• Title/Summary/Keyword: Thermal curing

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Numerical Simulation of Temperature and Stress Distribution in Mass Concrete with pipe cooling and Comparision with Experimental Measurements (매스콘크리트 시험체의 수화열 해석 및 실험)

  • 주영춘;김은겸;신치범;조규영;박용남
    • Proceedings of the Korea Concrete Institute Conference
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    • 1999.04a
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    • pp.269-274
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    • 1999
  • Various method have been developed for mass concrete structures to reduce the temperature increase of concrete mass due to exothermic hydration reactions of concrete compounds and thereby to avoid thermal cracks. One of the methods widely acceptable for practical use is pipe cooling, in which cooling is achieved by circulating cold water through thin-wall steel pipes embedded in the concrete. A numerical simulation was performed to investigate the effectiveness of pipe cooling. A three-dimensional finite element method was proposed to analyse the transient three-dimensional heat transfer between the hardening concrete and the cooling water in pipe and to predict the stress development during the curing process. The effects of the cement type and content and the environment were taken into consideration by the heat generation rate and the boundary conditions, respectively. In order to test the validity of the numerical simulation, a model RC structure with pipe cooling was constructed and the time-dependent temperature and stress distributions within the structure as well as the variation of the temperature of cooling water along the pipe were measured. The results of the simulation agreed well the experimental measurements. The results of this study have important implications for the optimal design of the cooling pipe layout and for the estimation of thermal stress in order to eliminate thermal cracks.

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Cure Characteristics, Mechanical Properties, Abrasion Property and Thermal Properties of EVM/EPM Blends Containing Flame Retardants

  • Sung, Il Kyung;Lee, Won Ki;Park, Chan Young
    • Elastomers and Composites
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    • v.52 no.2
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    • pp.105-113
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    • 2017
  • The curing behavior, mechanical properties, hot-air aging resistance, abrasion properties,thermal properties, etc., of EVM/EPM/APP (ammonium polyphosphate)/DPER (dipentaerythritol)/EG (expandable graphite) and EVM/EPM/ATH (aluminium trihydroxide) flame retarding systems in ethylene vinyl acetate rubber (EVM) blends with EPM (ethylene propylene rubber) were sequentially examined. For both flame retarding systems, the torque values increased with the content of EPM rubber and with the vulcanization time. As the content of EPM rubber increased, the scorch time became shorter, whereas the optimum cure time followed an increasing trend. For the EVM/EPM/APP/DPER/EG flameretarding system, as the content of EPM rubber increased, the hardness did not change,whereas the tensile strength and elongation at break decreased. A hot-air aging resistance test at $150^{\circ}C$ showed that the heat resistance decreased with the EPM content regardless of the kinds and contents of flame retardants. As the EPM content increased, the abrasion rate became higher and the abrasion resistance of the EVM/EPM/APP/DPER/EG flame retarding systems exceeded that of the EVM/EPM/ATH flame retarding counterparts. In comparison with the EVM/EPM/ATH flame retarding systems, the thermal stability of the EVM/EPM/APP/DPER/EG flame retarding system showed an increasing tendency.

Thermocompression Anisothropic Conductive Films(ACFs) bonding for Flat Panel Displays(FPDs) Application (평판디스플레이를 위한 열압착법을 이용한 이방성 도전성 필름 접합)

  • Pak, Jin-Suk;Jo, Il-Jea;Shin, Young-Eui
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.22 no.3
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    • pp.199-204
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    • 2009
  • The effect of temperature on ACF thermocompression bonding for FPD assembly was investigated, It was found that Au bumps on driver IC's were not bonded to the glass substrate when the bonding temperature was below $140^{\circ}C$ so bonds were made at temperatures of $163^{\circ}C$, $178^{\circ}C$ and $199^{\circ}C$ for further testing. The bonding time and pressure were constant to 3 sec and 3.038 MPa. To test bond reliability, FPD assemblies were subjected to thermal shock storage tests ($-30^{\circ}C$, $1\;Hr\;{\leftrightarrow}80^{\circ}C$, 1 Hr, 10 Cycles) and func! tionality was verified by driver testing. It was found all of FPDs were functional after the thermal cycling. Additionally, Au bumps were bonded using ACF's with higher conductive particle densities at bonding temperatures above $163^{\circ}C$. From the experimental results, when the bonding temperature was increased from $163^{\circ}C$ to $199^{\circ}C$, the curing time could be reduced and more conductive particles were retained at the bonding interface between the Au bump and glass substrate.

Thermal Frequency Tuning of Microactuator with Polymer Membrane (온도 변화를 이용한 고분자 막 마이크로 액추에이터의 공진 주파수 튜닝)

  • Lee, Seung-Hoon;Lee, Seok-Woo;Kwon, Hyuk-Jun;Lee, Kwang-Cheol;Lee, Seung-S.
    • Proceedings of the KSME Conference
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    • 2008.11a
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    • pp.1857-1862
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    • 2008
  • Resonant frequency tuning of micro devices is essential to achieve performance uniformity and high sensitivity. Previously reported frequency tuning methods using electrostatic force or mass deposition are not directly applicable to non-conducting polymer devices and have limitations such as dielectric breakdown or low tunable bandwidth. In this paper, thermally frequency-tunable microactuators with poly-dimethylsiloxane membranes are proposed. Permanent and/or nonpermanent frequency tunings are possible using a simple temperature control of the device. Resonant frequency and Q-factor variations of devices according to temperature change were studied using a micro heater and laser Doppler vibrometer. The initial resonant frequencies determined by polymer curing and hardening temperatures are reversibly tuned by thermal cycles. The measured resonant frequency of 9.7 kHz was tuned up by ${\sim}25%$ and Q-factor was increased from 14.5 to 27 as the micro heater voltage increased from 0 to 70 V.

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Change of transmission characteristics of FSSs in hybrid composites due to residual stresses

  • Hwang, In-Han;Chun, Heoung-Jae;Hong, Ik-Pyo;Park, Yong-Bae;Kim, Yoon-Jae
    • Steel and Composite Structures
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    • v.19 no.6
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    • pp.1501-1510
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    • 2015
  • The frequency selective surface (FSS) embedded hybrid composite materials have been developed to provide excellent mechanical and specific electromagnetic properties. Radar absorbing structures (RASs) are an example material that provides both radar absorbing properties and structural characteristics. The absorbing efficiency of an RAS can be improved using selected materials having special absorptive properties and structural characteristics and can be in the form of multi-layers or have a certain stacking sequence. However, residual stresses occur in FSS embedded composite structures after co-curing due to a mismatch between the coefficients of thermal expansion of the FSS and the composite material. In this study, to develop an RAS, the thermal residual stresses of FSS embedded composite structures were analyzed using finite element analysis, considering the effect of stacking sequence of composite laminates with square loop (SL) and double square loop (DSL) FSS patterns. The FSS radar absorbing efficiency was measured in the K-band frequency range of 21.6 GHz. Residual stress leads to a change in the deformation of the FSS pattern. Using these results, the effect of transmission characteristics with respect to the deformation on FSS pattern was analyzed using an FSS Simulator.

Using scratch test to evaluate cohesive bond strength of Mo composite coating

  • Koiprasert, Hathaipat;Thaiwatthana, Sirinee;Sheppard, Panadda
    • International Journal of Advanced Culture Technology
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    • v.3 no.2
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    • pp.34-41
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    • 2015
  • Bonding strength of a thermal sprayed coating is difficult to measure using a conventional pull-off test method. Scratch test is a potential alternative testing method. An adhesive and a cohesive bond strength of the coating can be measured by the pull-off test while the scratch test performed on the cross-section of the thermal sprayed coating can only demonstrate the cohesive bond strength of the coating. Nevertheless, it is still beneficial to perform the scratch testing on the cross-section of the coating for the sake of comparison thus providing an alternative to the pull-off test. The scratch test method can reduce testing time and cost in the long run due to a significant cost reduction in consumables and energy and time saving from the curing step of the glue used in the pull-off test. This research investigates the possibility of using the scratch test to measure the cohesive bond strength of Mo/NiCrBSi composite coating. The results from the pull-off test and the scratch test indicate that the cohesive bond strengths of the Mo composite coating show similar trend and that the cohesive bond strength are increased when increasing NiCrBSi content.

Developing Sealing Material of a Dye-Sensitized Solar Cell for Outdoor Power (실외 발전을 위한 염료감응형 태양전지의 봉지재 개발)

  • Ki, Hyun-Chul;Hong, Kyung-Jin
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.29 no.12
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    • pp.819-823
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    • 2016
  • DSSC (dye-sensitized solar cell) is expected to be one of the next-generation photovoltaics because of its environment-friendly and low-cost properties. However, commercialization of DSSC is difficult because of the electrolyte leakage. We propose thermal curable base on silicon resin and apply a unit cell and large area ($200{\times}200mm$) dye-sensitized solar cell. The resin aimed at sealing of DSSC and gives a promising resolution for sealing of practical DSSC. In result, the photoelectric conversion efficiency of the unit cell and the module was 6.63% and 5.49%, respectively. In the durability test result, the photoelectric conversion efficiency of the module during 500, 1,000, 1,500 and 2,000 hours was 0.73%, 0.73%, 1.82% and 2.36% respectively. It was confirmed that the photoelectric conversion efficiency characteristics are constant. We have developed encapsulation material of thermal curing method excellent in chemical resistance. A sealing material was applied to the dye-sensitized solar cell and it solved the problem of durability the dye-sensitized solar cell. Sealing material may be applied to verify the possibility of practical application of the dye-sensitized solar cell.

Effects of Reinforcing Fillers on Far-infrared Vulcanization Characteristics of EPDM (보강제에 따른 EPDM의 원적외선 가교 특성 연구)

  • Kim, J.S.;Lee, J.H.;Jung, W.S.;Bae, J.W.;Park, H.C.;Kang, D.P.
    • Elastomers and Composites
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    • v.44 no.1
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    • pp.47-54
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    • 2009
  • EPDM(Ethylene-propylene-diene-terpolymer) compound reinforced with carbon black having four different particle size, acetylene black(thermal conductivity carbon black), and silica were manufactured by internal mix and open mill. To investigate the effect of particle size of filler and filler type on far-infrared vulcanization, intermal temperature of compound, degree of curing, infrared spectroscopy, and thermal analysis were measured. The thermal conductivity of far-infrared vulcanized EPDM compound increased with increasing particle size of carbon filler, but hot air vulcanized EPDM compound is not affected by particle size. The thermal conductivity was increased in the order of carbon black < silica < acetylene black(thermal conductivity carbon black).

Effects of Cyclic Thermal Load on the Signal Characteristics of FBG Sensors Packaged with Epoxy Adhesives (주기적인 반복 열하중이 패키징된 FBG 센서 신호 특성에 미치는 영향)

  • Kim, Heonyoung;Kang, Donghoon
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.41 no.4
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    • pp.313-319
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    • 2017
  • Fiber optics sensors that have been mainly applied to aerospace areas are now finding applicability in other areas, such as transportation, including railways. Among the sensors, the fiber Bragg grating (FBG) sensors have led to a steep increase due to their properties of absolute measurement and multiplexing capability. Generally, the FBG sensors adhere to structures and sensing modules using adhesives such as an epoxy. However, the measurement errors that occurred when the FBG sensors were used in a long-term application, where they were exposed to environmental thermal load, required calibration. For this reason, the thermal curing of adhesives needs to be investigated to enhance the reliability of the FBG sensor system. This can be done at room temperature through cyclic thermal load tests using four types of specimens. From the test results, it is confirmed that residual compressive strain occurs to the FBG sensors due to an initial cyclic thermal load. In conclusion, signals of the FBG sensors need to be stabilized for applying them to a long-term SHM.

JAW RELATION WITH PERMANENT RECORD BASES IN THE EDENTULOUS PATIENTS (총의치 환자에 있어 Permanent record base를 이용한 악간관계 기록)

  • Heo, Yun-Seok;Shin, Sang-Wan
    • The Journal of Korean Academy of Prosthodontics
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    • v.33 no.2
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    • pp.231-239
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    • 1995
  • When the complete denture is made, the record base for jaw relation is divided into temporary record base and permanent record base. However, The temporary record base include some disadvantages such as, the lackness of intimate contact between model and base, the lackness of retention during the jaw relation registration, When we obtained jaw relation the permanent record bases made from heat curing resin were utilized. We could get several advantages as follows : 1. The permanent record base provided intimate contact between the model and record base. 2. In fabricating occlusal rim on record base, the dimensional change of record base was little because the permanent record base was lesser influenced to thermal change of occlusal rim than the temporary record base. 3. At the stage of jaw relation, the retention of final denture could be early checked. 4. It could be able to get more accurate registration of jaw relation because all procedure were done on the same base during the jaw relation, artificial teeth arrangement, try-in, and final denture construction. 5. Although there was an inconvenience due to double curing procedure, the shrinkage rate in resin polimerization was relatively reduced so that more dimensional stability could be taken.

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