• Journal of Welding and Joining
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• v.16 no.3
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• pp.157-166
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• 1998

Recently as environmental pollution caused by Pb has posed a serious threat to the global environment, the trend to regulate the usage of Pb in electronic industry is one the rise. Currently, the solder alloy with high Pb content, Sn-37%Pb, is utilized in the electronic assembly therefore, the objective of this study is to develop an alternative solder alloy for the existing Sn-37%Pb solder alloy. First thing, this work choosed Sn-5%Pb-1.5%Ag, Sn-5%Pb-1.5%Ag-x%Bi(x=1~5%) for candidate solder alloys, and examined their properties such as melting range, wettability, microhardness, tensile property, oxidation behavior and microstructure. Wettability was on the same level of Sn-37%Pb. Dissolution of Pb ion in Sn-5%Pb solder was 0.46ppm. This solder alloy revealed cellular dendrite microstructure $\beta$-Sn matrix, Pb-rich phase, Ag/Sn, and Cu/Sn Intermetallic compounds. The range of solidification temperature was within 3$0^{\circ}C$. Also these alloy displayed higher tensile strength and lower elongation than Sn-37%Pb. The resistance of oxidation in Sn-5%Pb-1.5%Ag solder alloy was superior to that of Sn-37%Pb solder alloy. But that of Sn-5%Pb-1.5%Ag-5%Bi solder alloy was equal to that of Sn-37%Pb solder alloy.

• Journal of Welding and Joining
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• v.16 no.3
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• pp.148-156
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• 1998

The purpose of this study is to investigate the characteristics of Pb-Free Sn-2%Ag-Bi solder alloys. The solder alloys used in this study is Sn-2%Ag-(3,5,7,9%) Bi It is examined that their properties such as melting range, wettability, microstructure, microhardness, and tensile property. The addition of Bi(3,5,7,9%) lowered the melting point of the solder and the melting range was 196~203$^{\circ}C$. The wettability of the solder as equal to that of Sn-37% Pb solder. The morphology of structure did not change largely by addition of Bi. But the structure of cellular dendrite of linear type displayed. The tensile strength of the solder was superior to that of Sn-37%Pb solder. But the elongation was inferior to that of Sn-37%Pb solder. The hardness of Sn-2%Ag solder was tow times and that of Sn-2%Ag-Bi solder was three times of that in Sn-37%Pb solder. But the effect of increment of Bi content did not change largely.

• Journal of Mechanical Science and Technology
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• v.20 no.6
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• pp.819-827
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• 2006

The stress-strain relation of aluminum (Al) alloy foam cell wall was evaluated by the instrumented sharp indentation method. The indentation in a few micron ranges was performed on the cell wall of Al-alloy foam having a composition or Al-3wt.%Si-2wt.%Cu-2wt.%Mg as well as its precursor (material prior to foaming). To extract the stress-stram relation in terms of yield stress ${\sigma}_y$, strain hardening exponent n and elastic modulus E, the closed-form dimensionless relationships between load-indentation depth curve and elasto-plastic property were used. The tensile properties of precursor material of Al-alloy foam were also measured independently by uni-axial tensile test. In order to verify the validity of the extracted stress-strain relation, it was compared with the results of tensile test and finite element (FE) analysis. A modified cubic-spherical lattice model was proposed to analyze the compressive behavior of the Al-alloy foam. The material parameters extracted by the instrumented nanoindentation method allowed the model to predict the compressive behavior of the Al-alloy foam accurately.

• Journal of the Korean Society of Mechanical Technology
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• v.13 no.2
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• pp.93-100
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• 2011

This study deals with the high frequency induction hardening (HF at $850^{\circ}C$, 120kHz & 50kW condition) SM45C steel. (1) The HF specimen, which was tempered at $150^{\circ}C$, did not show any tempering effect. A brittle fracture occurred at rounded area of the tensile specimen. AE (acoustic emission) amplitude distribution showed between 45dB and 60dB. (2) A slip and fracture occurred at the hole area of the HF specimen which was tempered at $300^{\circ}C$. As they pass the yield point, the AE energy is increased intermittently and AE amplitude distribution exists between 70dB and 85dB. In addition, after imposing the maximum tensile load, AE signals showed high amplitude and energy distribution. The AE amplitude showed between 45dB and 70dB. (3) A brittle fracture occurred at HF specimen which was tempered at $450^{\circ}C$ as if it is torn in the direction of $45^{\circ}$ on parallel area over the both sides of the tensile specimen, which lead to several peak appeared in AE energy. It was found that the AE amplitude was relatively low and the AE energy was high.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.32 no.2
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• pp.116-121
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• 2019

Hexagonal boron nitride particles (s-hBN) modified with 3-aminopropyl triethoxysilane (APTES) were used for the preparation of silicone composite materials. The microstructure of the composite materials was observed, and the thermal conduction and mechanical characteristics of the composite sheets were studied based on the compositions and microstructures. When a small amount of s-hBN particles was used, the thermal conductivity of the composite improved as a whole, and the tensile strength of the sheet also increased. The thermal conductivity and tensile strength of the composite in which a small amount of carbon fiber was added along with s-hBN were further improved. However, the use of carbon nanotubes with structural characteristics similar to those of carbon fiber resulted in lower thermal conductivity and tensile strength. Elastic silicone composites exhibiting 2.5 W/mK of thermal conductivity and a low hardness are expected to be used as thermally conductive interfacial sheet materials.

• Journal of Powder Materials
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• v.28 no.5
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• pp.375-380
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• 2021

In this study, we investigate the effect of the duration of mechanical alloying on the microstructures and mechanical properties of ODS ferritic/martensitic steel. The Fe(bal.)-10Cr-1Mo pre-alloyed powder and Y₂O₃ powder are mechanically alloyed for the different mechanical alloying duration (0 to 40 h) and then constantly fabricated using a uniaxial hot pressing process. Upon increasing the mechanical alloying time, the average powder diameter and crystallite size increased dramatically. In the initial stages within 5 h of mechanical alloying, inhomogeneous grain morphology is observed along with coarsened carbide and oxide distributions; thus, precipitate phases are temporarily observed between the two powders because of insufficient collision energy to get fragmented. After 40 h of the MA process, however, fine martensitic grains and uniformly distributed oxide particles are observed. This led to a favorable tensile strength and elongation at room temperature and 650℃.

• Transactions of Materials Processing
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• v.30 no.3
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• pp.134-141
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• 2021

In order to improve excessive spring-back behavior as a result of the roll forming process using ultra high strength steel (UHSS) sheet, local softening in region of a partial area expected to be deformed on an initial blank is considered in this study. With SPFC1470 UHSS sheet with initial blank thickness of 1.20mm, the local softening is performed with the following conditions: temperatures of 500℃, 550℃, 600℃ and 650℃, and holding time of 20s, 40s, 80s and 160s. Mechanical properties, such as yield stress and tensile strength, as well as elongation, are evaluated through uniaxial tensile tests, while the microstructural characteristics as a result of local softening are also investigated using the heat-treated specimens. As a result, it is shown that the spring-back behavior of the roll-formed prototype was reduced about by 78.9%, when the local softening at about 500℃ was performed for 160s considering the practical manufacturing condition.

• Korean Journal of Materials Research
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• v.33 no.1
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• pp.1-7
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• 2023

The physical and antibacterial properties of ophthalmic lenses fabricated by copolymerization with hydrogel monomers using two types of graphene were measured, and their usability as contact lens materials was analyzed. For polymerization, silicone monomers, including SID-OH, 3-(methacryloxy)propyl tris(trimethylsiloxy)silane, and decamethylcyclopentasiloxane, were used, and N,N-dimethylacetamide, ethylene glycol dimethacrylate as a crosslinking agent, and azobisisobutyronitrile as an initiator were added. Also, graphene oxide nanoparticle (GON) and graphene nanoplate (GNP) were used as an additive, and the physical properties of the lenses fabricated after copolymerization were evaluated. The fabricated lenses satisfied the basic physical properties of general hydrogel contact lenses and showed the characteristics of lenses with high water content, and the disadvantage of very weak durability, due to low tensile strength. However, it was confirmed that the tensile strength and antibacterial properties were greatly improved by adding GON and GNP. With GON, the oxygen permeability and refractive index of the fabricated lenses were slightly improved. Therefore, it was determined that the graphene materials used in this study can be used in various ways as a contact lens material.

• Progress in Superconductivity and Cryogenics
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• v.26 no.2
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• pp.19-23
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• 2024

3D printing has the advantage of being able to process various types of parts by layering materials. In addition to these advantages, 3D printing technology allows models to be processed quickly without any special work that can be used in different fields to produce workpieces for various purposes and shapes. This paper deals to not only increase the utilization of 3D printing technology, but also to revitalize 3D printing technology in applications that require similar cryogenic environments. The goal of this study is to identify the mechanical properties of polylactic acid and photopolymer resin processed by Fused Deposition Modeling (FDM) and Digital Light Processing (DLP) respectively. The entire process is meticulously examined, starting from getting the thermal contraction using an extensometer. A uniaxial tensile test is employed, which enables to obtain the mechanical properties of the samples at both room temperature (RT) and cryogenic temperature of 77 K. As the results, photopolymer resin exhibited higher tensile properties than polylactic acid at RT. However, at cryogenic temperatures (77 K), the photopolymer resin became brittle and failure occurred due to thermal contraction, while polylactic acid demonstrated superior tensile properties. Therefore, polylactic acid is more suitable for lower temperatures.

• Korean Journal of Materials Research
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• v.14 no.1
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• pp.73-77
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• 2004

The mechanical and electrical properties of $Cu-TiB_2$ composites prepared by hot extrusion and cold drawing according to the variation of $TiB_2$ contents and the size of $TiB_2$ particle have been studied. The experimental results showed that the electrical conductivity was decreased with increasing the $TiB_2$ content, and their tensile strength and hardness increased inversely. In the case of the same content of $TiB_2$ particle, the smaller $TiB_2$ particle, the higher their mechanical properties. The electrical conductivity of $Cu-TiB_2$ composites showed more than 70%IACS. Their yield strength and hardness were more than 120 MPa and HRB 60～70, respectively.