• 폴리머
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• 제24권3호
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• pp.358-365
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• 2000

Miscibility itnd thermal behavior of blends of synthetic biodegradable aliphatic polyester (Bionolle) with poly(epichlorohydrin) (PECH) were investigated by a differential scanning calorimetry (DSC), a dynamic mechanical thermal analyzer (DMTA) and a rotational rheometer. Observed both single glass transition temperatures from the DSC in agreement with the Fox equation and single T$_{g}$ changes as a function of composition from the DMTA indicate that these blend mixtures are miscible. In addition, the miscibility of this blend system was also observed from the single curve of the Cole-Cole Plot of log G′($\omega$) vs. log C"($\omega$) from the dynamic test using a rotational rheometer. This was further verified from the cryogenically fractured surface of BDP/PECH blends by scanning electron microscopy.

• 식품과학과 산업
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• 제53권3호
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• pp.256-263
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• 2020

Milk pasteurization is used to destroy harmful bacteria present in the raw milk for improvement of the keeping quality of dairy products. It is generally carried out in dairy industries as the heating process of raw milk in properly designed and operated equipment to a specific temperature for a specified a specified period. However, thermal processing may cause quality changes in milk as well as significant nutritional losses. Hence, many researchers have started work to design alternative strategies to produce safer foods with minimal thermal treatments for pasteurization. Therefore, the present paper shows the current status of commercial pasteurization system of dairy products in korean industry and the research efforts carried out by researchers on novel milk pasteurization system that could be an alternative to traditional thermal processes for maintaining the freshness of dairy products.

• Journal of Industrial and Engineering Chemistry
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• 제67권
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• pp.1-11
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• 2018

Polymer composites offered broad engineered applications, however their diversity get restricted owing to fluctuations in thermomechanical properties during heating or cooling hence great concern required prior their applications through thermomechanical analysis (TMA). Traditionally, TMA or dilatometry found to be simple, ideal, reliable, sensitive, excellent and basic thermal analytical technique. TMA provides valuable information on thermal expansion, glass transitions temperature (Tg), softening points, composition and phase changes on material of having different geometries simply by applying a constant force as a function of temperature. This compilation highlights the basics and experimental of TMA for both research and technical applications and also provide literature on TMA of polymers, hybrid composites, nanocomposites and their diverse applications.

• Structural Engineering and Mechanics
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• 제82권6호
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• pp.701-711
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• 2022

The nonlocal elasticity as well as Mindlin's first-order shear deformation plate theory are proposed to investigate thermal vibrational of a nanoplate placing on a three-factor foundation. The Winkler-Pasternak elastic foundation is connected with the viscous damping to obtain the present three-parameter viscoelastic model. Differential equations of motion are derived and resolved for simply-supported nanoplates to get their natural frequencies. The influences of the nonlocal index, viscous damping index, and temperature changes are investigated. A comparison example is dictated to validate the precision of present results. Effects of other factors such as aspect ratio, mode numbers, and foundation parameters are discussed carefully for the vibration problem. Additional thermal vibration results of nanoplates resting on the viscoelastic foundation are presented for comparisons with future investigations.

• Applied Microscopy
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• 제50권
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• pp.12.1-12.11
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• 2020

Hot stage microscopy (HSM) is a thermal analysis technique that combines the best properties of thermal analysis and microscopy. HSM is rapidly gaining interest in pharmaceuticals as well as in other fields as a regular characterization technique. In pharmaceuticals HSM is used to support differential scanning calorimetry (DSC) and thermo-gravimetric analysis (TGA) observations and to detect small changes in the sample that may be missed by DSC and TGA during a thermal experiment. Study of various physical and chemical properties such sample morphology, crystalline nature, polymorphism, desolvation, miscibility, melting, solid state transitions and incompatibility between various pharmaceutical compounds can be carried out using HSM. HSM is also widely used to screen cocrystals, excipients and polymers for solid dispersions. With the advancements in research methodologies, it is now possible to use HSM in conjunction with other characterization techniques such as Fourier transform infrared spectroscopy (FTIR), DSC, Raman spectroscopy, scanning electron microscopy (SEM) which may have additional benefits over traditional characterization techniques for rapid and comprehensive solid state characterization.

• 한국전기전자재료학회논문지
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• 제37권4호
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• pp.439-444
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• 2024

This study investigates the post-thermal treatment effects on the efficiency of silicon heterojunction solar cells, specifically examining the influence of annealing on p-type microcrystalline silicon oxide and ITO thin films. By assessing changes in carrier concentration, mobility, resistivity, transmittance, and optical bandgap, we identified conditions that optimize these properties. Results reveal that appropriate annealing significantly enhances the fill factor and current density, leading to a notable improvement in overall solar cell efficiency. This research advances our understanding of thermal processing in silicon-based photovoltaics and provides valuable insights into the optimization of production techniques to maximize the performance of solar cells.

• 한국재료학회지
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• 제16권5호
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• pp.292-296
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• 2006

Effects of rapid thermal annealing of bismuth telluride thin films on their thermoelectric properties were investigated. Films with four different compositions were elaborated by co-sputtering of Bi and Te targets. Rapid thermal treatments in range of $300{\sim}400^{\circ}C$ were carried out during 10 minutes under the reducing atmosphere (Ar with 10% $H_2$). As the temperature of thermal treatment increased, carrier concentrations of films decreased while their mobilities increased. These changes were clearly observed for the films close to the stoichiometric composition. Rapid thermal treatment was found to be effective in improving the thermoelectric properties of $Bi_2Te_3$ films. Recrystallization of $Bi_2Te_3$ phase has caused the enhancement of thermoelectric properties, along with the decrease of the carrier concentration. Maximum values of Seebeck coefficient and power factor were obtained for the films treated at $400^{\circ}C$ (about $-128{\mu}V/K$ and $9{\times}10^{-4}\;W/K^2m$, respectively). With further higher temperature ($500^{\circ}C$), thermoelectric properties deteriorated due to the evaporation of Te element and subsequent disruption of film's structure.

• 설비공학논문집
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• 제28권7호
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• pp.293-298
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• 2016

A three-dimensional (3D) numerical model of the vertical ground-coupled heat exchanger is useful for analyzing the modern ground source heat pump system. Furthermore, a detailed description of the inner side of the exchanger allows to account for the effects of the thermal capacity. Thus, both methods are included in the proposed numerical model. For the ground portion, a FDM (Finite Difference Method) scheme has been applied using the Cartesian coordinate system. Cylindrical grids are applied for the borehole portion, and the U-tube configuration is adjusted at the grid, keeping the area and distance unchanged. Two sub-models are numerically coupled at each time-step using an iterative method for convergence. The model is validated by a reference 3D model under a continuous heat injection case. The results from a periodic heat injection input show that the proposed thermal capacity model reacts more slowly to the changes, resulting in lower borehole wall temperatures, when compared with a thermal resistance model. This implies that thermal capacity effects may be important factors for system controls.

• 한국해양공학회지
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• 제19권6호통권67호
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• pp.64-71
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• 2005

The welding methods have been applied to the most structural products used in the automobile, ship construction, and construction. The structure steel must have sufficient strength of structure; However, the mechanical properties of the welded part changes when it is welded. Therefore, the stability or life of the structure may be affected by the changed mechanical properties. The mechanical properties of the welded part must be examined in order to ensure the safety of structure. In this research, the SS400 steel and the STS304 steel were used to estimate the mechanical properties of the HAZ by weld thermal cycle simulation. In this study, the materials were used to examine the weld thermal cycle simulation characteristic, under two conditions: the drawing with diameter of $\Phi$10 and the residual stress removal treatment. To examine the mechanical properties by the weld thermal cycle simulation, the tensile test was carried out in room temperature. The crosshead speed was lmm/min.

• 한국가구학회지
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• 제27권2호
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• pp.122-127
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• 2016

The increasing interest in the environment and climate change around the globe, while the importance of building energy saving is increasing. The building energy simulation program is used for evaluating of energy performance of buildings. However, an input value of wood thermal conductivity in the programs is different from each other. Therefore, in this study, wood thermal conductivity was measured according to species. Through construction database by species of wood, the error of simulation program are able be decreased. In addition, if used as a structural and interior of buildings, the thermal conductivity and moisture of the wood is difficult to apply to the program because they were changed according to the occupant's lifestyle. In this paper, thermal conductivity and moisture content.of wood confirmed changes in the constant temperature and relative humidity ($25^{\circ}C$, 50% R.H.) condition.