• 한국세라믹학회지
• /
• 제49권4호
• /
• pp.385-396
• /
• 2012

Thermal shock test methods and thermal shock parameters for ceramics were reviewed from the following viewpoints: (1) The test methods should be based on the precise estimation of both temperature and thermal stress distributions in a specimen taking into account the temperature-dependent thermo-mechanical properties; (2) The thermal shock parameters must be defined as a physical property of the materials and described as a function of temperature at the fracture point of the specimen; (3) The relation between the strength and fracture toughness of brittle ceramics under a thermal shock load must be the same as the relation under a mechanical load. In addition, appropriate thermal shock parameters should be defined by the thermal shock strength and thermal shock fracture toughness based on stress and energy criteria, respectively. A constant heat flux method is introduced as a testing technique suitable for estimating these thermal shock parameters directly from the electric power charged.

• 한국전기전자재료학회논문지
• /
• 제23권8호
• /
• pp.611-616
• /
• 2010

This study investigated the characteristics of fracture behavior and mode on solder joints before and after thermal shock test for automotive application component using Sn-3.0Ag-0.5Cu solder, which has a outstanding property as lead-free solder. The shear strength was decreased with thermal cycle number, after 432 cycles of thermal shock test. In addition, fracture mode was verified to ductile, brittle fracture and base materials fracture such as different kind fractured mode using SEM and EDS. Before the thermal shock, the fractured mode was found to typical ductile fracture in solder layer. After thermal shock test, especially, Ag was found on fractured portion as roughest surface. Moreover, it occurred delamination between a PCB and a Cu land. Before thermal shock test, most of fractured mode in solder layer has dimples by ductile fracture. However, after thermal shock test, the fractured mode became a combination of ductile and brittle fracture, and it also could find that the fracture behavior varied including delamination between substrate and Cu land.

• 한국자동차공학회논문집
• /
• 제19권6호
• /
• pp.90-96
• /
• 2011

In this study, the characteristic of fractured portion and shape on solder joints were investigated according to the thermal shock test for Automotive Application Component using Sn-3.0Ag-0.5Cu solder, which has a outstanding property as Lead-free solder. The value of pull and shear strength was decreased in principle after 432 cycles thermal shock test. In addition, fracture mode was verified by using EDS and SEM to observe fractured shape on the solder joints before and after thermal shock. In before thermal shock test, the fracture mode revealed typically solder layer's fracture mode. In after thermal shock test, we identified multiple fracture mode of the ductile and brittle fracture. Even though same composition of solder was used to experimental for estimating. the fracture mode varied on the fracture portion's height and the directional angles of shear strength. In conclusion, we identified that mechanical strength was affected on the solder layer's fracture mode.

• 수산해양기술연구
• /
• 제43권4호
• /
• pp.362-369
• /
• 2007

This paper was studied on the characteristics of acid resistance and thermal shock for epoxy coatings in the strong acidic environment. The exhaust gas system, such as a air preheater, desulfurization equipment, for industrial boiler is damaged by dew point corrosion. To protect the acid corrosion, the coating using nonmetal was applied. The electrochemical polarization test, acid resistance and thermal shock test for epoxy coatings were carried out. And the acid resistance and thermal shock characteristics, aspect, and electrochemical anti-corrosion characteristics for epoxy coatings in the strong acidic environment were considered. The main results are as followings: As the epoxy glass flake coating by acidic thermal shock was damaged to the crack, blistering and elution etc., the current density of epoxy glass flake coating is high. But the damage of epoxy metal complex coating by acidic thermal shock was not occurred. Therefore the characteristics of acid resistance and thermal shock for epoxy metal complex coating is better than those for epoxy glass flake coating.

• 한국분말재료학회지
• /
• 제29권6호
• /
• pp.505-510
• /
• 2022

The thermal shock resistance of cement composites with hollow glass microspheres (HGM) is investigated. Cement composites containing various concentrations of HGM are prepared and their properties studied. The density, thermal conductivity, and coefficient of thermal expansion of the composites decrease with increasing HGM concentration. A thermal shock test is performed by cycling between -60 and 50℃. After the thermal shock test, the compressive strength of the cement composite without HGM decreases by 28.4%, whereas the compressive strength of the cement composite with 30 wt% HGM decreases by 5.7%. This confirms that the thermal shock resistance of cement is improved by the incorporation of HGM. This effect is attributed to the reduction of the thermal conductivity and coefficient of thermal expansion of the cement composite because of the incorporation of HGM, thereby reducing the occurrence of defects due to external temperature changes.

• 한국세라믹학회지
• /
• 제36권10호
• /
• pp.1062-1068
• /
• 1999

상온 25$^{\circ}C$의 증류수에 단일 열충격을 시행한 후 ball-on-3 ball test로 강도를 측정하고 강도의 변화를 관찰하였다. 시편은 상용 알루미나 시편을 사용하였고, disc 형태의 시편에 대하여 열충격 후의 균열의 모양과 강도 시험 후의 균열의 모양을 잉크 침투법에 의해 관찰하였다. 통계적인 파괴 확률방법을 제시하였으며, thermal shock Weibull plot을 이용하여 3점 꺾임 강도와 비교하였다. ball-on-3 ball test 강도에 미치는 인자에 대해 통계학적인 접근을 통해 관찰한 결과, 시편중심에서 균열까지의 거리가 균열 밀도보다 더 큰 영향을 미치고 있음을 알 수 있었다.

• 한국세라믹학회지
• /
• 제43권4호
• /
• pp.247-252
• /
• 2006

Joining Yittria Stabilized Zirconia (YSZ) to NiCr metal was fabricated using YSZ/NiCr Functionally Graded Materials (FGM) Interlayer by hot pressing process. Microscopic observations demonstrate that the composition and microstructure of YSZ/NiCr FGM distribute gradually in stepwise way, eliminating the macroscopic ceramic/metal interface such as that in traditional ceramic/metal joint. The thermal characteristics of this YSZ/FGM/NiCr joint were studied by thermal shock testing and therml barrier testing. Thermal shock test was conducted by gas burner rig. Acoustic Emission (AE) monitoring was performed to analyze the microfracture behavior during the thermal shock test. It could be confirmed that FGM was the excellent performance of thermal shock/barrier resistance at above $1000^{\circ}C$.

• 한국해양공학회지
• /
• 제27권5호
• /
• pp.22-27
• /
• 2013

The present work dealt with the high temperature thermal shock properties of 316 stainless steels, in conjunction with a detailed analysis of their microstructures. In particular, the effects of the thermal shock temperature difference and thermal shock cycle number on the properties of 316 stainless steels were investigated. A thermal shock test for 316 stainless steel was carried out at thermal shock temperature differences from $300^{\circ}C$ to $1000^{\circ}C$. The cyclic thermal shock test for the 316 stainless steel was performed at a thermal shock temperature difference of $700^{\circ}C$ up to 100 cycles. The characterization of 316 stainless steels was evaluated using an optical microscope and a three-point bending test. Both the microstructure and flexural strength of 316 stainless steels were affected by the high-temperature thermal shock. The flexural strength of 316 stainless steels gradually increased with an increase in the thermal shock temperature difference, accompanied by a growth in the grain size of the microstructure. However, a thermal shock temperature difference of $800^{\circ}C$ produced a decrease in the flexural strength of the 316 stainless steel because of damage to the material surface. The properties of 316 stainless steels greatly depended on the thermal shock cycle number. In other words, the flexural strength of 316 stainless steels decreased with an increase in the thermal shock cycle number, accompanied by a linear growth in the grain size of the microstructure. In particular, the 316 stainless steel had a flexural strength of about 500 MPa at 100 thermal-shock cycles, which corresponded to about 80% of the strength of the as-received materials.

• 열처리공학회지
• /
• 제14권3호
• /
• pp.155-159
• /
• 2001

The thermal shock resistance has been investigated and compared in three hot-work tool steels. The resistance to thermal shock is first of all a matter of good toughness and ductility. Therefore, a proper hot-work tool steel should be characterized by high fracture strength and high temperature toughness. In this study, new test method is proposed to measure the thermal shock resistance. New method is basically based on Uddeholm' thermal shock test but some modification has been properly applied. Based on these results, some critical temperature($T_{fractures}$) at which fracture occur can be measured to characterize the thermal resistance of the materials. The specific values of ${\Delta}T$, the temperature difference between holding temperature and $T_{fractures}$, has been successfully used as a measure of the thermal shock resistance in this study, the results showed that the thermal shock method used in this study was properly modified.

• 대한금속재료학회지
• /
• 제48권8호
• /
• pp.775-779
• /
• 2010

Functionally graded materials (FGM) of PSZ/NiCrAlY on Inconel substrate were fabricated by detonation gun spraying method. A thick ceramic layer generally has a high thermal barrier effect however, because failure often occurs, the use of an FGM layer gives an advantage in thermal property. During the thermal shock test, micro fracture processes were detected by the AE method. Also, the thermal shock test was performed for NFGM, FGM and the changed FGM in the layered composition profile. It was found through AE testing and the observation of fracture surface that FGM was superior to NFGM in thermal shock properties. The linear or metal-rich type FGM in composition profile had the best resisting property among the FGM. It was found that the controlled composition profile of the graded layers had better thermal properties.