}C$ and calcination at $840^{\circ}C$ for 4h, the (001)peak of the high Tc phase was cleary observed. Experimental results suggest that the intermediate phase formed before the formation of the superconducting phase may be the most important factro in determining whether it is easy to form the high Tc phase or not, because the nucleation barriers of the two superconducting phase may be altered by the variation of the crystal structures of those intermediate phase.

  • PDF

Fabrication of High Tc Superconductor for Electric power transmission (열분해법에 의한 전력기기용 고온 초전도체의 합성)

  • Lee, Sang-Heon
    • Proceedings of the KIEE Conference
    • /
    • 2005.07c
    • /
    • pp.1962-1963
    • /
    • 2005
  • A high Tc superconducting with a nominal composition of $Bi_2Sr_2Ca_2Cu_3O_Y$ was Prepared by the citarte method. The solid Precursor produced by the dehydration of the gel at $120^{\circ}C$ for 12h is not in the amorphous state as expected but in a crystalline state. X-ray diffraction peaks of nearly the same angular position as the peaks of high Tc phase were observed in the precursor. After pyrolysis at $400^{\circ}C$ and calcination at $840^{\circ}C$ for 4h, the (001)peak of the high Tc phase was cleary observed. Experimental results suggest that the intermediate phase formed before the formation of the superconducting phase may be the most important factro in determining whether it is easy to form the high Tc phase or not, because the nucleation barriers of the two superconducting phase may be altered by the variation of the crystal structures of those intermediate phase.

  • PDF

Fabrication of BSCCO High Tc Superconducting Precursor (BSCCO 초전도 전구체의 합성)

  • Lee, Sang-Heon;Lee, Young-Hie
    • Proceedings of the KIEE Conference
    • /
    • 2005.07c
    • /
    • pp.1964-1965
    • /
    • 2005
  • A high Tc superconducting with a nominal composition of $Bi_2Sr_2Ca_2Cu_3O_Y$ was prepared by the citarte method. The solid precursor produced by the dehydration of the gel at $120^{\circ}C$ for 12h is not in the amorphous state as expected but in a crystalline state. X-ray diffraction peaks of nearly the same angular position as the peaks of high Tc phase were observed in the precursor. After pyrolysis at $400^{\circ}C$ and calcination at $840^{\circ}C$ for 4h, the (001)peak of the high Tc phase was cleary observed. Experimental results suggest that the intermediate phase formed before the formation of the superconducting phase may be the most important factro in determining whether it is easy to form the high Tc phase or not, because the nucleation barriers of the two superconducting phase may be altered by the variation of the crystal structures of those intermediate phase.

  • PDF

Fabrication of BSCCO High Tc Superconducting Precursor (BSCCO 초전도 전구체의 합성)

  • Lee, Sang-Heon
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 2005.07a
    • /
    • pp.290-291
    • /
    • 2005
  • A high Tc superconducting with a nominal composition of $Bi_2Sr_2Ca_2Cu_3O_Y$ was prepared by the citarte method. The solid precursor produced by the dehydration of the gel at $120^{\circ}C$ for 12h is not in the amorphous state as expected but in a crystalline state. X-ray diffraction peaks of nearly the same angular position as the peaks of high Tc phase were observed in the precursor. After pyrolysis at $400^{\circ}C$ and calcination at $840^{\circ}C$ for 4h. the (001)peak of the high Tc phase was cleary observed. Experimental results suggest that the intermediate phase formed before the formation of the superconducting phase may be the most important factor in determining whether it is easy to form the high Tc phase or not. because the nucleation barriers of the two superconducting phase may be altered by the variation of the crystal structures of those intermediate phase.

  • PDF

Fabrication of High Tc Superconductor Using Thermal Pyrolysis (열분해법에 의한 고온 초전도 합성)

  • Lee, Sang-Heon
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 2006.06a
    • /
    • pp.85-86
    • /
    • 2006
  • A high Tc superconducting with a nominal composition of $Bi_2Sr_2Ca_2Cu_3O_y$ was prepared by the citarte method. The solid precursor produced by the dehydration of the gel at $120^{\circ}C$ for 12h is not in the amorphous state as expected but in a crystalline state. X-ray diffraction peaks of nearly the same angular position as the peaks of high Tc phase were observed in the precursor. After pyrolysis at $400^{\circ}C$ and calcination at $840^{\circ}C$ for 4h, the (001)peak of the high Tc phase was cleary observed. Experimental results suggest that the intermediate phase formed before the formation of the superconducting phase may be the most important factro in determining whether it is easy to form the high Tc phase or not, because the nucleation barriers of the two superconducting phase may be altered by the variation of the crystal structures of those intermediate phase.

  • PDF

Labeling Efficiency of $^{99m}Tc$-Labeled RBC Due to Labeling Time Change (표지시간 변화에 의한 $^{99m}Tc$과 적혈구 표지효율)

  • Dong, Kyeong-Rae;Kim, Ho-Seong;Choi, Seong-Kwan
    • Journal of radiological science and technology
    • /
    • v.30 no.3
    • /
    • pp.259-263
    • /
    • 2007
  • For the preparation of $^{99m}Tc$-labeled RBC, $10{\sim}20\;{\mu}g/kg$ of Stannous(II) chloride and $10{\sim}40\;min$ of preparation was used. For finding out the effect of contrast agent, the blood samples were collected in three days, seven days, and 1 months after the diagnostic procedure. In the normal volunteer, the concentration of reducing agent and preparation time did not effect on the radiochemical yield. But in the patients, 10 mg of Stannous(II) chloride and 60 min incubation times was shown high radiochemical yield. Contrast agent has a significant effect on the radiochemical yield. Although the blood samples which were collected after seven days of diagnostic procedure did not effect on the radiochemical yield of $^{99m}Tc$-labeled RBC, but the radiochemical yield of $^{99m}Tc$-labeled RBC which was prepared with a sample of high concentration of contrast agent in blood led to low radiochemical yield. For these samples, the modified method showed high radiochemical yield than previous in vivo preparation method. The recommended method is followed. Blood collecting was performed at 30 minutes after injection of reducing agent, and it is centrifuged for removal of plasma. After addition of $^{99m}TcO^-_4$, sample reservoir was rotated. After addition of normal saline, and it is centrifuged for separation of saline. Then $^{99m}Tc$-labeled RBC was obtained after removal of saline.

  • PDF

Comparative analysis of Glomerular Filtration Rate measurement and estimated glomerular filtration rate using 99mTc-DTPA in kidney transplant donors. (신장이식 공여자에서 99mTc-DTPA를 이용한 Glomerular Filtration Rate 측정과 추정사구체여과율의 비교분석)

  • Cheon, Jun Hong;Yoo, Nam Ho;Lee, Sun Ho
    • The Korean Journal of Nuclear Medicine Technology
    • /
    • v.25 no.2
    • /
    • pp.35-40
    • /
    • 2021
  • Purpose Glomerular filtration rate(GFR) is an important indicator for the diagnosis, treatment, and follow-up of kidney disease and is also used by healthy individuals for drug use and evaluating kidney function in donors. The gold standard method of the GFR test is to measure by continuously injecting the inulin which is extrinsic marker, but it takes a long time and the test method is complicated. so, the method of measuring the serum concentration of creatinine is used. Estimated glomerular filtration rate (eGFR) is used instead. However, creatinine is known to be affected by age, gender, muscle mass, etc. eGFR formulas that are currently used include the Cockroft-Gault formula, the modification of diet in renal disease (MDRD) formula, and the chronic kidney disease epidemilogy collaboration (CKD-EPI) formula for adults. For children, the Schwartz formula is used. Measurement of GFR using 51Cr-EDTA (diethylenetriamine tetraacetic acid), 99mTc-DTPA (diethylenetriamine pentaacetic acid) can replace inulin and is currently in use. Therefore, We compared the GFR measured using 99mTc-DTPA with the eGFR using CKD-EPI formula. Materials and Methods For 200 kidney transplant donors who visited Asan medical center.(96 males, 104 females, 47.3 years ± 12.7 years old) GFR was measured using plasma(Two-plasma-sample-method, TPSM) obtained by intravenous administration of 99mTc-DTPA(0.5mCi, 18.5 MBq). eGFR was derived using CKD-EPI formula based on serum creatinine concentration. Results GFR average measured using 99mTc-DTPA for 200 kidney transplant donors is 97.27±19.46(ml/min/1.73m2), and the eGFR average value using the CKD-EPI formula is 96.84±17.74(ml/min/1.73m2), The concentration of serum creatinine is 0.84±0.39(mg/dL). Regression formula of 99mTc-DTPA GFR for serum creatinine-based eGFR was Y = 0.5073X + 48.186, and the correlation coefficient was 0.698 (P<0.01). Difference (%) was 1.52±18.28. Conclusion The correlation coefficient between the 99mTc-DTPA and the eGFR derived on serum creatinine concentration was confirmed to be moderate. This is estimated that eGFR is affected by external factors such as age, gender, and muscle mass and use of formulas made for kidney disease patients. By using 99mTc-DTPA, we can provide reliable GFR results, which is used for diagnosis, treatment and observation of kidney disease, and kidney evaluation of kidney transplant patients.

Development of the Fabrication Technology of High Tc Superconductor for Electrical Energy Storage (전기 에너지 저장을 위한 초전도 나노 합성 기술)

  • Lee, Sang-Heon
    • The Transactions of the Korean Institute of Electrical Engineers C
    • /
    • v.55 no.9
    • /
    • pp.442-445
    • /
    • 2006
  • In order to realize the commercial application of HTSC materials, it is necessary to develop the fabrication process of high Tc oxide superconductor materials with desired shape and for practical application and high critical current density as well as good mechanical strength which can withstand high lorenz force generated at high magnetic field. Much studies have been concentrated to develop the fabrication technique for high critical current density but still there are a lot of gap which should be overcome for large scale application of HTSC materials at liquid nitrogen temperature. Recently some new fabrication techniques have been developed for YBaCuO bulk superconductor with high mechanical strength and critical current density. In this project, the establishment of fabrication condition and additive effects of second elements were examined so as to improve the related properties to the practical use of YBaCuO superconductor, and we reported the production of the YBaCuO high Tc superconductor by the pyrolysis method.

Analysis of Cell Stream Scheme and Service Transmission using Time-Stamp Method in the Wireless ATM (무선 ATM에서 타임스탬프 방식을 이용한 셀 스트림 구조와 서비스전송 해석)

  • Kim, Jeong-Ho
    • The Transactions of the Korea Information Processing Society
    • /
    • v.6 no.8
    • /
    • pp.2179-2187
    • /
    • 1999
  • To privide multimedia mobile communication services for the users in scattered locations, the application ATM cells efficiently in wireless communications, it is effective to the use TDMA method. However, it is necessary to have methods to compensate the CDV(cell delay variation) caused by the difference between TDMA-ATM and cell stream multiplexing of the users. This paper optimizes the cell control time(Tc) when VBR traffic inputs have MMPP by applying CDV characteristics of time stamp method, which has the most advantages among compensation methods of CDV. This paper suggests a cell stream multiplex method employing time stamp techniques to reduce CDV for wireless suggest method shows that CDV distribution and cell stream multiples rangd can be controlled to 1.2${\times}$Tc which reduced over the VBR service in the TDMA-WATM transmission. This paper also presents evaluation of the suggested architecture obtained simulation.

  • PDF

Characteristics of a Planar Multijunction Thermal Converter (평면형 다중접합 열전변환기의 특성)

  • Jo, Hyeon-Deok;Kim, Jin-Seop;Lee, Jong-Hyeon;Lee, Jeong-Hui;Park, Se-Il;Gwon, Seong-Won
    • Journal of the Institute of Electronics Engineers of Korea SD
    • /
    • v.38 no.10
    • /
    • pp.699-705
    • /
    • 2001
  • Six types of planar thermal converters from TC 1 to TC 6 were designed and fabricated for the purpose of being used as practical standards to alternating current. The respective voltage responses in air and in a vacuum of TC 6, which has the smallest thermal loss, were about 4.03mV/mW and about 6.38 mV/mW. Thermal time constant of TC 6, which has also the smallest heater thermal inertia, was about 8 ms. The respective variations of AC-DC voltage and current transfer errors from sample to sample, which were measured by FRDC(fast reversed DC) method, were about $\pm$0.41 ~$\pm$0.85 ppm and about $\pm$0.15~$\pm$1.16 ppm in the frequent range of 40 Hz~10 KHz with appling 1 V and 5 mA rms sine waves to the converters. All converters investigated exhibited sufficiently low AC-DC transfer errors to be used as practical standards.

  • PDF