• Journal of Pharmaceutical Investigation
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• 제12권4호
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• pp.112-125
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• 1982

Sulfamethoxazole particles were microencapsulated using the gelatin-acacia complex coacervation method. Micromeritic properties and dissolution characteristics of the microcapsules were studied. The particle size distribution followed log-normal form. As the hardening time increased, the particle size and wall thickness increased ($45.3-52.0\;{\mu}m$, $2.02-5.12\;{\mu}m$, respectively). This is considered to be due to the cross-linked wall structure of formalized microcapsules which prevents shrinking of gelatin during the dehydration and drying processes. An increase of hardening time clearly delayed the release rate. The in vitro 50% dissolution time $(t_{50})$ for unencapsulated sulfamethoxazole powder was less than 3 min.; for microcapsules hardened for 30 min, the $t_{50}$ was 20.1 min.; for those hardened for 60 min. the $t_{50}$ was 25.0 min.; for those hardened for 120 min., the $t_{50}$ was 35.8 min. The surface of the unhardened microcapsules was smooth and had no cracking or pore penetration. However, the surface of the hardened microcapsules was folded and invaginated.

• 열처리공학회지
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• 제3권2호
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• pp.10-19
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• 1990

The tempering behavoirs of 0.45% carbon steel treated by automatic progressive high frequency induction hardening equipment have been investigated. In order to examine the correlation of hardness with both tempering temperature and time, simple regression analysis has been made using the statistical quality control package. The maximum surface hardness value of induction hardened zone and its effective hardening depth have been determined to be Hv 810 and 0.76mm, respectively. The hardness obtained after tempering has been shown to vary lineary with tempering time at six different temperatures. The activation energies during tempering have been calculated to be 25.34kcal/mole, 32.73kcal/mole and 49.24kcal/mole for HRcs 60, 50 and 40, respectively, showing that tempering process occurs by a complex mechanism, The tempering hardness equation of $H=90.113{\sim}4.531{\times}10^{-3}$ [T(11.996+log t)] has proved to be in a reasonably good agreement with experimently determined data and it is also expected to be useful for the determination of tempering treatment conditions to obtain a required hardness value.

• 한국농공학회:학술대회논문집
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• 한국농공학회 2005년도 학술발표논문집
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• pp.117-122
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• 2005

Prepacked polymer mortar that is mainly composed of MMA monomer and used for the patching and restoring materials of concrete structures was developed, and its hardening and strength properties were experimentally surveyed. Results of study show that the permeance of binder into the aggregate was excellent for the case of PMMA mixing ratio of below 10%, the surface hardening inferiority was not generated for the case of the ratio of over 5%. Working time of the prepacked polymer mortar and hardening shrinkage tended to decrease as the PMMA mixing ratio increased. On the other hand, the ratio turned out not to decisively affect on compressive and flexural strengths. Regardless of PMMA mixing content, the adhesive strength was about 2.5 MPa. Occurring the desquamation on the substrate of cement concrete showed the adhesive strength of MMA prepact polymer mortar was excellent.

• 열처리공학회지
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• 제24권4호
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• pp.193-198
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• 2011

Effect of CaO addition on age hardening response has been studied by using optical microscopy, scanning electron microscopy and differential thermal analysis in AZ91 and CaO-containing ECO-AZ91 alloys. After solution treatment, the ${\beta}$($Mg_{17}Al_{12}$) phase formed during solidification mostly disappeared in the microstructure in the AZ91 alloy, whereas numerous ${\beta}$ precipitates containing Ca were still observed in the ECO-AZ91 alloy due to its enhanced thermal stability. The ECO-AZ91 alloy showed the delayed peak aging time and higher peak hardness compared with those of the AZ91 alloy. The activation energies for ${\beta}$ precipitation calculated by means of Kissinger method increased from 71.4 to 85.6 kJ/mole by the addition of CaO, which implies that CaO plays a role in reducing ${\beta}$ precipitation rate in the AZ91 alloy.

• 한국전산구조공학회:학술대회논문집
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• 한국전산구조공학회 1998년도 가을 학술발표회 논문집
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• pp.92-98
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• 1998

Nonlinear finite element analyses of one dimensional consolidation problem were performed using an anisotropic hardening constitutive model. For the analyses, the anisotropic hardening elasto-plastic constitutive model based on the generalized isotropic hardening(GIH) rule was implemented into a nonlinear finite element analysis program, PLASTIC. In order to preserve the accuracy of the finite element solution for nonlinear problems, an implicit stress integration algorithm was employed. A consistent tangent moduli could also ensure the quadratic convergence of Newton's method. As a result, the nonlinear solution was accurately calculated and was converged to be asymptotically quadratic. In a consolidation problem, the relationship between load and settlement and between settlement and time vertical was analyzed comparing with results using the Cam-clay type model and the final consolidation settlement and the duration of primary consolidation could be evaluated rigorously using the GIH constitutive model.

• 한국정밀공학회지
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• 제22권11호
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• pp.51-58
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• 2005

Laser surface hardening technologies have been used to improve characteristics of wear and to enhance the fatigue resistance for automotive parts. The objective of this research work is to investigate the influence of the process parameters, such as power of laser and defocused spot position, on the characteristics of laser heat treatment for the case of SM45C medium carbon steel. CW Nd:YAG laser is selected as the heat source. The optical lens with the elliptical profile is designed to obtain a wide heat treatment area with a uniform hardness. From the results of the experiments, it has been shown that the maximum hardness is approximatly 780 Hv when the power and the travel speed of laser are 1,095 W and 0.6 m/min, respectively. In addition, the hardening width using the elliptical lens was three time larger than that using the defocusing of laser beam.

• 한국재료학회지
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• 제23권3호
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• pp.199-205
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• 2013

The mechanical properties and microstructures of aluminum-matrix composites fabricated by the dispersion of fine alumina particles less than $20{\mu}m$ in size into 6061 aluminum alloys are investigated in this study. In the as-quenched state, the yield stress of the composite is 40~85 MPa higher than that of the 6061 alloy. This difference is attributed to the high density of dislocations within the matrix introduced due to the difference in the thermal expansion coefficients between the matrix and the reinforcement. The difference in the yield stress between the composite and the 6061 alloy decreases with the aging time and the age-hardening curves of both materials show a similar trend. At room temperature, the strain-hardening rate of the composite is higher than that of the 6061 alloy, most likely because the distribution of reinforcements enhances the dislocation density during deformation. Both the yield stress and the strain-hardening rate of the T6-treated composite decrease as the testing temperature increases, and the rate of decrease is faster in the composite than in the 6061 alloy. Under creep conditions, the stress exponents of the T6-treated composite vary from 8.3 at 473 K to 4.8 at 623 K. These exponents are larger than those of the 6061 matrix alloy.

• 대한금속재료학회지
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• 제48권12호
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• pp.1103-1108
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• 2010

We fabricated flanged outer races for wheel bearing units using 0.52%C clean steels, and then characterized and studied the transformation behavior. The outer races produced by hot forging and high frequency induction hardening in this study were analyzed through microstructural characterization using OM, SEM, TEM, and X-ray diffractometer and their microhardness depth profiles of the raceway contacted by balls were measured using MVH tester. The surface hardened layers with a uniform hardness profile in the raceway consisting of very fine martensite with sub-micron sized retained austenite could be formed for very short time during high frequency induction hardening after hot forging. The very fine martensite may be transformed on rapid cooling, from the inhomogeneous austenite nucleated on rapid heating in small particles of pearlitic cementite fragmentated by hot forging. On the other hand the sub-micron sized retained austenite may be chemically stabilized due to their extremely small size, from the small austenite nucleated at the grain boundaries.

• Restorative Dentistry and Endodontics
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• 제17권2호
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• pp.331-341
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• 1992

The purpose of this study was to measure the polymerization contraction stress of two types of composite resins; chemical cured type(Cliarfil F II, Kuraray, Japan) and photo-cured type(Photo-Clearfil Bright, Kuraray, Japan). The stresses of composite resin by contraction measured with specially designed measuring device(Fig. 1). The stresses caused by shrinkage during hardening of specimens were measured according to the type of composite resins, thickness of specimen(0.65, 1.30 and 1.95mm), and ratio of catalyst to base in case of only chemical cured composite resin(0.5, 1.0 and 1.5). As the composite resin specimen shrank on hardening, the load cell recorded force vs time automatically on pen-recorder(Toa, Japan) with a cross-head speed 60mm/hr at 0~10 voltages up to 2 hours. The experiments were conducted in a room maintained at $23{\pm}2^{\circ}C$ and relative humidity $50{\pm}10%$. The results were as follows. 1. The contraction stress during hardening was higher in photo cured composite resin than in chemical cured composite resin. 2. The contraction stress during hardening was increased with thickness of composite resin specimen. 3. In chemical cured composite resin, the polymerization contraction stress was decreased with ratio of catalyst and base. 4. The contraction stress during polymerization was higher in early time after insertion of photo cured composite resin and chemical cured composite resin.

• 한국작물학회지
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• 제39권3호
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• pp.205-210
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• 1994

최근 담수직파 재배양식중 승용형 골뿌림 파종기를 이용하여 파종골을 작성, 이와 동시에 종자를 파종하고, 생육기간동안 골이 자연적으로 매몰됨으로서 도체가 지지력을 가져 직파재배시 단점중의 하나인 도복을 경감시킬 수 있다는데 근거를 두고 시험연구가 급속히 진행되고 있는 무논 골 뿌림 재배법 확립의 일환으로, 먼저 초기 입묘와 밀접한 관계가 있는 파종전 토양굳힘정도, 파종 골 깊이, 그리고 파종후 담수시기 구명을 위하여 시험한 결과는 아래와 같다. 1. 파종전 토양의 굳힘정도는 파종시 종자의 매몰정도, 파종후 담수시 종자 부유상태 및 생육기간동안 골 매몰로 인한 줄기매몰심도등을 고려할때 경운정지후 낙수하여 3일정도 굳힌상태 즉, 115g의 원추관입심이 6~7cm정도인 상태가 적절하였다. 2. 파종골 깊이별 최고 분얼기에 조사한 토양매몰정도는 4~6cm심도의 경우 3~4cm정도의 토양매몰이 이루어졌으며, 입묘율은 골 깊이가 깊을수록 떨어지는 경향이었다. 표면조파(0cm)의 경우 부묘가 발생되었으며, 골 깊이별 뿌리 분포비율은 파종심도가 낮을수록 표층의 뿌리 분포 비율이 높고, 도복정도 역시 8 정도로 매우 높아서, 줄기 매몰심도 및 도복정도 그리고 수량성으로 볼때 파종골 깊이는 4cm정도가 적당하였다. 3. 파종후 담수시기가 늦어질수록 입묘율이 떨어졌으며, $m^2$ 당수수의 확보 역시 적어서 담수시기는 파종직후 담수가 바람직 하였다.