• Title/Summary/Keyword: Thermal and Metallurgical Behavior

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A Study on the Mechanical Properties of AC8A/$Al_2O_3$ Composites. (용탕단조법에 의한 AC8A/$Al_2O_3$ 복합재료의 기계적 성질에 관한 연구)

  • Kim, Ki-Bae;Kim, Kyoung-Min;Cho, Soon-Hyung;Yoon, Eui-Park
    • Journal of Korea Foundry Society
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    • v.11 no.6
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    • pp.475-481
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    • 1991
  • In this study the fabrication technology and mechanical properties of AC8A/$Al_2O_3$ Composites by squeeze casting process were investigated to develope for application as the piston materials that require good friction, wear resistance, and thermal stability. AC8A/$Al_2O_3$ composistes without a porosity and the break of preform were fabricated at the melt temperature of $740^{\circ}C$, the preform temperature of $500^{\circ}C$, and mold temperature of $400^{\circ}C$ under the applied pressure of $1200kg/cm^2$ as the results of the observation of microstructures. As the results of this study, the tensile strength of AC8A/$Al_2O_3$ composites was not increased linearly with $Al_2O_3$ volume fraction and so it seemed not to agree with the rule of mixture, which had been used often in metal matrix composite. Also the tensile strength after thermal fatigue test was little different from that before the test. Consequently it was thought that AC8A/$Al_2O_3$ composites fabricated under our experimental conditions had a good thermal stability and subsequently a good interface bonding. Wear rate(i.e., volume loss per unit sliding distance) of AC8A/$Al_2O_3$ composites was decreased with $Al_2O_3$ volume fraction and the sliding speed at both room temperature and $250^{\circ}C$ and so there was a good correlation between wear rate and hardness. Also the wear rate of AC/8A20% $Al_2O_3$ composities was obtained the value of $1.65cm^3/cm$ at sliding speed of 1.14m/sec as compared with about $3.0\;{\times}10^{-8}cm^3/cm$ hyereutectie Al-Si alloy(Al-16%Si-2%Cu-1%Fe-1%Ni), which applied presently for piston materials. The wear behavior of $Al_2O_3$ composites was observed to a type of abrasive wear by the SEM view of wear surface.

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Unidirectional Solidification of $Al-CuAl_2$ Eutectic Composites under Forced Convection by Vibration (진동하에서 일방향응고 시킨 $Al-CuAl_2$ 공정복합재료의 응고에 관한 연구)

  • Lee, Hyun-Kyu;Lee, Kil-Hong
    • Journal of Korea Foundry Society
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    • v.18 no.3
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    • pp.234-239
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    • 1998
  • Unidirectional solidification of $Al-CuAl_2$ eutectic composites was studied under the condition of forced convection by vibration. It has been shown that thermal gradient for solid is different from that for liquid during solidification under force convection by vibration. With increase of vibration, mobility of liquid increases, but decreases with decreasing vibration. The rate of solidification is very high initially, and decreases suddenly. For further solidification, the rate of solidification decrceases slowly, and shows a L-type behavior. The mechanical vibration during solidification effects efficiently on nucleation, and induces a forced convection in liquid. By the forced convection, great thermal gradient of liquid interface between solid and liquid can be obtained. The amount of solute near the interface also decreases as solute distribution is improved by the forced convection.

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Thermal Diffusion behavior of Al-Si Deposited Electrical Steels (Al-Si 합금 증착 전기강판의 열확산 거동)

  • Kim, C.W.;Cho, K.H.;Suk, H.G.
    • Journal of Surface Science and Engineering
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    • v.40 no.5
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    • pp.214-218
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    • 2007
  • The objective of this study is to evaluate the diffusion behavior of Al and Si from a coatings in the microstucture of Fe-Si steel. Steel samples deposited with Al-Si alloy are prepared by ion plating process, followed by annealing treatments for diffusion at $1050^{\circ}C$. Several intermetallic phases are found in the coatings and they are identified as Fe-Al and an orderd Fe-Si compounds. Series of different concentration profiles through the sample have been obtained and Si content reaches about 5 wt% in case of 90 minutes of diffusion time.

Solidification Characteristics of Squeeze Cast Al Alloy Composites (Squeeze Cast한 Al기지 금속복합재료의 응고거동)

  • Kim, Dae-Up;Kim, Jin;Park, Ik-Min
    • Journal of Korea Foundry Society
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    • v.11 no.3
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    • pp.208-216
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    • 1991
  • The solidification behavior of the squeeze cast composites of aluminum alloys reinforced with boron fiber($100{\mu}m$) and silicon carbide fibers($140{\mu}m$ and $15{\mu}m$) were investigated. Al-4.5wt%Cu and Al-l0wt%Mg were chosen for the matrix phase of the composites. In the squeeze cast specimen with high thermal difference between fiber and melt, the average secondary dendrite arm spacing(DAS) in reinforced alloy is smaller than that in unreinforced alloy. It was also observed that primary ${\alpha}$ and non-equilibrium eutectic, which seems to be penetrated and solidified at the final stage of the solidification of the matrix, are irregularly distributed around fibers. It is considered that cold fibers serve as heterogeneous nucleation site. While in the remelted and resolidified specimen without temperature difference, the DAS was not changed with reinforcement and microstructure reveals non-equilibrium eutectic with relatively uniform thickness around fibers. It might be evident the nucleation starts at interfiber region. Microsegregation decreases with the decrease in cooling rate and with reinforcement in the as-squeeze cast specimen. Al-10wt% Mg alloy shows less microsegregation than Al-4.5wt%Cu alloy.

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Effect of Si and Ca Addition on the Strengthening Behavior of Gravity-cast AM60 Magnesium Alloys (중력주조 AM60 마그네슘 합금의 강화 거동에 미치는 Si 및 Ca 첨가영향)

  • Kim, Jae-Woo;Kim, Do-Hyang;Shin, Kwang-Seon
    • Journal of Korea Foundry Society
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    • v.18 no.4
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    • pp.364-372
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    • 1998
  • Effects of Si and Ca additions on the mechanical properties of AM60 based Mg alloys have been investigated. Hardness of the AM60 based Mg alloys reached a maximum value after aging for approximately 33 hours but the amount of hardness increase was negligible. The poor age hardening response of the alloys was due to low Al content, which implies that Al content must be >6 wt.% to observe age hardening effect. The tensile and yield strength increased with increasing Al, Si, and Ca content but elongation decreased with increasing Al and Si content. The best mechanical properties obtained in AM 40-2.5Si-0.2Ca alloy after T4 heat treatment were as follows; tensile strength 193.4 MPa, yield strength 79.2 MPa, and elongation 11.2%. High temperature property obtained from creep test was also improved by introducing $Mg_2Si$ which has high hardness, high melting temperature and low thermal expansion coefficient.

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Oxidation Behavior at the Interface between E-beam Coated $ZrO_{2}$-7wt.%$Y_{2}O}_{3}$and Plasma Sprayed CoNiCrAlY (전자빔 코팅 및 플라즈마 용사에 의한 안정화지르코니아/CoNiCrAlY 계면의 산화거동)

  • Choi, Won-Seop;Kim, Young-Do;Jeon, Hyeong-Tag;Kim, Hyon-Tae;Yoon, Kook-Han;Hong, Kyung-Tae;Park, Jong-Ku;Park, Won-Sik
    • Korean Journal of Materials Research
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    • v.8 no.6
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    • pp.538-544
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    • 1998
  • The spallation of a thermal barrier coating layer depends on the formation of brittle spinels. thermal expansion mismatch between ceramic and metal. the phase transformation of a ceramic layer and residual stress of coating layer. In this work. the formation mechanism of oxide scale formed by oxidation treatment at 90$0^{\circ}C$ was investigated in order to verify oxidation behavior at the interface between E-beam coated $Zr0_2$-7wt.% $Y_20_3$ and plasma sprayed CoNiCrAIY. Some elements distributed in the bond coating layer were selectively oxidized after oxidation. At the initial time of oxidation. AI-depletion zone and $\alpha$-$Al_O_3$,O, were formed at the bond coating layer by the AI-outward diffusion. After layer grew until critical thickness. spinels. $Cr_20$, and $C0_2CrO_4$ by outward diffusion of Co. Cr, Ni were formed. It was found that the formation of spinels may be related to the spallation of $Zr0_2$-7wt.% $Y_20_3$ during isothermal oxidation.

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Influence of Welding Residual Stress on the Mechanical Behavior of Externally Loaded Dissimilar SS400-STS304 Steel Weldment (SS400-STS304 이재용접부의 외력작용시 용접잔류응력 특성)

  • Bang, Hee-Seon;Bang, Han-Sur;Kim, You-Chul;Joo, Sung-Min;Joa, Soon-Won;Ro, Chan-Seoung
    • Journal of Welding and Joining
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    • v.27 no.5
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    • pp.34-41
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    • 2009
  • Thermal and mechanical characteristics in dissimilar SS400-STS304 steel weldment have been investigated by 3D thermal elastic-plastic analysis. Moreover, the influence of welding residual stresses on the mechanical behaviour of this welded joint, by applying superimposed external load (tension load) was determined. The residual stresses obtained by numerical simulation were compared with the experimentally measured results. The FE results were in good agreement with the measured values. The mechanical test (hardness, tensile test) and metallurgical analysis was carried out to ensure the weld integrity. Hence, possibility of applying SS400-STS304 dissimilar steels in industries has been established.

Analysis of Thermal Behavior and Temperature Estimation by using an Observer in Drilling Processes (드릴링 공정의 열거동 해석과 관측기를 이용한 온도 추정법)

  • Kim, Tae-Hoon;Chung, Sung-Chong
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.27 no.9
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    • pp.1499-1507
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    • 2003
  • Physical importance of cutting temperatures has long been recognized. Cutting temperatures have strongly influenced both the tool life and the metallurgical state of machined surfaces. Temperatures in drilling processes are particularly important, because chips remain in contact with the tool for a relatively long time in a hole. Tool temperatures tend to be higher in drilling processes than in other in machining processes. This paper concerns with modeling of thermal behaviors in drilling processes as well as estimation of the cutting temperature distribution based on remote temperature measurements. One- and two-dimensional estimation problems are proposed to analyze drilling temperatures. The proposed thermal models are compared with solutions of finite element methods. Observer algorithms are developed to solve inverse heat conduction problems. In order to apply the estimation of cutting temperatures, approximation methods are proposed by using the solution of the finite element method. In two-dimensional analysis, a moving heat source according to feedrate of the drilling process is regarded as a fixed heat source with respect to the drilling location. Simulation results confirm the application of the proposed methods.

The Effect of Calcium on Microstructure of AZ61 Magnesium Alloy during Annealing Heat Treatment (AZ61 마그네슘 합금의 어닐링 중 Ca의 첨가에 따른미세조직 변화에 미치는 영향)

  • Kim, Kibeom;Jeon, Joonho;Kim, Kwonhoo
    • Journal of the Korean Society for Heat Treatment
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    • v.34 no.2
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    • pp.53-59
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    • 2021
  • Due to high specific strength and low density, AZ series magnesium alloys have been receiving high interest as a lightweight material. However, their industrial application is limited due to the phenomenon that the strength decreases at elevated temperature by the occurrence of softening effect because of the Mg17Al12 phase decomposition. To solve this problem, many research were conducted to increase the high-temperature strength by forming a thermal stable second-phase component by adding new elements to the AZ magnesium. Especially, adding Ca to AZ magnesium has been reported that Ca forms the new second-phase. However, studies about the analysis of decomposition or precipitation temperature, formation composition, and components to understand the formation behavior of these precipitated phases are still insufficient. Therefore, the effect of Ca addition to AZ61 on the phase change and microstructure of the alloy during annealing was investigated. As a result of analysis of the initial and heat-treated specimen, AZ61 formed α-Mg matrix and precipitated phase of Mg17Al12, and AZX611 formed one more type of precipitated phase, Al2Ca. Also, Al2Ca was thermal stable at high temperatures. And after annealing, the laves phase was decomposed to under 10 ㎛ size and distributed in matrix.

Investigation of field emission mechanism of undoped polyucrystalline diamond films

  • Shim, Jae-Yeob;Chi, Eung-Joon;Song, Kie-Moon;Baik, Hong-Koo
    • Proceedings of the Korean Vacuum Society Conference
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    • 1999.07a
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    • pp.62-62
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    • 1999
  • Carbon based materials have many attractive properties such as a wide band gap, a low electron affinity, and a high chemical and mechanical stability. Therefore, researches on the carbon-based materials as field emitters have been drawn extensively to enhance the field emission properties. Especially, diamond gives high current density, high current stability high thermal conductivity durable for high temperature operation, and low field emission behaviors, Among these properties understanding the origin of low field emission is a key factor for the application of diamond to a filed emitter and the verification of the emission site and its distribution of diamond is helpful to clarify the origin of low field emission from diamond There have been many investigations on the origin of low field emission behavior of diamond crystal or chemical vapor deposition (CVD) diamond films that is intentionally doped or not. However, the origin of the low field emission behavior and the consequent field emission mechanism is still not converged and those may be different between diamond crystal and CVD diamond films as well as the diamond that is doped or not. In addition, there have been no systematic studies on the dependence of nondiamond carbon on the spatial distribution of emission sites and its uniformity. Thus, clarifying a possible mechanism for the low field emission covering the diamond with various properties might be indeed a difficult work. On the other hand, it is believed that electron emission mechanisms of diamond are closely related to the emission sites and its distributions. In this context, it will be helpful to compare the spatial distribution of emission sites and field emission properties of the diamond films prepared by systematic variations of structural property. In this study, we have focused on an understanding of the field emission variations of structural property. In this study, we have focused on an understanding of the field emission mechanism for the CVD grown undoped polycrystalline diamond films with significantly different structural properties. The structural properties of the films were systematically modified by varying the CH4/H2 ratio and/or applying positive substrate bias examined. It was confirmed from the present study that the field emission characteristics are strongly dependent on the nondiamond carbon contents of the undoped polycrystalline diamond films, and a possible field emission mechanism for the undoped polycrystalline diamond films is suggested.

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