• 한국세라믹학회지
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• 제55권6호
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• pp.597-607
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• 2018

In this study, a wet chemical method was used to synthesize nanostructured hydroxyapatite for biomedical applications. Diammonium hydrogen phosphate and calcium nitrate 4-hydrate were used as starting materials with a sodium hydroxide solution as an agent for pH adjustment. Scanning electron microscopy, transmission electron microscopy, Fourier-transform infrared spectroscopy, differential thermal analysis, thermal gravimetric analysis, atomic absorption spectroscopy, and ethylenediaminetetraacetic acid (EDTA) titration analysis were used to characterize the synthesized powders. Having been uniaxially pressed, the powders formed a disk-like shape. The sinterability and electrical properties of the samples were examined, and the three-point bending test allowed for the measurement of their mechanical properties. Sedimentation analysis was used to analyze the slurry ability of hydroxyapatite. As in-vitro biological properties of the samples, biocompatibility and cytotoxicity were assessed using osteoblast-like cells and the L929 cell line, respectively. Solubility was assessed by employing a simulated body fluid.

• 한국복합재료학회:학술대회논문집
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• 한국복합재료학회 2001년도 추계학술발표대회 논문집
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• pp.125-128
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• 2001

In this wort, the $Na^+-MMT$ has organically modified with silane intercalant to prepare the polymer/clay nanocomposites. The pH. X-ray diffraction (XRD), and contact angles were used to analyze the surface properties of clay and the exfoliation phenomenon of clay interlayer, The mechanical interfacial properties of epoxy/clay nanocomposites were investigated by three-point bending test. From the experimental results. the surface modification made by silane intercalant on clay surface leads to an increase of distance of silicate layers, surface acid value. and electron acceptor parameter of organoclay. The treatments are also necessary and useful for epoxy to intercalate into the interlayer by interacting of electron donor-accepter between basic epoxy and clay surface. The mechanical interfacial properties of the nanocomposites was improved by the presence of dispersed clay nanolayer containing low content of organoclay in comparison with the conventional, which increase the interfacial adhesion between dispersed clay and epoxy resins.

• 대한기계학회논문집
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• 제14권1호
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• pp.79-86
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• 1990

본 연구에서는 균열 길이의 별도 측정없이, 하중변위 곡선에서 직접 $J_{IC}$를 결정하는 방법을 제안하고 그 타당성을 조사한다. 또한 키이 곡선(key curve)을 이용하여 $J_{IC}$를 좀더 간단하게 구하는 방법에 대해서도 알아본다. 위의 방법으 로 결정된 $J_{IC}$의 값은 ASTM에 의해 제안된 R-곡선 방법으로 고한 $J_{IC}$의 값 과 비교된다. 본 연구의 타당성을 조사하기 위하여 기계 구조용합금강인 SCM4를 사 용한 파괴 실험을 수행한다.

• 한국재료학회지
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• 제14권9호
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• pp.642-648
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• 2004

The microstructure and crack tip opening displacement (CTOD) of deposit weld metal were investigated for a 30 mm- thick plate welded with flux cored arc welding (FCAW) and submerged arc welding (SAW) processes. The CTOD test was carried out both as welded condition and as stress-relieved specimen by local compression. The crack growth rates in FCAW were faster than those in a SAW, and the acicular ferrite content by the SAW process was increased relatively more than that by the FCAW process. The fatigue crack growth rate in a welded specimen was faster than that in locally compressed specimen. The CTOD value of locally compressed specimens was lower than that of as welded specimen. Furthermore, the CTOD value tested with the SAW process was higher than that tested with the FCAW process.

• 한국안전학회지
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• 제32권4호
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• pp.1-6
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• 2017

Functionally Graded Materials (FGM) as advanced heterogeneous composite materials have a higher performance than a conventional composite or bimaterial composite under some severe environments. As a heterogeneous material, FGM is commonly used in spacecraft, defense, nuclear and automotive industries due to its excellent properties. The purposes of this study are to evaluate the stress distribution and crack behaviors by the multiscale simulation. FGM contains two or more than two materials that the composition is structured continuously. Two types of FGM model are suggested, which are created by arbitrary prediction of the volume fraction and the exponential function. Aluminum as the metal matrix constituent and silicon carbide as the ceramic particle constituent are structured gradually by two types and the three point bending test also estimated. Moreover, two kinds of crack location were introduced in order to get the influences of material property distribution on the stress intensity factor. From the results we found that the stress intensity factors are increased in the case from softer to stiffer material, while vice versa.

• 한국신뢰성학회지:신뢰성응용연구
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• 제16권2호
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• pp.104-109
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• 2016

Purpose: The purpose of this study is to analyze fracture behavior and failure mechanism of porous titanium for dental implant fabricated by space holder process. Method: Three porous titanium specimens with a specific volume fraction of open pore were test by 3 point bending and compression stress condition, respectively. Fracture appearance was observed by scanning electron microscope and discussed in relation with oxygen content. Results: For compression-tested specimens, two specimen showed brittle failure, while the other one showed normal failure after deformation. High oxygen content was detected in the brittle-fractured specimen. Several micro-cracks initiated at the struts propagated down to the bottom of the specimen resulting in normal failure. Conclusion: Oxygen contamination during the fabrication process can leads brittle premature failure, and hence quality problem of the porous titanium for dental implant.

• Steel and Composite Structures
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• 제13권5호
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• pp.489-500
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• 2012

Cold-formed steel profile sheets acting as decks have been popularly used in composite slab systems in steel structural works, since it acts as a working platform as well as formwork for concreting during construction stage and also as tension reinforcement for the concrete slab during service. In developing countries like India, this system of flooring is being increasingly used due to the innate advantage of these systems. Three modes of failure have been identified in composite slab such as flexural, vertical shear and longitudinal shear failure. Longitudinal shear failure is the one which is difficult to predict theoretically and therefore experimental methods suggested by Eurocode 4 (EC 4) of four point bending test is in practice throughout world. This paper presents such an experimental investigation on embossed profile sheet acting as a composite deck where in the longitudinal shear bond characteristics values are evaluated. Two stages, brittle and ductile phases were observed during the tests. The cyclic load appears to less effect on the ultimate shear strength of the composite slab.

• Advances in concrete construction
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• 제2권2호
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• pp.145-162
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• 2014

In this study, the fracture toughness $K_{IC}$ of high performance concrete (HPC) was determined by conducting three-point bending tests on eighty notched HPC beams of $500mm{\times}100mm{\times}100mm$ at high temperatures up to $450^{\circ}C$ (hot) and in cooled-down states (cold). When the concrete beams exposed to high temperatures for 16 hours, both thermal and hygric equilibriums were generally achieved. $K_{IC}$ for the hot concrete sustained a monotonic decrease tendency with the increasing temperature, with a sudden drop at $105^{\circ}C$. For the cold concrete, $K_{IC}$ sustained a two-stage decrease trend, dropping slowly with the heating temperature up to $150^{\circ}C$ and rapidly thereafter. The fracture energy-based fracture toughness $K_{IC}$' was found to follow similar decrease trends with the heating temperature. The weight loss, the fracture energy and the modulus of rapture were also evaluated.

• Corrosion Science and Technology
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• 제6권6호
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• pp.286-290
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• 2007

Biocompatible Hydroxy apatite (HAp) coatings on metallic substrate by plasma spray techniques have been developed. Long-term credibility of plasma spray HAp coatings has been evaluated in physiological saline by electrochemical measurements. It was found that the corrosion resisitance of SUS316L based HAp/Ti conbined coatings was excellent even after more than 10 weeks long-term immersion. It was shown that postal heat treatment improved both the crystallinity and corrosion resistance of HAp. By lowering cooling rate during heat treatment process, less cracks produced in HAp coating layer, which lead to higher credibility of HAp during immersion in physiological saline. The ICP results showed that the dissolution level of substrate metallic ions was low and HAp coatings produced in this research can be acceptable as biocompatible materials. Also, the concentration of dissolved ions from HAp coatings with postal heat treatment was lower compared to those from samples without postal heat treatment. The adherence of HAp coatings with Ti substrate and other mechanical properties were also assessed by three-point bending test. The poor adhesion of HAp coating to titanium substrate can be improved by introducing a plasma spray titanium intermediate layer.

• 한국생산제조학회지
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• 제23권2호
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• pp.145-151
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• 2014

Recently, the growing demand for weight reduction and improved structure durabilityfor commercial vehicles has led to active research into the development and application of suitablecomposite materials. This studysuggests abimaterial composite frame produced by apultrusion process to replace steel frames. We focused on the development of a composite frameconsisting of two types of materialsby mixing anorthotropic material with anisotropic material. The inside layer consisted of an aluminum pipe, and the outside layer was composed of a glass fiber pipe. To determine the strength and failure mechanisms of the composite material, tensile tests, shear tests, and three-point bending tests were conducted, followed by fatigue tests. After static testing, the fatigue tests were conducted at a load frequency of 5 Hz, a stress ratio (R) of 0.1, and an endurance limit of $10^6$ for the S-N curve. The resultsshowed that the failure modes were related to both the core design and the laminating conditions.