• Analytical Science and Technology
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• v.24 no.3
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• pp.231-235
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• 2011

A spectrofluorimetric method for the determination of EDTA in real samples such as mayonnaise, powder detergent and cleansing cream with tiron (4,5-dihydroxy-1,3-benzenedisulfonic acid) as a fluorimetric reporter was developed. When tiron is chelated with Cu(II), the fluorescent intensity is decreased by a quenching effect. However, when Cu(II)-tiron chelate reacts with EDTA, fluorescent intensity is increased as tiron is released. Several experimental conditions such as pH of the sample solution, the amount of Cu(II), the amount of tiron, heating temperature and heating time were optimized. Fe(III) interfered more seriously than any other ions, interference of Fe(III) could be disregarded, because Fe(III) was scarcely contained in selected real samples. The linear range of EDTA was from $8.0{\times}106{-8}\;M$ to $2.0{\times}10^{-6}\;M$. With this proposed method, the detection limit of Fe(III) was $5.2{\times}10^{-8}\;M$. Recovery yields of 92.7~99.3% were obtained. Based on experimental results, it is proposed that this technique can be applied to the practical determination of EDTA.

• Journal of the Korean Electrochemical Society
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• v.3 no.4
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• pp.232-234
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• 2000

Determination of uric acid by electrochemical method using ultrasonic stimulation has been investigated. Effects of sonication power, sonication time, pH of the solution and temperature were studied to obtain the optimal analytical conditions. The stability of the electrode was also examined. The optimal conditions for the sonovoltammetric determination of uric acid were as follows: temperature, $25.0^{\circ}C$ pH 7.0; sonication power, $20W/cm^2$. The calibration curve for the determination of uric acid by sono-LSV was linear over the range of$8.0{\times}10^{-6}\~5.0\times10^{-4}M$ and the limit of detection was $6.5\times10^{-6}M$.

• KSII Transactions on Internet and Information Systems (TIIS)
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• v.10 no.10
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• pp.4933-4956
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• 2016

Use-After-Free (UAF) is a common lethal form of software vulnerability. By using tools such as Web Browser Fuzzing, a large amount of samples containing UAF vulnerabilities can be generated. To evaluate the threat level of vulnerability or to patch the vulnerabilities, automatic deduplication and exploitability determination should be carried out for these samples. There are some problems existing in current methods, including inadequate pertinence, lack of depth and precision of analysis, high time cost, and low accuracy. In this paper, in terms of key dangling pointer and crash context, we analyze four properties of similar samples of UAF vulnerability, explore the method of extracting and calculate clustering eigenvalues from these samples, perform clustering by fast search and find of density peaks on a large number of vulnerability samples. Samples were divided into different UAF vulnerability categories according to the clustering results, and the exploitability of these UAF vulnerabilities was determined by observing the shape of class cluster. Experimental results showed that the approach was applicable to the deduplication and exploitability determination of a large amount of UAF vulnerability samples, with high accuracy and low performance cost.

• Bulletin of the Korean Chemical Society
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• v.17 no.11
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• pp.995-999
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• 1996

A method for the determination of cobalt(Ⅱ) by differential pulse voltammetry using a carbon paste electrode constructed by incorporating 1-(2-pyridylazo)-2-naphthol(PAN) into a conventional carbon paste mixture composed of graphite powder and Nujol oil has been developed. Several influencing factors for the determination of cobalt(Ⅱ) were studied in detail and the optimum analytical conditions were found to be as follows: pH, 4.6; composition of electrode, 20%; temperature of deposition, 43 ℃; time of preconcentration, 15 min. Regeneration of the electrode surface for the continuous uses of the electrode was achieved by exposing the carbon paste electrode to an acidic solution. Response of the electrode was reproducible for the uses of five times and the relative standard deviations were 6.7 and 4.6% for 2.0×10-5 M and 4.0×10-6 M cobalt(Ⅱ), respectively. The calibration curve for cobalt(Ⅱ) obtained by differential pulse voltammetry was divided into two linear ranges of 1.7× 10-6-1.3×10-4 M and 2.0×10-7-8.0×10-7 M. The detection limit was estimated to be 1.3×10-7 M. The effects of coexisting ions were also investigated to test the applicability of the proposed method to the determination of cobalt(Ⅱ) in real samples.

• Korean Journal of Soil Science and Fertilizer
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• v.43 no.6
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• pp.1008-1011
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• 2010

A method currently used to determine soil organic matter (SOM), Tyurin method, is time consuming and expensive while accurate. Recently, a spectrophotometric determination was reported to be rapid, accurate, stable, easy to execute, and amendable to field use for soil samples obtained from Texas, USA. The objective of this study was to test if the spectrophotometric method is applicable to soils in Korea. Soil organic matter was extracted by 1 M HCl followed by a 0.25 M NaOH-0.1 M sodium pyrophosphate solution at a ratio of 1:250 soil:extractant. Soil organic matter determined by Tyurin method was linearly related to the value based on absorbance at 300 nm of the soil extracts with a coefficient of determination ($r^2$) of 0.81. Therefore, the result imply that this spectrophotometric method can be used to determine the soil organic matter of agricultural soils in Korea.

• Journal of Korean Society of Transportation
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• v.26 no.4
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• pp.217-227
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• 2008

The purpose of this research is the estimation of a transfer ratio according to transfer time reflecting passenger attributes such as sex, age, income, job, the car ownership, and other variables with the assumption that a transfer ratio would be different depending on each passenger attribute. This research tested transfer time through a question-survey, estimated transfer time according to the passenger attributes using a data sample, and presented some applicable models about marginal transfer time for the case of the determination of transfer ratios according to transfer time. In this research the sample which had been surveyed for passengers walking to access a transfer station was used to test and estimate and the question was present walking time to the transfer time and the marginal transfer walking time.

• Proceedings of the Korean Society for Agricultural Machinery Conference
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• 2000.02a
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• pp.457-463
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• 2000

• Proceedings of the Korean Society for Agricultural Machinery Conference
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• 1998.12a
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• pp.368-373
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• 1998

• Bulletin of the Korean Space Science Society
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• 2004.10b
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• pp.59-59
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• 2004

• Bulletin of the Korean Chemical Society
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• v.23 no.12
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• pp.1816-1818
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• 2002