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Derivation of predicting regression equations of bonding thickness and deflection of glass edge considering the interaction effects between the parameters (공정변수간의 교호작용을 고려한 모서리 접합두께 및 처짐량 예측 회귀식 도출)

  • Kim, Youngshin;Jeon, Euysik
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.14 no.2
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    • pp.511-516
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    • 2013
  • The thickness and deflection of melting parts of the glass edge reach the biggest effect on the intensity and thermal insulation performance. During the sealing process using a hydrogen mixed gas torch, the thickness and the deflection effect of the edge part are affected by process parameters. In order to analyze the correlative relationship of the thickness prediction and the deflection of the edge part according to the process parameters, data was obtained by conducting sealing experiments. The main effects and interaction effects of process parameters for the thickness and the shape of the glass edge parts were analyzed through the design of experiment. A mathematical experiment equation that can predict the thickness and deflection of the edge part according to the process parameters was developed by conducting multiple regression equations.

A study on the titanium welding process according to the temperature characteristics of shielding methods (티타늄 용접공정에서 온도특성에 따른 실딩방법에 관한 연구)

  • Chung, Han-Shik;Jeong, Hyo-Min;Lee, Dae-Chul;Lee, Byeong-Yong
    • Journal of Advanced Marine Engineering and Technology
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    • v.37 no.1
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    • pp.29-34
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    • 2013
  • The welds tent to be weakened if it is exposed to the air during the welding process. In titanium welding with Gas Tungsten Arc Welding, inappropriate colors of the welds, such as purple/red, blue, yellow, gray, white and pink represents that it is contaminated by oxygen and nitrogen in the air. Shielding gases can be used to protect welds from the contamination. In addition, Weld metal and heat affected zone (HAZ) are also shielded from the air when it is cooled down to the room temperature. In this paper, appropriate shielding gases for the shape and form of Trailing Shielding Jig and torch shielding ($13{\sim}20{\ell}/min$), after shielding ($22{\sim}30{\ell}/min$), and back shielding ($25{\sim}30{\ell}/min$) are studied.

Color Enhancement for Cubic Zirconia with Low Temperature Annealing (큐빅지르코니아의 색향상을 위한 저온열처리 공정 연구)

  • Li, Feng;Shen, Yun;Song, Oh-Sung
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.11 no.4
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    • pp.1186-1191
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    • 2010
  • Colored cubic zirconia specimen made by skull melt process were annealed in vacuum at the temperature of $1200^{\circ}C{\sim}1400^{\circ}C$ for 10~60 minutes to enhance the color. All the seven specimen become darker and eventually be black as annealing temperature and time increase. The black samples turned into original colors when we elevated the temperature with oxy-acetylene torch for around 10 minutes in the air. Finally, we could tune the colors of cubic zirconia either anneal in vacuum or the black samples in the air to obtain the proposed colors. Our proposed new process may be appropriate to fabricate the precious synthetic colored cubic zirconia to simulate the natural colored gem quality diamonds.

A Case of Fetal Hepatic Calcificaion with a Good Prognosis (양호한 예후를 보인 태아 간 석회화 1례)

  • Na, Kyong Hee;Lee, Hyun Jung;Kim, Eun Young;Kim, Sung Soo;Kim, Kyoung Sim;Kim, Yong Wook
    • Clinical and Experimental Pediatrics
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    • v.45 no.3
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    • pp.395-400
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    • 2002
  • Recently, the increasing use of antenatal high resolutional ultrasonographic studies, and the increasing expertise of sonographers have contributed to the more frequent prenatal detecton of fetal hepatic calcification. Fetal hepatic calcification can arise from peritoneal, ischemic, infectious, neoplastic, and idiopathic causes. There are many reports that the prognosis is good in isolated fetal hepatic calcification without chromosomal aberrations, associated congenital malfomations or other organ abnormalities. We report one case of fetal hepatic calcification diagnosed by prenatal ultrasonography at gestational age of 27 weeks, without chromosomal abnormalities or other associated organ abnormalities, showing good prognosis.

DEVELOPMENT OF COMBIND WELDING WITH AN ELECTRIC ARC AND LOW POWER CO LASER

  • Lee, Se-Hwan;Massood A. Rahimi;Charles E. Albright;Walter R. Lempert
    • Proceedings of the KWS Conference
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    • 2002.10a
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    • pp.176-180
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    • 2002
  • During the last two decades the laser beam has progressed from a sophisticated laboratory apparatus to an adaptable and viable industrial tool. Especially, in its welding mode, the laser offers high travel speed, low distortion, and narrow fusion and heat-affected zones (HAZ). The principal obstacle to selection of a laser processing method in production is its relatively high equipment cost and the natural unwillingness of production supervision to try something new until it is thoroughly proven. The major objective of this work is focused on the combined features of gas tungsten arc and a low-power cold laser beam. Although high-power laser beams have been combined with the plasma from a gas tungsten arc (GTA) torch for use in welding as early as 1980, recent work at the Ohio State University has employed a low power laser beam to initiate, direct, and concentrate a gas tungsten arcs. In this work, the laser beam from a 7 watts carbon monoxide laser was combined with electrical discharges from a short-pulsed capacitive discharge GTA welding power supply. When the low power CO laser beam passes through a special composition shielding gas, the CO molecules in the gas absorbs the radiation, and ionizes through a process known as non-equilibrium, vibration-vibration pumping. The resulting laser-induced plasma (LIP) was positioned between various configurations of electrodes. The high-voltage impulse applied to the electrodes forced rapid electrical breakdown between the electrodes. Electrical discharges between tungsten electrodes and aluminum sheet specimens followed the ionized path provided by LIP. The result was well focused melted spots.

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A Study on Two-Dimensional Forming of Ship Hull Plate by Geometrical Approach (곡가공 공정에서 기하학적 접근법에 의한 2차원 성형에 관한 연구)

  • Seong, Woo-Jae;Ahn, Jun-Su;Kim, Hyun-Uk;Na, Suck-Joo
    • Journal of Welding and Joining
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    • v.27 no.2
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    • pp.32-37
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    • 2009
  • In shipyard, plate forming is widely used to form the ship hull plate in various shapes. Line heating method by using a flame torch is one of the major shipbuilding processes carried out by skilled workers. Since the forming characteristics depend upon their experiences in manual forming, there are much variations between products and difficulties in communication between engineers and workers. Hence, it needs to develop an automatic forming system which can not only reduce the working time and rework costs but also improve the working environment and hull forming productivity. One of the final goals of plate forming automation is to form a target shape from the initial plate automatically. For automated plate forming, it is required to determine where and how to heat on the plate. To realize this procedure, the inverse problem should be first solved and the effect of curvature shape formed at the heating path should be investigated. In this study, the inverse problem was solved by geometrical approach using the relationship between bending angle and radius of curvature of the curved shape. In addition, experiments of two-dimensional plate forming were performed with the distance-based method considering the curved bending with curvature. The result of the formed shape agreed considerably well with the target shape.

Microstructure and Ablation Performance of CNT-phenolic Nanocomposites (삭마 효과에 대한 CNT-페놀 나노복합재료의 미세구조 분석)

  • Wang, Zuo-Jia;Kwon, Dong-Jun;Park, Jong-Kyoo;Lee, Woo-Il;Park, Joung-Man
    • Composites Research
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    • v.26 no.5
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    • pp.309-314
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    • 2013
  • Highly ablation resistant carbon nanotube (CNT)-phenolic composites were fabricated by the addition of low concentrations of CNT nanofiller. Tensile and compressive properties as well as ablative resistance were significantly improved by the addition of only 0.1 and 0.3 wt% of uniformly dispersed CNTs. An oxygen-kerosene-flame torch and a field emission scanning electron microscope (FE-SEM) were used to evaluate the ablative properties and microstructures of these CNT-phenolic composites. Thermal gravimetric analysis (TGA) revealed that the ablation rate was lower for the 0.3 wt% CNT-phenolic composites than for neat phenolic or the composite with 0.1 wt% CNT. Ablative mechanisms for all three materials were investigated using this TGA in conjunction with microstructural studies using a FE-SEM. The microstructural studies revealed that CNT acted as an ablation resistant phase at high temperatures, and that the uniformity of dispersion of the CNT played an important role in this resistance to ablation.

Fire-Retardation Properties of Silicone/Perlite Composites (실리콘/펄라이트 복합체의 난연 특성)

  • Lee, Byunggab;Won, Jongpil;Jang, Ilyoung;Bang, Daesuk
    • 한국방재학회:학술대회논문집
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    • 2011.02a
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    • pp.154-154
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    • 2011
  • 최근 세계 각지에서 발생하는 대규모 터널 화재사고는 많은 사상자를 동반하고 이에 따른 경제적, 사회적 손실 또한 방대하게 진행되는 실정이다. 터널 구조물의 화재 특성상 외부에 쉽게 노출되지 않기 때문에 화재 발생 시 화재에 노출된 표층이 박리되거나 비산해서 단면결손이 생기는 폭렬 현상(explosive spalling)이 발생하게 된다. 이러한 폭렬 현상은 붕괴와 같은 대형 참사로 이어질 가능성이 크다. 따라서 본 연구에서는 터널 내 화재 발생 시 콘크리트 구조물의 폭렬에 의한 붕괴를 예방하기 위하여 이액형 상온경화 실리콘 고무와 인체에 무해한 친환경 첨가제인 펄라이트를 일정한 혼합비(5wt%, 10wt%, 15wt%, 20wt%)로 혼합하여 고성능 난연 복합체를 제조하고, 열적 특성과 난연 특성을 연구를 진행하였다. 열적 특성에 관한 시험으로 TGA를 측정하였으며, 난연 특성에 관한 시험으로는 화염 시험, 내화로 시험, 탄화로 시험을 진행하였다. 우선 TGA 시험은 $20^{\circ}C/min$ 승온 속도로 $800^{\circ}C$까지 실험을 하였고, 화염 시험은 제작한 시편과 gas torch($1200^{\circ}C$)의 화염 거리를 약 10cm로 하여 약 1시간 동안 시험을 하였다. 내화로 시험은 내화로 장치를 이용하여 RABT curve(5분만에 $1200^{\circ}C$도달 후 한 시간 동안 유지 후 냉각, 총 시험 시간 180분) 조건을 만족하는 환경에서 제작한 시편을 콘크리트에 부착하여 콘크리트의 내부온도를 측정하였다. 탄화로 시험은 탄화로 장치를 이용하여 $2^{\circ}C/min$ 승온속도로 $900^{\circ}C$까지 실험을 하여 외부 형태 변화를 관찰하였다. 각각의 시험 결과 TGA 열분해 결과 순수한 실리콘 고무보다 난연제인 펄라이트를 첨가했을 때 더 높은 온도에서 초기 분해 거동을 보였으며, 최종 잔류량은 80%를 보였고, 5 wt%의 펄라이트가 혼합된 시편의 최종 잔류량이 높은 것으로 보아 열분해에 가장 강한 조성임을 알 수 있었다. 화염 시험 결과 펄라이트가 혼합된 모든 시편에서 $300^{\circ}C$가 넘지 않은 결과를 보였다. 이는 제조된 복합체가 화염에 직접적으로 장시간 노출이 되어도 안전하다는 것을 알 수 있다. 내화로 및 탄화로 시험 결과 펄라이트가 15wt%와 20wt%가 첨가된 시편들보다 5wt%와 10wt% 첨가된 시편들이 고온에서 안정하다는 것을 보였다.

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Development of an Axially Viewed Inductively Coupled Plasma for Atomic Emission Spectrometry and Comparison between the Detection Limits of Lead (원자방출 분광분석을 위한 수평형 유도결합 플라스마의 개발과 납 검출한계 비교)

  • Cho, Sung Il;Han, Myung Sub;Lee, Sang Hwa;Lee, Joung Hae;Woo, Jin Chun
    • Journal of the Korean Chemical Society
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    • v.41 no.6
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    • pp.292-298
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    • 1997
  • An ICP(Inductively Coupled Plasma) emission spectrometer was developed with an axially viewed ICP source incorporated by a 5-turned induction coil and a torch, outer quartz tube of which was 50 mm longer than that used in conventional ICP/AES(Inductively Coupled Plasma Atomic Emission Spectrometry). The Optimization of the system has been performed in terms of the determination of signal-to-noise ratio and background intensity at various rf powers, sample flow rates, argon gas flow rates and cut-off gas flow rates. The spectro-analytical characteristics of the spectrum obtained between 200 and 500 nm was revealed to be similar compared with a vertically viewed ICP source. The detection limit of Pb(Ⅱ) at 220.35 nm was 11 ppb which was 5 times lower than that obtained with a vertically viewed ICP source.

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Characteristics of Plasma Blacks Used as an Electrode of Direct Formic Acid Fuel Cell

  • Park, Young-Sook;Choi, Jong-Ho;Han, Jong-Hee;Lim, Tae-Hoon;Beak, Young-Soon;Ju, Jeh-Beck;Shon, Tae-Won;Lee, Joong-Kee
    • Carbon letters
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    • v.6 no.1
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    • pp.41-46
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    • 2005
  • Plasma carbon blacks of 20~30 nm diameter were synthesized by direct decomposition of natural gas using a hybrid plasma torch system with 50 kW direct current and 4 MHz of radio frequency. The insulating rector which inside diameter of 400 mm and length of 1500 mm, respectively was kept at 300~$400^{\circ}C$ during the preparation. The ultimate analysis of plasma carbon blacks reveals that the raw plasma carbon blacks contains a large quantity of volatile which is mainly consist of hydrogen. Therefore devolatilization of raw plasma carbon blacks were carried out at $900^{\circ}C$ for one hour under nitrogen atmosphere. The devolatilization leads to the decrease in electrical resistivity and surface oxygen functional groups of plasma carbon black significantly. In order to investigate the plasma carbon as a catalyst support, devolatilized plasma black at $900^{\circ}C$ (DPB) supported PtAu catalyst was synthesized by sodium boronhydride reduction method. Electrochemical measurements and direct formic acid fuel cell test indicated that catalytic activity of DPB supported PtAu catalyst for formic acid oxidation was similar to that of Vulcan XC-72 of commercial carbon black supported one.

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