• Title/Summary/Keyword: Three-dimensional microstructure

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Computer Simulation of Quench-Hardening of Alloy Steel for Structural Purposes by the Modified Finite Difference Method (개량차분법에 의한 임의의 형상의 열처리제품의 급냉경화 해석)

  • Kim, K.S.;Song, Y.B.;Hong, C.P.
    • Journal of the Korean Society for Heat Treatment
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    • v.2 no.2
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    • pp.11-16
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    • 1989
  • Understanding and control of thermal history of heat-treated components are very important in heat treating process. A computer program was developed for prediction of thermal history in quenching process with various cooling media and agitation conditions. Computer simulation of heat flow in quenching treatment of spur gear of SCM 22 H was carried out by two and three dimensional finite difference method. Distributions of microstructure and hardness in heat-treated spur gear were predicted by computer simulation, and the results showed a good agreement with the experiments. It was concluded that the

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Effect of lubrication on the evolution of strain states in AA 5052 sheet during shape rolling (알루미늄 5052 합금 판재의 이형 압연 시 변형률 상태에 미치는 윤활의 영향)

  • Park, E.S.;Hwang, K.C.;Huh, M.Y.;Kim, H.J.;Bae, J.C.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2009.05a
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    • pp.256-259
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    • 2009
  • In order to investigate the effect of strain states attributed to the lubrication during shape rolling, shape rolling for V-sectioned sheets was carried out with and without lubrication. The evolution of strain states during shape rolling was studied by three-dimensional finite element method (FEM). Shape rolling with and without lubrication produces shape-rolled samples in fairly similar outer shapes, since the distribution of normal strain components is nearly independent of the lubrication condition. In contrast, the distribution of shear strain components strongly depends on the lubrication condition.

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Homogenized thermal properties of 3D composites with full uncertainty in the microstructure

  • Ma, Juan;Wriggers, Peter;Li, Liangjie
    • Structural Engineering and Mechanics
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    • v.57 no.2
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    • pp.369-387
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    • 2016
  • In this work, random homogenization analysis for the effective thermal properties of a three-dimensional composite material with unidirectional fibers is presented by combining the equivalent inclusion method with Random Factor Method (RFM). The randomness of the micro-structural morphology and constituent material properties as well as the correlation among these random parameters are completely accounted for, and stochastic effective thermal properties as thermal expansion coefficients as well as their correlation are then sought. Results from the RFM and the Monte-Carlo Method (MCM) are compared. The impact of randomness and correlation of the micro-structural parameters on the random homogenized results is revealed by two methods simultaneously, and some important conclusions are obtained.

Rheological Behavior of Polymer/Layered Silicate Nanocomposites under Uniaxial Extensional Flow

  • Park Jun-Uk;Kim Jeong-Lim;Kim Do-Hoon;Ahn Kyung-Hyun;Lee Seung-Jong;Cho Kwang-Soo
    • Macromolecular Research
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    • v.14 no.3
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    • pp.318-323
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    • 2006
  • We investigated the rheological behaviors and orientation of three different types of layered silicate composite systems under external flow: microcomposite, intercalated and exfoliated nanocomposites. Rheological measurements under shear and uniaxial extensional flows, two-dimensional, small-angle X-ray scattering and transmission electron microscopy were conducted to investigate the properties, as well as nano- and micro-structural changes, of polymer/layered silicate nanocomposites. The preferred orientation of the silicate layers to the flow direction was observed under uniaxial extensional flow for both intercalated and exfoliated systems, while the strain hardening behavior was observed only in the exfoliated systems. The degree of compatibility between the polymer matrix and clay determined the microstructure of polymer/clay composites, strain hardening behavior and spatial orientation of the clays under extensional flow.

Investigation on the Sintering Behavior of P/M Al-Zn-Mg-Cu Alloy

  • Shahmohammadi, M.;Simchi, A.;Danninger, H.;Arvand, A.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.536-537
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    • 2006
  • In the present work, the sintering behavior of high strength Al-5.6Zn-2.5Mg-1.6Cu (in wt.%) alloy compacts prepared from elemental powders was investigated. Microstructural evaluation was accompanied by XRD and DSC methods in order to determine the temperature and chemical composition of the liquid phases formed during sintering. It was found that three transient liquid phases are formed at 420, 439 and 450 $^{\circ}C$. Microstructural study revealed the progressive formation of sintered contacts due to the presence of the liquid phases, although the green compact expands as a result of the melt penetration along the grain boundaries. While Zn melts at ${\sim}420\;^{\circ}C$, the intermetallic phases formed between Al and Mg were found to be responsible for the formation of liquid phase and the dimensional change at higher temperatures.

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Three-dimensional microstructure analysis of small animal bone using synchrotron radiation (방사광을 이용한 작은 동물 뼈의 3차원 미세구조 분석)

  • Kim, Su-Bok;Jang, Sang-Hoon;Lee, On-Seok
    • Proceedings of the Korea Information Processing Society Conference
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    • 2018.10a
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    • pp.795-796
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    • 2018
  • 방사광은 기존 기계학적인 방법으로 분석했던 연구보다 더 정확한 관찰이 가능해 신뢰도가 높은 결과를 얻을 수 있다. 본 연구의 목적은 흰쥐 정강뼈의 미세구조를 3차원적으로 분석 가능한 방사광기반 경X선을 이용해 골다공증의 진단 및 평가에 필요한 정량화된 분석을 구축하고자 하였다. 흰 쥐의 정강뼈를 방사광을 통해 해부학 구조 및 미세내부구조를 얻은 뒤 3차원적 구조분석을 하였다. 그 후, 방사광으로 얻은 영상 데이터를 통해 뼈 내부 구조를 높은 해상도 이미지로 시각화하여 분석을 할 수 있었다. 따라서, 골다공증과 관련된 퇴행성 골격질환의 정량화된 분석방법을 제시하여 근거중심의 평가와 예방의 기초자료가 될 것으로 기대한다.

Electrochemical Properties of Carbonized Phenol Resin (탄화된 페놀레진의 전기화학적 성질)

  • 김한주;박종은;홍지숙;류부형;박수길
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1999.11a
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    • pp.629-632
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    • 1999
  • For replacing Li metal ai Lithium ton Bakery(LIB) system. we used carbon powder material which prepared by pyrolysis of phenol resin as starting material. It became amorphous carbon by pyrolysis through it\`s self condensation by thermal treatment. Amorphous carbon can be doped with Li intercalation and deintercalation because it has wide interlayer. however it has a problem with structural destroy causing weak carbon-carbon bond. So. we used ZnCl$_2$ as the pore-forming agent. This inorganic salt used together with the resin serves not only as the pore-forming agent to form open pores, which grow Into a three-dimensional network structure in the cured material, foul also as the microstructure-controlling agent to form a loose structure dope with bulky dopants. We analyzed SEM in order to find to different of structure. and can calculate distance of interlayer. CV test showed oxidation and reduction

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Shape Control of Automotive Flexible Plate in Press Quenching (프레스 퀜칭 공정에 의한 자동차 Flexible Plate의 형상 제어 연구)

  • Park, I.H.;Jeong, W.C.
    • Journal of the Korean Society for Heat Treatment
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    • v.21 no.4
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    • pp.189-198
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    • 2008
  • The production of automotive chassis parts requiring both high hardness and good shape-holdability is better realized by using press quenching technology, comprising the austenitizaton and the subsequent press quenching in a specially designed stamping tool. The effect of press quenching mold shape on the hardness distribution, bending height, and degree of planeness of automotive flexible plate during press quenching and tempering has been investigated. The preferable shape of the projections of punch and die in contact with the flexible plate was close to oval to improve the flow of cooling oil, leading to the higher hardness. The press quenching mold with three separate parts was more effective to control the dimensional change due to thermal deformation during press quenching. Some decrease in the bending height during tempering may be related to some recovery of the residual stress at $400^{\circ}C$.

Micro-CT analysis of LPS-induced Alveolar Bone Loss in Diabetic Mice

  • Park, Hae-Ryoung;Park, Byung-Ju
    • International Journal of Oral Biology
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    • v.37 no.3
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    • pp.85-90
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    • 2012
  • Periodontal disease induces an increased incidence of tooth loss, particularly in cases with an associated loss of alveolar bone and periodontal ligaments. In this study, alveolar bone loss was detected by micro-computed tomography (CT) following exposure to E. coli lipopolysaccharide (LPS) in a streptozotocin (STZ)-induced diabetic mouse model. A 10 mg/ml dosage of E. coli LPS was applied between the first, second and third molars of the mice three times a week for 10 weeks. The loss of periodontal ligaments and alveolar processes was then evaluated by micro-CT using two and three dimensional microstructure morphometric parameters. In the diabetic mice, E. coli LPS induced the destruction of periodontal ligaments and loss of alveolar process spaces. The distances between periodontal ligaments were significantly widened in the STZ-LPS group compared with the untreated STZ group. The 10 mg/ml exposure to E. coli LPS in the STZ mice also resulted in a significant decrease in the alveolar bone volume fraction. The results of our study suggest that alveolar bone loss can be readily detected by volumetric micro-CT analysis as an increase in the distance between periodontal ligaments and in the alveolar process length.

Comparison of Milk-clotting Activity of Proteinase Produced by Bacillus Subtilis var, natto and Rhizopus oligosporus with Commercial Rennet

  • Chen, Ming Tsao;Lu, Ying Yu;Weng, Tien Man
    • Asian-Australasian Journal of Animal Sciences
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    • v.23 no.10
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    • pp.1369-1379
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    • 2010
  • This study investigated purification and milk-clotting activity of the enzymes produced by Bacillus subtilis var, natto and Rhizopus oligosporus compared with that of commercial rennet. The clotting time, viscosity, tension and microstructure of the curd and electrophoretic patterns of milk proteins were determined. The milk-clotting activity/proteolytic activity ratios (MCA/PA ratio) of B. subtilis, R. oligosporus and commercial rennet were also compared. The results revealed that the curd formed by the commercial rennet had the highest viscosity and curd tension and the shortest clotting time among the three enzymes. However, curd produced by Rhizopus enzymes was ranked as second. From the MCA/PA ratio and electrophoretogram analyses it could be concluded that the enzyme produced by B. subtilis had the highest proteolytic activity, while the commercial rennet had the highest milk-clotting activity. Observations of microstructures of SEM showed that the three-dimensional network for curd formed by commercial rennet was denser, firmer and more smooth. The milk-clotting activity, specific activity, purification ratio and recovery of the purified enzymes produced by both the tested organisms were also determined with ion exchange chromatography and gel filtration.