• Bulletin of the Korean Chemical Society
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• 제22권2호
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• pp.241-243
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• 2001

• 한국산학기술학회논문지
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• 제3권3호
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• pp.161-165
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• 2002

게르마늄첨가 다성분계 산화물 유리를 제조하여 자외선(UV) 조사에 따른 유리의 미세 구조변화를 PL(photo-luminescence)과 ESR(electron spin resonance)을 이용하여 관찰하였다. 게르마늄 첨가량이 증가함에 따라 PL방사량은 증가하였으며, UV 조사 후에는 처음과 반대되는 광혹화 현상으로 감소하는 현상을 나타냈다. UV조사로 변화된 특성은 열처리를 통하여 회복이 가능하였으며, ESR 측정에서도 PL결과와 같은 광혹화 현상(phodarkenine effect)과 열표백화 현상(thermal bleaching effect)이 확인되었다. 또한, XRD 분석을 통하여 이러한 현상이 비정질 상은 그대로 유지하는 미세구조 변화임을 알 수 있었다.

• Journal of Ginseng Research
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• 제11권2호
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• pp.91-100
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• 1987

인삼(Panax ginseng C.A. Meyer) 엽소병에 대한 고사원인을 현상학적 측면에서 관찰, 분석한 결과 chlorohphyll의 bleaching현상은 적색광(660~700nm)에서 일어났으며, 청색광(400~500nm)에서는 광산화에 의한 bleaching현상이 일어나지 않았다. 엽소병에 의한 고사원인으로 대두되었던 환경요인 "온도"는 chlorohphyll의 bleaching현상에 전혀 영향을 미치지 않았다. 따라서 단순연소(simple burning)설은 본 실험을 통해 배재되었으며, 낮은 pH는 chlorohphyll의 bleaching속도를 가속화시켜 주었다. 엽소병에서 chlorohphyll의 bleaching현상을 유발시키는 1차적요인은 인삼잎의 독특한 구조적 차이에 의한 것이었다.

• Bulletin of the Korean Chemical Society
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• 제17권9호
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• pp.865-868
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• 1996

• 한국염색가공학회지
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• 제31권3호
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• pp.155-164
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• 2019

This study comparatively analyzed hair bleaching and degree of damage by the temperature of a heating tool after coloring hair with a permanent, semi-permanent or plant hair dye. According to analysis by spectrophotometer, 'semi-permanent hair dye' was the highest, followed by 'permanent hair dye' and 'plant hair dye' in terms of changes in $L^*$ values. In terms of changes in hair shape when analyzed using FE-SEM, 'semi-permanent hair dye($150^{\circ}C$ or lower)' was the greatest, followed by 'plant hair dye($180^{\circ}C$ or lower)' and 'permanent hair dye($200^{\circ}C$ or lower)'. Therefore, it is reasonable to flat iron hair at low temperature. According to the test, amino acid values gradually decreased in both bleached and colored hair. The results obtained through TGA-based thermal analysis confirmed that as brightness increases, hair moisture contents decrease. This study aimed to protect hair by suggesting a correct use of a flat iron by the hair dye type during hair coloring. It appears that the study results would help hairdressers minimize hair damage by using a hair dye at proper temperature.

• 한국염색가공학회지
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• 제8권2호
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• pp.35-42
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• 1996

Peroxodisulfates are being developed as low temperature bleaching agents for cotton fabrics to save the thermal energy. In this research we used the colar difference meter to determine the whiteness which peroxide booster will possibly make an effect on cotton fabric at the low temperature process using consist of temperature with different conditions agents, such as sodium hydroxide, sodium peroxodisulfate and potassium peroxodisulfate. The peroxide bleaching follows a laboratory experiments, using a statistical plan for three variables: the concentrations of hydrogen peroxide and sodium hydroxide and the temperature of bathing. The purpose of this research was to use the response surface analysis method to evaluate the relative importance of factors providing optimum whiteness. A ridge analysis of the data on whiteness response results in 3-D response surface diagrams for optimizing the concentrations of hydrogen peroxide and sodium hydroxide at about 42~52$^{\circ}C$.

• Restorative Dentistry and Endodontics
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• 제38권1호
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• pp.43-47
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• 2013

Objectives: The aim of this study was to determine an appropriate application duration of sodium ascorbate (SA) antioxidant gel in reducing microleakage of bonded composite restoration in intracoronally-bleached teeth. Materials and Methods: Eighty endodontically-treated human incisors were randomly divided into eight groups: control, no bleaching; IB and DB, immediate and delayed bonding after bleaching, respectively; S10m, S60m, S24h, S3d and S7d, bleaching + SA gel for 10 min, 60 min, 24 hr, 3 day and 7 day, respectively. For bleaching, a mixture of 30% hydrogen peroxide and sodium perborate was applied for 7 day. All access cavities were restored using One-Step adhesive (Bisco Inc.) and then Aelite LS Packable composite (Bisco Inc.). The bonded specimens were subjected to 500 thermal cycles, immersed in 1% methylene blue for 8 hr, and longitudinally sectioned. Microleakage was assessed with a 0 - 4 scoring system and analyzed using nonparametric statistical methods (${\alpha}$ = 0.05). Results: Group IB showed a significantly higher microleakage than the control group (p = 0.006) and group DB a statistically similar score to the control group (p > 0.999). Although groups S10m, S60m, and S24h exhibited significantly higher scores than group DB (p < 0.05), the microleakage in groups S3d and S7d was statistically similar to that in group DB (p = 0.771, p > 0.999). Conclusions: Application of SA gel for 3 day after nonvital bleaching was effective in reducing microleakage of composite restoration in intracoronally-bleached teeth.

• 한국세라믹학회지
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• 제37권3호
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• pp.219-226
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• 2000

Amorphous Ge20As20Se60 chalcogenide thin films were prepared by spin coating technique from mixed solutions of As40Se60 and Ge40Se60 dissolved in ethylenediamine. Films were prepared at a roating speed of 3500 rpm and spinning time was 10 second and heat-treateed at 27$0^{\circ}C$ for 1 hour. The resulting film thickness and RMS roughness were approximately 340 nm and 15$\AA$. Photostructure changes were investigated with 514.5nm Ar+ laser irradiation and heat-treatment. After Ar+ laser irradiation, transmittance and transmission efficiency decreased respectively up to 24.9% at 2.43 eV and 67.5% at 3.27 eV, and absorption edge shifted toward long wavelength. Optical bandgap changed from 2.03 to 1.83 eV, and absoprtion coefficient and absorption efficiency increased up to 0.33$\times$105cm-1 at 3.37eV and 88.3% at 1.31 eV, respectively. These photodarkening state were recovered reversibly by heat-treatment at 27$0^{\circ}C$ for 1 hour. Photodarkening and thermal bleaching effects by laser irradiation and heat-treatment revealed reversible amorphous-to-amorphous transition varying only coordination number.

• 한국응용과학기술학회지
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• 제32권3호
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• pp.363-371
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• 2015

n-Butanol and ethyl acetate extracts of thermal treatment yam (Dioscorea batatas $D_{ECNE.}$) belonging to the family Dioscoreaceae were measured for their radical scavenging activity and lipid peroxidation inhibition ability. In this study, ethyl acetate extract showed the most potent antioxidant activity evaluated by ferrous ion chelating activity and NO radical scavenging activity. Nevertheless, n-butanol extract was more effective in inhibiting linoleic acid peroxidation. A significant difference between n-butanol extract and ethyl acetate extract in nitrite scavenging activity ${\beta}$-carotene bleaching assays could not be found. Also, the results of this study showed that thermal treatment yam could be used as easily accessible source of natural antioxidants and as a possible food supplement.

• 한국전기전자재료학회논문지
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• 제15권5호
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• pp.435-440
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• 2002

In this study, we have investigated photo-induced changes of optical energy gap( $E_{OP)}$ and photoluminescence (PL) in amorphous ($\alpha$-) S $e_{100-x}$G $e_{x}$ (x=5, 25 and 33) thin films prepared by conventional thermal evaporation method. In the $\alpha$-S $e_{100-x}$G $e_{x}$ thin film, the $E_{OP}$ is obtained by a linear extrapolation of the ($\alpha$hν)$^{\frac{1}{2}}$ versus hν plot to the energy axis using the optical absorption coefficient ($\alpha$) calculated from the extinction coefficient k measured in the wavelength range of 290~900nm. Although the values of $\Delta$ $E_{OP}$ are very different, all films exhibit photo-induced photo-darkening (PD) effect that is a red shift of $E_{OP}$ . In particular, $\Delta$ $E_{OP}$ in $\alpha$-S $e_{75}$ G $e_{25}$ thin film exhibits the largest value (i, e., $\Delta$ $E^{OP}$ ~40meV for $\alpha$-S $e_{95}$ G $e_{5}$ , $\Delta$ $E_{OP}$ ~200meV for $\alpha$-S $e_{75}$ G $e_{25}$ , $\Delta$ $E_{OP}$ ~130meV for $\alpha$-S $e_{67}$ G $e_{33}$ ). PL spectra in $\alpha$-SeGe by hν$_{HeCd}$ have no-Stokes shift (SS) and show a tendency dependent on both composition and illumination time. We explain the energy-induced phenomena such as the PD and thermal bleaching, the native charged-defect generation and the no-SS PL, etc..the PD and thermal bleaching, the native charged-defect generation and the no-SS PL, etc..tc..