• Journal of the Korean Society of Safety
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• v.4 no.1
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• pp.25-39
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• 1989

Cyclic temperature creep tests were carried out an AS 7075 alloy specimens were subjected to a constant load and stepwise temperature cycles in which temperature was fluctuated between 30$0^{\circ}C$ and 25$0^{\circ}C$ with three different cycle ratios. The highest frequency of cycling was 1 cycle per 10 hr and the lowest one was 1 cycle per 12 hr. From the creep experimental results with the above conditions the creep strain under cyclic temperature can be predicted easily by introd ucing the equivalent steady temperature because defined by Eq.(16), but the rupture life is 1.1 time than those of constant temperature because of effect of temperature history at tertiary creep range. Besides thlis result, the results of the creep test under cyclic temperature conditions are respectively compayiea with calculated rupture lives using the life fraction law and Eq.(18). The agreement between the obseried rupture times and calculated ones is fairly good. So creep rupture lives can be respectively predicted using life fraction law and Eq.(18).

• Journal of the Microelectronics and Packaging Society
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• v.15 no.2
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• pp.55-61
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• 2008

This paper shows quantitative reliability evaluations of a Bluetooth module through extending previous qualitative methods limited to structure reliability tests and solder joint reliability tests for Bluetooth modules. Accelerated Life Testing (ALT) of the modules using temperature difference in temperature cycling as an accelerated stress was conducted for quantitative reliability evaluation under field environment conditions. Lifetime distribution parameters were estimated using the failure times obtained through the ALT, and then Coffin-Manson model was implemented. Results of the ALT showed that the failure mode of the modules was open and the failure mechanisms are both crack and delamination. The ALT reproduced the failure mode and mechanisms of failed Bluetooth modules collected from the field. Further, a quantitative reliability evaluation method with respect to various temperature differences in temperature cycling was proposed in this paper. $B_{10}$ lifetime of the module for the temperature difference $70^{\circ}C$ using the proposed method would be estimated as about 4 years.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2003.10a
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• pp.115-118
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• 2003

This research aims to measure mechanical tensile properties of CFRP composites for cryogenic tank material. Through the cryogenic chamber, tensile tests are peformed under cryogenic temperature for graphite/epoxy fabric specimen aged at $-150^{\circ}C$ for 30hrs with load and graphite/epoxy unidirectional specimen 3-cycled from RT to $-100^{\circ}C$ with load. For graphite/epoxy fabric specimen, tensile modulus showed to increase after aging at cryogenic temperature(CT) while to decrease after aging at room temperature(RT) and tensile strength is more decreased after CT-aged than at RT-aged. For graphite/epoxy unidirectional specimen, tensile modulus was almost not changed after 3-cycling but strength showed the trend of decrease as increase the number of cycling.

• Journal of Electrochemical Science and Technology
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• v.8 no.3
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• pp.197-205
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• 2017

Lead dioxide thin films were electrodeposited on nickel substrate from acidic lead nitrate solution. Current efficiency and thickness measurements, cyclic voltammetry, AFM, SEM, and X-ray diffraction experiments were conducted on $PbO_2$ surface to elucidate the effect of lead nitrate concentration, current density, temperature on the morphology, chemical behavior, and crystal structure. Experimental results showed that deposition efficiency was affected by the current density and solution concentration. The film thickness was independent of current density when deposition from high $Pb(NO_3)_2$ concentration, while it decreased for low concentration and high current density deposition. On the other hand, deposition temperature had negative effect on current efficiency more for lower current density deposition. Cyclic voltammetric study revealed that comparatively more ${\beta}-PbO_2$ produced compact deposits when deposition was carried out from high $Pb(NO_3)_2$ concentration. Such compact films gave lower charge discharge current density during cycling. SEM and AFM studies showed that deposition of regular-size sharp-edge grains occurred for all deposition conditions. The grain size for high temperature and low concentration $Pb(NO_3)_2$ deposition was bigger than from low temperature and high concentration deposition conditions. While cycling converted all grains into loosely adhered flappy deposit with numerous pores. X-ray diffraction measurement indicates that high concentration, high temperature, and high current density favored ${\beta}-PbO_2$ deposition while ${\alpha}-PbO_2$ converted to ${\beta}-PbO_2$ together with some unconverted $PbSO_4$ during cycling in $H_2SO_4$.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.14 no.5
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• pp.120-125
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• 2015

This research aims to increase the reliability and reproducibility of the ambient cycling test by properly making corrections to the test procedure. The vessel (106 L) is initially filled with 70 L of water and horizontally placed on a balance. The pressure range inside the vessel varies from 2.5 to 25.9 MPa at the frequency of 6 cycles per minute. After reviewing the results, there was a temperature difference of approximately $10^{\circ}C$ between the air pocket and the water, and the upper part of the liner faced a repeated temperature change of $40^{\circ}C$. It is possible for the aluminum liner of the composite vessel to be damaged by such a sharp change in temperature. Additionally, as a result, no pass having anything to do with the purpose of the test would occur. Therefore, it is suggested that the air pocket be completely removed.

• Composites Research
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• v.30 no.1
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• pp.7-14
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• 2017

In this paper, the inter-lamina shear strength (ILSS) of multi-wall carbon nanotube (MWNT) reinforced carbon fiber reinforced plastics (CFRP) and thin-ply composites were verified under low earth orbit (LEO) space environment. CFRP, MWNT reinforced CFRP, thin-ply CFRP and MWNT reinforced thin-ply CFRP were tested after aging by using accelerated ground simulation equipment. The used ground simulation equipment can simulate high vacuum ($2.5{\times}10^{-6}torr$), atomic oxygen (AO, $9.15{\times}10^{14}atoms/cm^2{\cdot}s$), ultraviolet light (UV, 200 nm wave length) and thermal cycling ($-70{\sim}100^{\circ}C$) simultaneously. The duration of aging experiment was twenty hours, which is an equivalent duration to that of STS-4 space shuttle condition. After the aging experiment, ILSS were measured at room temperature ($27^{\circ}C$), high temperature ($100^{\circ}C$) and low temperature ($-100^{\circ}C$) to verify the effect of operation temperature. The MWNT and thin-ply shows good improvement of ILSS at ground condition especially with the thin-ply. And after LEO exposure large degradation of ILSS was observed at MWNT added composite due to the thermal cycle. And the degradation rate was much higher under the high temperature condition. But, at the low temperature condition, the ILSS was largely recovered due to the matrix toughening effect.

• Animal cells and systems
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• v.1 no.4
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• pp.609-617
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• 1997

Polygenic variation of sternopleural bristle number was investigated at the whole chromosome level in a natural population of Drosophila melanogasfer. Fifty pairs of second and third chromosomes were analyzed at $25^\circ{C}$. Since environmental factors such as temperature influence polygenic expression of quantitative traits, whole chromosomal effects of 28 pairs from the larger original sample were measured under cycling temperature, a $10-30\circ{C}$ cycle in 24 hours, to reveal any polygenic alleles whose effects might be masked under the constant temperature. While third chromosomes typically showed a larger contribution to polygenic variation in both environments, second chromosomes showed greater sensitivity to environmental changes. Cluster analyses of second and third chromosomes produced a limited number of clusters. Such a small number of cluster's implies that there may be a small number of genes, or quantitative trait loci (QTLs), having large effects on phenotypic variation. The genetic structure assessed under constant temperature, however, did not show any correlation with the structure under cycling temperature. The discrepancy could be caused by independent response of each polygenic allele to temperature changes. Thus, polygenic structure in natural populations should be thought of as a temporally changing profile of interactions between gene and ever-changing environment.

• Journal of the Microelectronics and Packaging Society
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• v.10 no.3
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• pp.9-17
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• 2003

In this paper, thermo-mechanical and rheological properties of NCPs (Non-Conductive Pastes) depending on silica filler contents and diluent contents were investigated. And then, thermal cycling (T/C) reliability of flip chip assembly using selected NCPs was verified. As the silica filler content increased, thermo-mechanical properties of NCPs were changed. The higher the silica filler content was added, glass transition temperature ($T_g$) and storage modulus at room temperature became higher. While, coefficient of thermal expansion (CTE) decreased. On the other hand, rheological properties of NCPs were significantly affected by diluent content. As the diluent content increased, viscosity of NCP decreased and thixotropic index increased. However, the addition of diluent deteriorated thermo-mechanical properties such as modulus, CTE, and $T_g$. Based on these results, three candidates of NCPs with various silica filler and diluent contents were selected as adhesives for reliability test of flip chip assemblies. T/C reliability test was performed by measuring changes of NCP bump connection resistance. Results showed that flip chip assembly using NCP with lower CTE and higher modulus exhibited better T/C reliability behavior because of reduced shear strain in NCP adhesive layer.

• Journal of Hydrogen and New Energy
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• v.9 no.3
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• pp.111-118
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• 1998

The intrinsic degradation behavior of $(V_{0.53}Ti_{0.47})_{0.925}Fe_{0.075}$ alloy with BCC structure and the two plateau regions (the low and high plateau region) has been investigate during the temperature-induced hydrogen absorption-desorption cycling (thermal cycling). After 400 thermal cycles between room temperature and $600^{\circ}C$ under 10atm $H_2$, the total reversible hydrogen absorption capacity decreased by about 40%. From thermal desorption analysis it was found that the degradation behavior at each plateau region was different. In addition, XRD analysis showed that the crystal structure of the sample in de-hydrided state was changed from BCC to BCT after degradation, and that of the sample in hydrided state it was maintained as FCC although peaks were broadened after degradation. From the result of static isothermal hydrogenation treatment it were found that crystal structure change from BCC to BCT was caused by the thermal energy. TEM analysis showed that the peak broadening was due to the formation of an amorphous phase in FCC matrix.

• Proceedings of the Korea Institute of Applied Superconductivity and Cryogenics Conference
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• 2003.10a
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• pp.131-133
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• 2003

The effect of axial strain and thermal cycling on the critical current is investigated for the Bi-2223/Ag PIT tapes. The axial strain was applied to the tapes by the U-shape sample holder. Two kinds of Bi-2223/Ag tapes with different Ag sheath are used to know the effect of sheath alloying for the tensile strain. The influence of thermal cycling between room temperature and 77 K on critical current are examined. Critical current is drastically decreased for Ag/alloy and Ag/alloy/alloy sheathed tapes at tensile strain above 0.22％ and 0.3％, respectively.