• Title/Summary/Keyword: Temperature control curing

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Prediction Equation of Setting Time for Mortar Using Super Retarding Agent Using Equivalent Age (등가재령을 이용한 초지연 모르타르의 응결시간 예측식 제안)

  • Han, Min-Cheol;Hyun, Seung-Yong;Kim, Jong
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.10 no.1
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    • pp.80-91
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    • 2022
  • This study is to provide an prediction model of setting time of super retarding mortar based on equivalent age method under various super retarding agent contents, curing temperature, and water-binder ratio (W/B). An equation for predicting setting time using maturity was proposed. Test results indicated that the setting time can be predicted by determining the curing temperature, W/B, and super retarding agent contents and substituting it into the equation proposed in this study. The coefficient of determination of the equation is 0.9 or more, and the reliability was confirmed through the F-test. Finally, using the equation proposed in this paper, reasonable quality control is possible regarding the setting of super retarding concrete in practice.

Non-Solvent Liquid Resin of Non-Discoloration Type at Room Temperature (비변색타입의 무용제형 상온 액상수지)

  • Moon, Jin-Bok;Mok, Dong-Yeop;Kim, Gu-Hyun
    • Korean Chemical Engineering Research
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    • v.47 no.6
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    • pp.669-675
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    • 2009
  • A study has been made on the preparation of liquid resin of non-solvent and non-discoloration type for replacement of the soft PVC at room temperature. A new synthetic process was developed by structure-control design of polyurethane synthesis using pre-polymer and polyols as curing agent. The optimum recipe was made according to macro-glycols, molecular weight and reaction conditions, and the final products indicated that the mechanical properties such as tensile strength, tear strength and flexibility was very excellent than PVC products. Also, viscosity, hardness and color operations of the final products can be controlled by this system. And yellowing property by UV and NOx gas was improved from the various additive experiment.

A Study on Trend of Tensile Properties with Ratio of Water Mixture under Low and High Temperature Environment in Hydroponic Polyurethane Waterproofing Materials (수경화성 폴리우레탄 도막재의 물 혼합비에 따른 저온 및 고온 환경에서의 인장성능 변화 추이 연구)

  • Kim, Dong-Bum;An, Hyun-Ho;Kim, Sun-Do;Park, Wan-Goo;Park, Jin Sang;Oh, Sang-Keun
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2016.05a
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    • pp.211-212
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    • 2016
  • Due to a lack of objective and adequate study on the physical effects on hydroponic polyurethane waterproofing material water mixture ratio, construction site workers are having to rely on their hands-on experience to determine a mixture ratio, resulting in difficulty of maintaining quality management. Particularly in cases of rooftop exposed type hydroponic polyurethane materials, the varying temperature conditions make it further difficult for quality management control. in this regard, this study conducts tensile strength testing and compares the tensility change rates hydroponic polyurethane waterproofing materials with various water mixture ratios ranging from 0%~50% and exposed to alternating temperature change between -20℃ to 60℃ in the span of 1 hour after curing for 14 days.

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A study on the Relation between Strain & Conductivity of the Printed Pattern in Post-Printing Section of Roll to Roll process (롤투롤 공정의 인쇄 후 구간에서 변형률과 인쇄한 패턴의 전기 전도도와의 관계에 대한 연구)

  • Choi, Jae-Ho;Lee, Chang-Woo;Shin, Kee-Hyun
    • Journal of Institute of Control, Robotics and Systems
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    • v.15 no.9
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    • pp.877-880
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    • 2009
  • A curing process in post-printing section of R2R process is required for an electrical property of the printed pattern when devices such as RFID, Solar cell are printed. PEN as well as heat-stabilized PET which is used as a plastic substrate would be deformed at high temperature due to change of its elastic modulus. And crack in the printed pattern, which is on the plastic substrate is occurred due to the deformation of the substrate. The occurrence of crack causes electrical resistance to increase and the quality of the device to deteriorate. In case of RFID antenna, the range of reading distance is shortened as the electrical resistance of the antenna is increased. Therefore, the deformation of the plastic substrate, which causes the occurrence of crack, should be minimized by setting up low operating tension in R2R process. In low tension, slippage between a moving substrate and a roller would be generated when the operating speed is increased. And scratch would be occurred when slippage is generated due to an air entrainment, which is related to the thickness of the air film. The thickness of the air film is increased when operating speed is increased as shown by simulation based on mathematical model. The occurrence of scratch in conductive pattern printed by roll to roll process is a critical damage because it causes degradation or failure of electrical property of it.

THE EFFECT OF TEMPERATURE CHANGES ON THE PHYSICAL PROPERTIES OF POSTERIOR COMPOSITE RESINS (구치부용 복합 레진 가열시 물리적 성질의 변화에 관한 실험적 연구)

  • Park, Yeon-Hong;Min, Byung-Soon;Choi, Ho-Young;Park, Sung-Jin
    • Restorative Dentistry and Endodontics
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    • v.14 no.1
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    • pp.41-56
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    • 1989
  • The purpose of this study was to examine the effect of temperature dependence of the behavior on the physical properties of posterior composite resins. Three light cure posterior composite resins (Heliomolar, Litefil-P, and P-50) and one chemical cure posterior composite resin (Bisfil-II) were used as experimental materials. Composite resin was placed in a cylindrical brass mold (2.5 mm high and 6.5 mm inside diameter) that was rested on a glass plate. Another flat glass was placed on top of the mold, and the plate was tightly clamped together. After the mold had been filled with the light cure composite material, the top surface was cured for 30 seconds with a light source. Chemical cure resin specimens were made in the same manner as above. Three hundreds and twenty composite resin specimens were constructed from the four composite materials. One hundred and sixty specimens of them were placed in a heater at $50^{\circ}C$, $75^{\circ}C$, $100^{\circ}C$, $125^{\circ}C$, $150^{\circ}C$, $175^{\circ}C$ and $200^{\circ}C$ for 5 minutes or 10 minutes respectively before compressive strengths were measured. Another one hundred and sixty specimens were tested for the diametral tensile strengths in the same way as above. They were randomly divided into eight groups according to the mode of heating methods as follows and stored in distilled water at $37^{\circ}C$ for 24 hours. Group $37^{\circ}C$ - specimens were stored at $37^{\circ}C$ in distilled water for 24 hours. Group $50^{\circ}C$ - specimens were heated at $50^{\circ}C$ after curing. Group $75^{\circ}C$ - specimens were heated at $75^{\circ}C$ after curing. Group $100^{\circ}C$ - specimens were heated at $100^{\circ}C$ after curing. Group $125^{\circ}C$ - specimens were heated at $125^{\circ}C$ after curing. Group $150^{\circ}C$ - specimens were heated at $150^{\circ}C$ after curing. Group $175^{\circ}C$ - specimens were heated at $175^{\circ}C$ after curing. Group $200^{\circ}C$ - specimens were heated at $200^{\circ}C$ after curing. Twenty specimens of each of four composite resins were respectively made by insertion of materials into same mold for examining the dimensional changes between before and after heating. The final eighty specimens were stored in distilled water at $37^{\circ}C$ for 24 hours before testing the dimensional changes. Compressive and diametral tensile strengths were measured crosshead speed 1mm/minute and 500Kg in full scale with a mechanical testing machine (DLC 500 Type, Shimadzu Co., Japan). Dimensional changes were determined by measuring the diametral changes of eighty specimens with micrometer (Mitutoyo Co., Japan). Results were as follows: 1. Diametral tensile strengths of specimens in all groups were increased with time heated compared with control group except for that in group $50^{\circ}C$ and the maximum diametral tensile strength was appeared in the specimen of Litefil-P heated for 10 minutes at $100^{\circ}C$. In heliomolar and P-50, it could be seen in the specimen heated for 10 minutes at $150^{\circ}C$, but in Bisfil-II, it could be found in the specimen heated for 5 minutes at $150^{\circ}C$. 2. Compressive strengths of specimens in all groups was tended to be also increased with time heated but that in group $50^{\circ}C$ and the maximum compressive strengths were showed in the same specimens conditioned as the diametral tensile strengths of four composite materials tested. 3. In Heliomolar, Litefil-P, and Bisfil-II, it was decreased in diameters of resin specimens between before heating and increased in diameters of resin specimens after storing in distilled water, but it was not in P-50. 4. There is little difference in diametral tensile strengths, compressive strengths, and dimensional changes followed by heating the resin specimens for 5 minutes and 10 minutes, but there is no statistical significances.

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Measurement of the Early-Age Coefficient of Thermal Expansion and Drying Shrinkage of Concrete Pavement (콘크리트포장의 초기 열팽창계수 및 건조수축 측정 연구)

  • Yoon, Young-Mi;Suh, Young-Chan;Kim, Hyung-Bae
    • International Journal of Highway Engineering
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    • v.10 no.1
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    • pp.117-122
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    • 2008
  • Quality control of the concrete pavement in the early stage of curing is very important because it has a conclusive effect on its life span. Therefore, examining and analyzing the initial behavior of concrete pavement must precede an alternative to control its initial behavior. There are largely two influential factors for the initial behavior of concrete pavement. One is the drying shrinkage, and the other is the heat generated by hydration and thermal change inside the pavement depending on the change in the atmospheric temperature. Thus, the coefficient of thermal expansion and drying shrinkage can be regarded as very important influential factors for the initial behavior of the concrete. It has been a general practice up until now to measure the coefficient of thermal expansion from completely cured concrete. This practice has an inherent limitation in that it does not give us the coefficient of thermal expansion at the initial stage of curing. Additionally, it has been difficult to obtain the measurement of drying shrinkage due to the time constraint. This research examined and analyzed the early drying shrinkage of the concrete and measurements of the thermal expansion coefficients to formulate a plan to control its initial behavior. Additionally, data values for the variables of influence were collected to develop a prediction model for the initial behavior of the concrete pavement and the verification of the proposed model. In this research, thermal expansion coefficients of the concrete in the initial stage of curing ranged between $8.9{\sim}10.8{\times}10^{-6}/^{\circ}C$ Furthermore, the effects of the size and depth of the concrete on the drying shrinkage were analyzed and confirmed.

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A Study on the Thermal Crack Control of the In-Ground LNG Storage Tank as Super Massive Structures (지하식 LNG 저장탱크 구조물의 온도균열 제어에 관한 연구)

  • Kwon, Yeong-Ho
    • Journal of the Korea Concrete Institute
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    • v.23 no.6
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    • pp.773-780
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    • 2011
  • In this study, thermal stress analysis are carried out considering material properties, curing condition, ambient temperature, and casting date of the mass concrete placed in bottom slab and side wall of the in-ground type LNG tank as a super massive structure. Also, based on the numerical results, cracking possibility is predicted and counter measures to prevent the cracking are proposed. For the tasks, two optimum mix proportions were selected. From the results of the thermal stress analysis, the through crack index of 1.2 was satisfied for separately caste concrete lots except for the bottom slab caste in 2 separate sequences. For the double caste bottom slab, it is necessary introduce counter measures such as pre-cooling prior to the site construction. Also, another crack preventive measure is to lower the initial casting temperature by $25^{\circ}C$ or less to satisfy 1.2 through crack index criterion. In the $1^{st}$ and $2^{nd}$ caste bottom slab, the surface crack index was over 1.2. Therefore, the surface cracks can be controlled by implementing the curing conditions proposed in this study. Since the side wall's surface crack index was over 1.0, it is safe to assume that the counter preventive measures can control width and number of cracks.

Quality change of mini sweet pumpkins (suppress cultivation, fall planting) during storage at different conditions (가을작형 억제재배 미니단호박의 저장조건별 품질 변화)

  • Oh, Bong-Yun;Jo, Gyeong-Suk;Lee, You-Seok;Kang, Jeong-Hwa;Jang, Mi-Hyang;Hwangbo, In-Sik
    • Food Science and Preservation
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    • v.22 no.6
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    • pp.779-787
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    • 2015
  • We stored sweet pumpkins at $8^{\circ}C$, $12^{\circ}C$, $12^{\circ}C$ plasma curing and room temperature (control) for 180 days. During this time, the quality characteristics were analyzed within the different groups. No spoiling occurred in either of the storage conditions for up to 120 days, and the marketability was good. After 120 days, spoiling sharply increased by over 70% in the control group, while in the $12^{\circ}C$ group it decreased to 20~60%. Conversely, spoiling was completely absent in the $8^{\circ}C$ and $12^{\circ}C$ plasma curing groups during the overall 180 days of storage. The lowest moisture content was found in the $8^{\circ}C$ group and the quality of the pumpkins was excellent during the entire storage period. The color of pulp was better in the $12^{\circ}C$ and $12^{\circ}C$ plasma curing groups, with best results were found in the latest. Both the $8^{\circ}C$ and $12^{\circ}C$ plasma curing groups maintained their dark green surface colors, while both the $12^{\circ}C$ and control groups turned from green to yellow. All groups showed a reduction in their initial hardness, with the $8^{\circ}C$ group staying the hardest. Soluble solid and mealiness was increased to the storage during 90 days while decreased, that were long to maintain the mealiness texture in the $8^{\circ}C$ storage pumpkin. The overall acceptability from sensory evaluation was higher in the $12^{\circ}C$ plasma curing group, when compared to those of the $8^{\circ}C$, $12^{\circ}C$ and control groups storage conditions.

EFFECT OF CURING CONDITIONS ON THE MONOMER ELUTION OF ORTHODONTIC ACRYLIC RESIN (교정용 아크릴릭 레진의 중합조건에 따른 모노머 용리)

  • Noh, Hong-Seok;Kim, Jae-Moon;Kim, Shin;Jeong, Tae-Sung
    • Journal of the korean academy of Pediatric Dentistry
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    • v.35 no.3
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    • pp.477-486
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    • 2008
  • Acrylic resin is widely used in dental practice. However, the residual monomer in acrylic resin could act as a negative biocompatability on human body. The aim of this study was to evaluate the amount of the monomer elution from polymerized orthodontic acrylic resin. Orthodontic acrylic resin was used in the study. The curing condition of the resin was controlled by temperature, pressure, aquatic and atmospheric environment. The duration and amount of monomer elution and timedependent plot was recorded by high performance liquid chromatography. The result showed that the only monomer eluted from the resin was methyl methacrylic acid. And the amount of the monomer elution has diminished considerably by time progress especially within 24 hours. Furthermore, elution of the residual monomer was significantly lower in group of pressure, moisture and elevated temperature than control (p<.05). According to this study, it was thought that the elution of residual monomer might be influenced by curing environment.

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A Study on Smart Cure of Filament Wound Composite Flywheel (필라멘트 와인딩 플라이휠의 스마트 경화에 관한 연구)

  • 이도훈;김선경;김동진;이우일;하성규
    • Composites Research
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    • v.16 no.1
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    • pp.34-41
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    • 2003
  • A cure process control model was proposed to optimize the curing process of thick filament wound structure. There are two types of smart cure, one is that the boundary conditions of the hollow cylinder are same between inner surface and outer surface, and the other is that inner surface temperature is slightly higher than outer surface to initiate cure reaction from the inner side to the outer side to reduce residual stress.