• Journal of Institute of Control, Robotics and Systems
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• v.6 no.8
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• pp.727-731
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• 2000

This paper presents a new practical autopilot design approach to acceleration control for tail-controlled STT(Skid-to-Turn) missiles. The approach is novel in that the proposed parametric affine missile model adopts acceleration as th controlled output and considers the couplings between the forces as well as the moments and control fin deflections. The aerodynamic coefficients in the proposed model are expressed in a closed form with fittable parameters over the whole operating range. The parameters are fitted from aerodynamic coefficient look-up tables by the function approximation technique which is based on the combination of local parametric models through curve fitting using the corresponding influence functions. In this paper in order to employ the results of parametric affine modeling in the autopilot controller design we derived a parametric affine missile model and designed a feedback linearizing controller for the obtained model. Stability analysis for the overall closed loop sys-tem is provided considering the uncertainties arising from approximation errors. the validity of the proposed modeling and control approach is demonstrated through simulations for an STT missile.

• Journal of the Korean Ceramic Society
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• v.33 no.4
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• pp.411-417
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• 1996

Ultrafine NiO/YSZ (Yttria Stabilized Zirconia) powders were made by using a glycine nitrate process which is used as anode material for solid oxide fuel cells. The specific surface areas of synthesized NiO/YSZ powders were examined with controlling pH of a precursor solution and the content of glycine. The binding of glycine with metal nitrates occurring in the precursor solution was analyzed by using FTIR. The characteristics of synthesized powders were examined with X-ray diffraction(XRD) Brunauer Emmett Teller with N2 absorption. scanning electron microscopy (SEM). and transmission electron microscopy (TEM). Ultrafine NiO/YSZ powders of 15-18 m2/g were obtained through GNP when the content of glycine was controlled to 1 or 2 times the stoichiometric ratio in the precursor solutions. Strongly acid precursor solution increased the specific surface area of the synthesized powders. This is suggested to be the increased binding of metal nitrates and glycine under a strong acid solution of pH=0.5 that lets glycine consist of mainly the amine group of {{{{ { NH}`_{3 } ^{+ } }}. After sintering and reducing treatment of NiO/YSZ powders synthesized by GNP the Ni/YSZ pellet showed ideal microstructure where very fine Ni particles of 3-5 ${\mu}{\textrm}{m}$ were distributed uniformly and fine pore around Ni metal particles was formed. leading to anincrease of the triple phase boundary among gas Ni and YSZ.

• Korean Journal of Materials Research
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• v.21 no.2
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• pp.83-88
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• 2011

Nano-technology is a super microscopic technology to deal with structures of 100 nm or smaller. This technology also involves the developing of $TiO_2$ materials or $TiO_2$ devices within that size. The aim of the present paper is to synthesize $WO_x$ doped nano-$TiO_2$ by the Sonochemistry method and to evaluate the effect of different percentages (0.5-5 wt%) of tungsten oxide load on $TiO_2$ in methylene blue (MB) elimination. The samples were characterized using such different techniques as X-ray diffraction (XRD), TEM, SEM, and UV-VIS absorption spectra. The photo-catalytic activity of tungsten oxide doped $TiO_2$ was evaluated through the elimination of methylene blue using UV-irradiation (315-400nm). The best result was found with 5 wt% $WO_x$ doped $TiO_2$. It has been confirmed that $WO_x-TiO_2$ could be excited by visible light (E<3.2 eV) and that the recombination rate of electrons/holes in $WO_x-TiO_2$ declined due to the existence of $WO_x$ doped in $TiO_2$.

• Journal of Sensor Science and Technology
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• v.20 no.5
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• pp.305-310
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• 2011

This study focuses on the fabrication of $TiO_2$ nanosheets and their gas sensor application. A simple sonochemical method is employed to fabricate the $TiO_2$ nanosheets. The obtained samples were investigated by transmission electron microscope(TEM) and X-ray Diffraction(XRD). The $TiO_2$ nanosheets were coated on substrates by a dropping method followed by heat treatment. The sensor responses to volatile organic compounds(VOCs) such as toluene, benzene, ethanol and acetaldehyde were studied. It was found that the $TiO_2$ nanosheets sensors are able to detect ppb-levels of VOC gases.

• Journal of the Korean Vacuum Society
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• v.2 no.4
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• pp.501-506
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• 1993

The spatial potential distribution of electron cyclotron resonance plasma is measured as a function of tehsubstrate DC bias by Langmuir probe method. It is observed that the substrate DC bias changes the slope of the plasma potential near the subsrate, resulting in changes in flux and energy of the impinging ions across plasma $_strate boundary along themagnetric field. The effect of the substrate DC bias on the low-temperature silicon homoepitaxy (below $560^{\circ}C$) is examine dby in situ reflection high energy electron diffraction (RHEED), cross-section transmission electron microscopy (XTEM),plan-view TEM and high resolution transmision electron microscopy(HRTEM). While the polycrystalline silicon layers are grow withnegative substrate biases, the single crystaline silicon layers are grown with negative substrate biases, the singel crystalline silicon layers are grown with positive substrate biases. As the substrate bias changes form negative to positive values, the growth rate decreases. It is concluded that the control of the ion energy during plasma deposition is very important in silicon epitaxy at low temperatures below $560^{\circ}C$ by UHV-ECRCVD.VD.

• Journal of the Korean Vacuum Society
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• v.4 no.1
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• pp.109-117
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• 1995

고에너지 이온주입시 격자결함의 생성 및 열처리 거동이 double crystal X-ray와 단면 TEM을 사용하여 연구되었다. 3MeV P+ 이온주입한 실리콘의 DCXRD 분석 결과조사량 증가에 따라 모재 내의 변형량은 증가하였다. HRTEM 분석 결과 고에너지 이온주입시 결함은 표면 부근에 희박하고 Rp 부근에 집중되어 있었다. 또한 이온주입 상태의 결함층은 dark band의 형태로 존재하였으며 열처리시 이차결함은 이곳으로부터 생성됨이 관찰되었다. 3MeV P+,$1X1015extrm{cm}^2$의 조건으로 이온주입된 실리콘 시편의 열처리에 따른 X-ray rocking curve 분석을 통하여 열처리 온도가 $550^{\circ}C$에서 $700^{\circ}C$로 증가함에 따라 모재 내부의 최대 변형량이 7X10-4에서 2.9X10-4으로 감소함이 관찰되었다. 특히 $550^{\circ}C$ 열처리한 시편의 경우 표면으로부터$-1.5mu$m 영역에 작은 변형층이 넓게 잔존하였으며 열처리온도를 $700^{\circ}C$로 증가한 경우 제거되었다. 이온주입시 생성된 일차결함들은 $700^{\circ}C$ 열처리시 $60^{\circ}$ 전위와 <112> 막대 모양 결함, $1000^{\circ}C$ 열처리시 <110>방향의 전위루프로 열처리 조건에 따라 여러 가지 모양의 이차결함으로 변화하였다. 고에너지 이온주입에 의해 발생한 이차결함은 고온에서도 안정하여 고온 열처리에 의한 제거가 용이하지 않았다.

• Korean Journal of Materials Research
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• v.16 no.3
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• pp.198-202
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• 2006

Cadmium selenide (CdSe) nanoparticles with the diameter of about 3.4nm have been synthesized from the mixed aqueous solution of distilled water and diethanolamine at room temperature. The cadmium chloride ($CdCl_2$), sodium selenosulfate ($Na_2SeSO_3$) were used as the cadmium and selenium source, respectively. The properties of CdSe nanoparticles were characterized by using transmission electron microscopy (TEM), X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD) and UV-Vis measurements. CdSe nanoparticles were analyzed to be cubic phase with the absorption excition peaks between 540 and 600 nm. CdSe nanoparticles also showed red-shifted excition peaks with increasing the sonication time. This paper mainly presents the sonication effects on the formation of CdSe nanoparticles prepared from the mixed aqueous solution of distilled water and diethanolamine.

• Korean Journal of Fisheries and Aquatic Sciences
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• v.38 no.2
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• pp.94-99
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• 2005

The gametogenesis of the surf clam, Tresus keenae, were investigated by SEM and TEM. Both the testis and the ovary had follicle tubes surrounded by inter-tubal tissue composed of adipogranular cells that provided storage function. In the vitellogenic oocyte, lipid droplets and lipid yolk granules were found in the vacuoles formed by the Golgi apparatus. Proteid yolk granules were formed by the endoplasmic reticulum and cortical granules in the cytoplasm during vitellogenesis. The mature sperm was primitive and resembled a jar with a cover. The sperm heads were approximately $2.00-2.30 {\cal}um$. The acrosomal rod projected in front of the acrosome. In addition, four large mitochondria were in the midpiece.

• Journal of the Korean Ceramic Society
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• v.30 no.3
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• pp.222-228
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• 1993

In order to obtian TiO2 fine powder of high purity, the new method which is different from the sulfate process and the chloride one was employed. TiO2 was syntehsized by the reaction between elemental titanium particles and H2O2 solutiosn at 30~7$0^{\circ}C$, and then TiO2 powder was characterized using XRD, SEM, TEM, DTA and FT-IR. It was found that the initial reaction rate was fast at a high temperature due to the high generation of activated oxygen associated with thedecomposition of H2O2. However, the reaction was slowly proceeded at a low temperature due to slow decomposition of H2O2. In this experimental range, the optimum temeprature was ocnsidered to be about 5$0^{\circ}C$. The primary particles of the hydrous titanium dioxide (TiO2 gel) before aging were spherical, and their mean sizes were about 50nm. The similar shapes and sizes were observed with calcinatin at 40$0^{\circ}C$. The FT-IR spectrum of Ti-OH in the TiO2 gel powder appeared at around 3380cm-1, 1630cm-1 and 530cm-1. This gel powder was crystallized into the anatase type TiO2 at 300~40$0^{\circ}C$.

• Journal of the Korean Ceramic Society
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• v.35 no.4
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• pp.378-384
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• 1998

We investigated the possibility of systemizing data for the colour gradation of classical ceramics by build-ing program and D-basing each data information in pottery field that has been fall behind in forming data be-cause of many variable and lacking of data system. In this study we manufactured $CoAl_2O_4$ stain that has stable spinel structure at high temperature and then mixed base glaze with stain for the additive per-centage of 0.5 , 1, 5, 10, 15 wt% In thie colouring of Lime base glaze with the wide ranged melting tem-perature the colour development of cobalt-blue sintered at $1250^{\circ}C$ is better than that of $1150^{\circ}C$ $1350^{\circ}C$ The experimental conditions and data are D-based simulated programming of computer. The result of -based data appeared to be more smoothed fusion-adherence in the Matt glaze range of Lime base glaze, The variation of colouring is not found when additive content of glaze is more than 5 wt% and the stable colour development of stain was shown at the content that RO, $R_2O$ percentage is high (the content that R2O3 per-centage is low)