• 제목/요약/키워드: Ti(CN)

검색결과 121건 처리시간 0.023초

PECVD 에 의해 형성된 TiCN 박막의 형상 및 밀착성 (The Morphology and Adhesion of TiCN Film formed by PECVD)

  • 허정;남태운
    • 열처리공학회지
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    • 제15권3호
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    • pp.118-126
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    • 2002
  • TiCN thin films were deposited on tool steels at $510^{\circ}C$ by PECVD from a $TiCl_4+N_2+CH_4+H_2+Ar$ gaseous mixture. The microstructures and preferred orientation were investigated. The micro-scratch tests were performed using a system equipped with an acoustic emission sensor. Critical loads were determined to evaluate the adhesion of TiCN to substrate. The influences of the microstructures of substrates, double layered coatings, and coatings after nitriding(duplex coating) were investigated. The experimental results showed that the microstructures of substrates and double layered coating did not affect the critical loads considerably. By the duplex coating, critical loads were not always increased. In some cases, duplex coatings decreased critical loads significantly despite of absence of black layer. In this study, we tried to relate the results of scratch test to the residual stress analysis. Nitriding before the coating reduces the tensile residual stress in the film, which gives rise to low critical load in scratch test.

Effect of $Mo_2C$ Content on the Microstructure and Properties of Ti(CN)-$Mo_2C$ Ceramics

  • Park, Dong-Soo;Lee, Yang-Doo;Taejoo Jung
    • The Korean Journal of Ceramics
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    • 제5권3호
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    • pp.230-234
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    • 1999
  • Ti(CN)-0.3mole% $Mo_2C$ ceramics were prepared by pressureless sintering. $Mo_2C$ dissolved in Ti(CN) more easily in a nitrogen environment than in the other environment because nitrogen forced Mo to form a solid solution, (Ti, No)(C, N). A "core-rim" structure developed within the grains. The boundary between the "core" and the rim was delineated by thermal etching in the sample with more than 2 mole% $Mo_2C$. The rim thickness and the grain size decreased as the $Mo_2C$ content increased. The hardness and the flexural strength showed maxima of 18.2 GPa and 1.23 GPa, respectively when the $Mo_2C$ content was 2 mole%. The post-sintering heat treatments improved the properties.oved the properties.

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Tribological properties and thermal stability of TiAlCN coatings deposited by ICP-assisted sputtering

  • Choe, Han Joo;Kwon, Soon-Ho;Lee, Jung-Joong
    • 한국표면공학회:학술대회논문집
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    • 한국표면공학회 2013년도 춘계학술대회 논문집
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    • pp.209-210
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    • 2013
  • In this study, the tribological and thermal properties of TiAlCN coatings were investigated to evaluate their feasibility in automobile applications. TiAlCN coatings with carbon compositions between 25 and 65 at.% were prepared by inductively coupled plasma (ICP) assisted sputtering and were annealed at 400, 500, and $600^{\circ}C$ in air.

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Al 합금에 MO-PACVD법으로 증착시킨 Ti(CN) 코팅 층의 물성에 관한 연구 (Ti(CN) coating on aluminum alloy formed by MO-PACVD)

  • 김태형;김선규
    • 한국표면공학회지
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    • 제33권1호
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    • pp.38-47
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    • 2000
  • A Ti(CN) layer was formed on aluminum alloy by using diethylamino titanium, hydrogen and nitrogen with the pulsed DC PACVD process. Effect of process parameters such as precursor evaporation temperature, duty ratio, frequency, voltage, $H_2$/$N_2$gas ratio on the properties of Ti(CN) layer were investigated. The layer thus obtained had high hardness and low friction coefficient. Detailed results on the hardness, surface morphology, XRD, WDS analysis, wear test and scratch test of this layer are presented.

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SCM415강의 원형포켓 가공시 치수정밀도에 관한 연구 (A Study on Dimensional Accuracy in Circular Pocket Machining of SCM415 Steel)

  • 신미정;최철웅
    • 한국기계가공학회지
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    • 제18권9호
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    • pp.58-63
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    • 2019
  • In this research, we examine the change of dimensional accuracy in the cutting process while changing cutting conditions such as feed rate and spindle rotational speed with chromium molybdenum steel (SCM415) material and TiCN- and TiAlN-coated end mill tools. According to dimensional accuracy measurement, TiCN-coated tool displays the most accurate dimensional tolerance at ${\varnothing}20mm$ at feed rates of 200 mm/min and 250 mm/min at a spindle rotation speed of 4,000 rpm. The largest dimension of the coating tool was able to make the TiAlN-coated tool suitable when comparing the smallest dimension.

Nanocomposite Coating with TiAlN and Amorphous Carbon Phases Synthesized by Reactive Magnetron Sputtering

  • Kim, Bom Sok;Kim, Dong Jun;La, Joung Hyun;Lee, Sang Yong;Lee, Sang Yul
    • 대한금속재료학회지
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    • 제50권11호
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    • pp.801-808
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    • 2012
  • TiAlCN coatings with various C contents were synthesized by unbalanced magnetron sputtering. The characteristics, the crystalline structure, surface morphology, hardness, and friction coefficient of the coatings as a function of the C content were investigated by X-ray diffraction (XRD), atomic force microscopy (AFM), a microhardness tester, and a wear test. In addition, their corrosion behaviors in a deaerated 3.5 wt% NaCl solution at $40^{\circ}C$ were investigated by potentiodynamic polarization tests. The results indicated that the $Ti_{14.9}Al_{15.5}C_{30.7}N_{38.9}$ coating had the highest hardness, elastic modulus, and a plastic deformation resistance of 39 GPa, 359 GPa, and 0.55, respectively, and it also had the lowest friction coefficient of approximately 0.26. Comparative evaluation of the TiAlCN coatings indicated that a wide range of coating properties, especially coating hardness, could be obtained by the synthesis methods and processing variables. The microhardness of the coatings was much higher than that from previously reported coating using similar magnetron sputtering processes. It was almost as high as the microhardness measured from the TiAlCN coatings (~41 GPa) synthesized using an arc ion plating process. The potentiodynamic test showed that the corrosion resistance of the TiAlCN coatings was significantly better than the TiAlN coatings, and their corrosion current density ($i_{corr}$), corrosion potentials ($E_{corr}$) and corrosion rate decreased with an increasing C content in the coatings. The much denser microstructure of the coatings due to the increased amount of amorphous phase with increasing C contents in the coatings could result in the the improved corrosion resistance of the coatings.

IEEE 802.11기반 Mobile IPv6 Fast Handover에서 CN과의 Binding Update 향상 방안 (Fast Handover Performance Improvement Scheme with CN for Mobile IPv6 base on IEEE 802.11)

  • 류성근;문영성
    • 한국정보과학회:학술대회논문집
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    • 한국정보과학회 2004년도 가을 학술발표논문집 Vol.31 No.2 (3)
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    • pp.679-681
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    • 2004
  • 무선 통신 기술의 발달로 무선 인터넷에 대한 관심과 그에 따른 이동성 지원에 대한 관심이 증가하고 있다. 또한 이동성 지원을 위한 Mobile IPv6의 Handover 시에 상대노드(CN)와의 바인딩 갱신(Binding Update) 지연시간이 문제가 되고 있다. 문제 해결을 위해서 2계층과 3계층을 연동하는 Fast Handover를 이용하여, MN에서 CN으로의 바인딩 갱신 지연시간을 단축시키고자 2계층 Handover 메시지인 IEEE 802.11의 Reassociation Request 프레임을 이용한다. MN이 Binding 갱신 메시지를 보내기 전에 CN과의 보안을 위해서 Return Routability 절차을 수행하는데 이 절차 중의 메시지인 HoTI, CoTI 메시지를 2계층 Handover 중에 미리 보냄으로써 CN과의 바인딩 갱신 지연시간을 단축시키는 방안을 제안한다.

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