• Title/Summary/Keyword: Temperature hardening

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Study on Low Temperature Curing Emulsion of PLA Fiber for Bedding (침장용 PLA 섬유에 대한 저온 경화유제에 관한 연구)

  • Ahn, Young-Moo
    • Journal of Fashion Business
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    • v.16 no.1
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    • pp.41-51
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    • 2012
  • Polyester is mainly used as a bedding filler material. PLA fiber as an eco-friendly material for substituting polyester has a low melting temperature and therefore a hardening process is impossible. This study is to develop the oil for feather touch that can treat at the melting temperature of PLA. The slippery and soft aminosilicone emulsion, and the bulky epoxysilicone emulsion were used. They had proper viscosity and particle size for flexibility and elasticity. When using methoxy aminosilane [$H_2NSi(OCH_3)_3$] as an aminosilane and [$Zn(OCOCH_3)_2$] as a catalyst, the hardening reaction was fast and effective. Feather touch process were treated by 2 steps. At first step, aminosilicone emulsion, epoxysilicone emulsion and methylaminosilane were mixed and homogenized, and at second step, 5% blened solution of the first step, Zn catalyst 1%, distilled water 94% were treated at PLA fiber. After treatment the static friction coefficient and dynamic friction coefficient were reduced to 23.5-60.8% and 30.0-61.3% respectively, and the laundry and sun light fastnesses have not shown any decrease.

Prediction on Flow Stress Curves and Microstructure of 304 Stainless Steel (304 스테인리스강이 고온 유동응력곡선과 미세 조직의 예측)

  • 한형기;유연철;김성일
    • Transactions of Materials Processing
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    • v.9 no.1
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    • pp.72-79
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    • 2000
  • Dynamic recrystallization (DRX), which may occur during hot deformation, is important for the microsturctural evolution of 304 stainless steel. Especially, the current interest in modelling hot rolling demands quantitative relationships among the thermomechanical process variables, such as strain, temperature, strain rate, and etc. Thus, this paper individually presents the relationships for flow stress and volume fraction of DRX as a function of processing variables using torsion tests. The hot torsion tests of 304 stainless steel were performed at the temperature range of 900~110$0^{\circ}C$ and the strain rate range of 5x10-2~5s-1 to study the high temperature softening behavior. For the exact prediction of flow stress, the equation was divided into two regions, the work hardening (WH) and dynamic recovery (DRV) region and the DRX region. Especially, The flow stress of DRX region could be expressed by using the volume fraction of DRX (XDRX). Since XDRX was consisted of the critical strain($\varepsilon$c) for initiation of dynamic recrystallization (DRX) and the strain for maximum softening rate ($\varepsilon$*), that were related with the evolution of microstructure. The calculated results predicted the flow stress and the microstructure of the alloy at any deformation conditions well.

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Analysis of the Strength Property for TiC-Mo Composites at High Temperature

  • Shin, Soon-Gi
    • Korean Journal of Materials Research
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    • v.24 no.4
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    • pp.201-206
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    • 2014
  • TiC-21 mol% Mo solid solution (${\delta}$-phase) and TiC-99 mol% Mo solid solution (${\beta}$-phase), and TiC-(80~90) mol% Mo hypo-eutectic composite were deformed by compression in a temperature range from room to 2300 K and in a strain rate range from $4.9{\times}10^{-5}$ to $6.9{\times}10^{-3}/s$. The deformation behaviors of the composites were analyzed from the strengths of the ${\delta}$- and ${\beta}$-phases. It was found that the high strength of the eutectic composite is due primarily to solution hardening of TiC by Mo, and that the ${\delta}$-phase undergoes an appreciable plastic deformation at and above 1420 K even at 0.2% plastic strain of the composite. The yield strength of the three kinds of phase up to 1420 K is quantitatively explained by the rule of mixture, where internal stresses introduced by plastic deformation are taken into account. Above 1420 K, however, the calculated yield strength was considerably larger than the measured strength. The yield stress of ${\beta}$-phase was much larger than that of pure TiC. A good linear relationship was held between the yield stress and the plastic strain rate in a double-logarithmic plot. The deformation behavior in ${\delta}$-phase was different among the three temperature ranges tested, i.e., low, intermediate and high. At an intermediate temperature, no yield drop occurred, and from the beginning the work hardening level was high. At the tested temperature, a good linear relationship was held in the double logarithmic plot of the yield stress against the plastic strain rate. The strain rate dependence of the yield stress was very weak up to 1273 K in the hypo-eutectic composite, but it became stronger as the temperature rose.

Effect of Microstructural Factors on the Strength and Deformability of Ferrite-Pearlite Steels with Different Mn and V Contents (Mn 및 V 함량이 다른 페라이트-펄라이트 조직강의 강도와 변형능에 미치는 미세조직 인자의 영향)

  • Hong, Tae-Woon;Lee, Sang-In;Shim, Jae-Hyeok;Lee, Junho;Lee, Myoung-Gyu;Hwang, Byoungchul
    • Korean Journal of Materials Research
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    • v.28 no.10
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    • pp.570-577
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    • 2018
  • This study examines the effect of microstructural factors on the strength and deformability of ferrite-pearlite steels. Six kinds of ferrite-pearlite steel specimens are fabricated with the addition of different amounst of Mn and V and with varying the isothermal transformation temperature. The Mn steel specimen with a highest Mn content has the highest pearlite volume fraction because Mn addition inhibits the formation of ferrite. The V steel specimen with a highest V content has the finest ferrite grain size and lowest pearlite volume fraction because a large amount of ferrite forms in fine austenite grain boundaries that are generated by the pinning effect of many VC precipitates. On the other hand, the room-temperature tensile test results show that the V steel specimen has a longer yield point elongation than other specimens due to the highest ferrite volume fraction. The V specimen has the highest yield strength because of a larger amount of VC precipitates and grain refinement strengthening, while the Mn specimen has the highest tensile strength because the highest pearlite volume fraction largely enhances work hardening. Furthermore, the tensile strength increases with a higher transformation temperature because increasing the precipitate fraction with a higher transformation temperature improves work hardening. The results reveal that an increasing transformation temperature decreases the yield ratio. Meanwhile, the yield ratio decreases with an increasing ferrite grain size because ferrite grain size refinement largely increases the yield strength. However, the uniform elongation shows no significant changes of the microstructural factors.

Effect of Final Annealing Temperature on Microstructure and Creep Characteristics of Nb-containing Zirconium Alloys (Nb 첨가 Zr 합금의 미세조직과 Creep 특성에 미치는 마지막 열처리 온도의 영향)

  • Park, Yong-Gwon;Yun, Yeong-Gwon;Wi, Myeong-Yong;Kim, Taek-Su;Jeong, Yong-Hwan
    • Korean Journal of Materials Research
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    • v.11 no.10
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    • pp.879-888
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    • 2001
  • The effects of final annealing temperature on the microstructure and creep characteristics were investigated for the Zr-lNb-0.2X (X=0, Mo, Cu) and Zr-lNb- 1Sn-0.3Fe-0.1X (X=0, Mo, Cu) alloys. The microstructures were observed by using TEM/EDS, and grain size and distributions of precipitates were analyzed using a image analyzer. The creep test was performed at $400^{\circ}C$ under applied stress of 150 MPa for 10 days. The $\beta$-Zr was observed at annealing temperature above $600^{\circ}C$. In the temperature above$ 600^{\circ}C$, the grain sizes of both alloy systems appeared to be increased with increasing the final annealing temperature. The creep strengths of Zr-1Nb-1Sn-0.3Fe-0.1X alloys were higher than those of Zr-1Nb-0.2X ones due to the effect of solid solution hardening by Sn in Zr-lNb-lSn-0.3Fe-0.1X alloy system. Also, Mo addition showed the strong effect of precipitate hardening in both alloy systems. The creep strength rapidly decreased with increasing the annealing temperature up to $600^{\circ}C$. However, a superior creep resistance was obtained in the sample that annealed to have a second phase of $\beta$-Zr. It was considered that the appearance of $\beta$-Zr would play an important role in the strengthening mechanism of creep deformation.

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A Experimental Study on High Temperature Tensile Property of High Strength Steel (고강도강재의 고온인장특성에 관한 실험적 연구)

  • 장경호;이진형;신영의
    • Proceedings of the KWS Conference
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    • 2003.05a
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    • pp.260-262
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    • 2003
  • In this study, high temperature tensile properties of high tensile strength steels(POSTEN60, POSTEN80) were investigated by elevated temperature tensile test. According toe the results, high temperature tensile strength of POSTEN60 deteriorated slowly to 100$^{\circ}C$. As the temperature went up the tensile strength became better because of blue shortness and it deteriorated radically after reached to the maximum value around 300$^{\circ}C$. For the POSTEN80, high temperature tensile strength deteriorated slowly to 200$^{\circ}C$.As the temperature went up the tensile strength became better and it deteriorated slowly to 600$^{\circ}C$ after reached to the maximum value around 300$^{\circ}C$. Strain of high tensile strength steels at the elevated temperature increased radically after the mercury rose to 600$^{\circ}C$. The strain hardening ratio of POSTEN60 was larger then that of POSTEN80 at the elevated temperature as in the case at the room temperature and it became smaller radically after the mercury rose to 400$^{\circ}C$.

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An Economic Mix Design Methodology for the Development of Concrete Strength at Low Temperature (저온에서의 콘크리트 강도 확보를 위한 경제적 배합 방안)

  • Kim, Sang-Chel;Kim, Yong-Jic;Kim, Young-Jin
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.7 no.4
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    • pp.95-103
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    • 2012
  • Precast concrete method is known to have advantages of minimizing works in the construction, controlling concrete quality easily and saving construction period due to only fabrication work in the construction field, but it needs to apply steam curing to accelerate early concrete strength. In the meanwhile, the oil cost for steam curing has been continuously increased because of political instability in the middle East and international economic shaky. Thus, this study addresses the development of precast/ prestressed concrete which has over 14MPa at 1 day age and specified concrete strength of 40MPa at low temperature, not applying steam curing. Tests were carried out in terms of material characteristics in fresh concrete and compressive strength using 3 types of cement such as Type I, Type III and rapid hardening compound cement. As results of tests, it is found that cements for rapid hardening had disadvantages with respect to slump, slump loss, and air content, but showed higher compressive strength than specified one, especially the highest value when using rapid hardening compound.

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The Effects of Various Reaction Conditions on Trans Isomer Formation in Hydrogenating Edible Soybean Oil (식용(食用) 대두유(大豆油) 경화시(硬化時) 반응조건(反應條件)이 이성체(異性體) 생성(生成)에 미치는 영향(影響))

  • Choi, Eok;Joo, Hyun-Kyu;Lee, Si-Kyung
    • Korean Journal of Food Science and Technology
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    • v.27 no.2
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    • pp.205-209
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    • 1995
  • Edible hardened soybean oil is processed by hydrogenation of refined soybean oil in order to upgrade the heat and oxidation stability and to improve flavor and physical nature. This study aims to investigate the influences of various reaction conditions on iodine value, fatty acid composition and trans isomer formation in hydrogenating soybean oil. In case that hardening temperature is $180^{\circ}C$, trans acid formation increased by 6.2 times more under $3.0{\;}kg/cm^{2}H_{2}$ than under $0.5{\;}kg/cm^{2}H_{2}$, while linolenic acid decreased in contents. In case of $200^{\circ}C$ of hardening temperature trans acid formation showed 4.6% higher under $0.5{\;}kg/cm^{2}H_{2}$ than under $3.0{\;}kg/cm^{2}H_{2}$ while contents of linolenic and linoleic acids showed 0.51% and 2.5% lower respectively. It is concluded that $200^{\circ}C$ of hardening temperature under 0.5 and $3.0{\;}kg/cm^{2}H_{2}$ is better condition because trans isomers are little produced, and iodine value and linolenic acid content decreased in hardening soybean oil.

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Effect of Hardening of Granulated Blast Furnace Slag on the Liquefaction Strength (고로 수쇄슬래그의 경화가 액상화 강도에 미치는 영향)

  • Baek, Won-Jin
    • Journal of the Korean Geotechnical Society
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    • v.22 no.8
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    • pp.99-106
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    • 2006
  • In the present study, in order to clarify the effects of latent hydraulic property of granulated blast furnace slag (GBF slag) on the liquefaction, GBF slag was cured in the high temperature alkali water (adding the calcium hydroxide, pH=12, water temperature is about $30^{\circ}C$), and then the cyclic and the static tri-axial compression tests were carried out. Then the results were compared with those for Japanese standard sand of Toyoura sand and natural sand of Genkai sand. From the test results, it is clarified that the liquefaction strength of the GBF slag increases with the increase of the curing period by the hardening due to the latent hydraulic property. It is also shown that GBF slag with Dr=50% and 80% which was cured for 189 days in the fresh-water shows cohesion due to developing of latent hydraulic property. In addition, as for the liquefaction strength of GBFS during the hardening process, a linear relation between the cyclic stress ratio $R_{20}$ at the number of stress cycles Nc=20 and cohesion $C_{d}$ was observed. It is also clarified that the liquefaction strength for cured GBF slag in the high temperature alkali water is predicted by the cohesive strength or the unconfined compressive strength.

A Study on Trend of Tensile Properties with Ratio of Water Mixture in Hydroponic Polyurethane Waterproofing Materials (수경화성 폴리우레탄 방수재의 물 혼입량에 따른 인장성능 변화 추이 연구)

  • Park, Wan-Goo;An, Hyun-Ho;Kim, Sun-Do;Kim, Dong-Bum;Park, Jin Sang;Oh, Sang-Keun
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2016.05a
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    • pp.215-216
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    • 2016
  • Urethane waterproofing materials which currently being used most commonly in the Korean domestic market have high applicability and construct layers without forming any joints, but under the influence of low temperature and low humidity, as well as the thickness of the applied layer, the curing time of this material may become extended in construction sites. To resolve these issues, a proposed method of using water-hardening type of polyurethane waterproofing materials are being developed. However, there currently lacks any standards or evaluation methods on determining an optimal mixture ratio of water for the water-hardening polyurethane waterproofing materials. Therefore, for the establishment of a board applicability of the water-hardening polyurethane waterproofing methods in construction sites, this study objectively analyzes the changes in the performance of these materials depending on the changes of the water mixture ratio and attempts to procure the optimal ratio on the basis of forming a provisionary standard.

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