• Restorative Dentistry and Endodontics
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• 제46권1호
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• pp.6.1-6.10
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• 2021

Objectives: The aim of this study was to evaluate the corrosion resistance of heat-treated (Reciproc and WaveOne) and non-heat-treated (ProTaper and Mtwo) superelastic nickel-titanium endodontic files when immersed in a 5.25% sodium hypochlorite solution. Materials and Methods: Anodic polarization curves were obtained with potential sweeps that began at the open circuit potential or corrosion potential (E_corr). The pitting potential (E_pit) was identified on the anodic polarization curve as the potential at which a sudden increase in current was observed. The micromorphology of the 28 tested files was analyzed before and after the electrochemical assay using scanning electron microscope (SEM). The data were analyzed using 1-way analysis of variance with the post hoc Bonferroni test (for E_corr) and the Student t-test for independent samples (for E_pit). Results: The mean E_corr values were 0.506 V for ProTaper, 0.348 V for Mtwo, 0.542 V for Reciproc, and 0.321 V for WaveOne files. Only WaveOne and Protaper files exhibited pitting corrosion, with E_pit values of 0.879 V and 0.904 V, respectively. On the SEM images of the ProTaper and WaveOne files, cavities suggestive of pitting corrosion were detected. Conclusions: Signs of corrosion were observed in both heat-treated and non-heat-treated files. Of the evaluated files, WaveOne (a heat-treated file) and ProTaper (a non-heat-treated file) exhibited the lowest corrosion resistance.

• 대한기계학회논문집
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• 제10권5호
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• pp.625-634
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• 1986

본 연구에서는 알루미늄 합금인 알루미늄 2014와 6061의 이재를 V형 맞대기 이음을 한 후 정적인장하중을 가하여 모아레법에 광탄성 피복법을 조합한 방법에 의 해 변형율을 실시간(real time)에서 측정하고 유한요소법으로 해석한 결과와 비교검 토하였다.

• 한국자기학회지
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• 제7권4호
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• pp.180-185
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• 1997

비정질 리본으로 제조된 링 코아 시편의 자장중 열처리 조건에 따른 철손 및 보자력 등의 연자기 특성 변화를 BH loop tracer를 이용하여 최대인가자기유도 0.1 T를 유지하면서 10 kHz에서 측정하였다. 열처리 시간이 증가함에 따라 코아의 철손 및 보자력은 감소하여 최소값에 도달한 다음 다시 증가한다. 공기 중에서 열처리한 경우의 시료가 Ar 분위기에서 열처리한 시료 보다 우수한 연자기 특성을 나타낸다. 코아의 원주방향으로 자장을 인가한 경우에는 인가자장의 세기가 6 Oe 이상이어야 자장중 열처리 효과가 나타나 철손 및 보자력이 감소하였으며, 냉각시 Curie 온도근처에서의 냉각속도가 빠를 수록 철손과 보자력은 감소한다. 코아의 폭 방향으로 자장을 인가한 경우에는 보자력의 증가와 투자율의 감소 및 약간의 철손 증가가 나타났다.

• 열처리공학회지
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• 제26권6호
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• pp.279-287
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• 2013

Oxide Dispersion Strengthened (ODS) Fe with $Al_2O_3$ dispersoid was successfully produced by reactive milling with a mixture of Fe, $Fe_3O_4$ (Magnetite), $Fe_2O_3$ (Hematite) and Al reactants at cryogenic temperature. The milled powders were consolidated by Vacuum Hot Press (HP) at 1323 K, and the consolidated materials were characterized by Transmission Electron Microscopy (TEM), Scanning Transmission Electron Microscopy (STEM), and Energy Dispersive Spectroscopy (EDS); the yield strength and the hardness of the consolidated materials were determined by compressive test and Vickers hardness test at room temperature. The grain size of the materials was estimated by X-ray Diffraction technique using the scherrer's formula. The TEM observations showed that the microstructure was comprised with a mixture of nanocrystalline Fe matrix and $Al_2O_3$ nano-dispersoids with a bimodal size distribution; the 0.2% off-set yield strength of the materials was as high as $758{\pm}29$ MPa and the Vickers hardness was $358{\pm}2$. The effect of the cryogenic milling and addition of extra Fe powder was discussed on the suppression of MSR (Mechanically induced Self-sustaining Reaction) for the desired microstructural evolution of ODS alloys.

• 한국주조공학회지
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• 제19권6호
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• pp.456-465
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• 1999

The overall objective of this study is to investigate the effect of Ag addition on the mechanical properties and microstructure of rapid solidified 7000 Al series alloys. Al-Zn-Mg-Cu alloys with small amounts of Ag was fabricated into the powder by gas atomization. The powder was extruded after the cold compaction and degassing and then followed by T6 heat treatment. Microstructure observation, phase analysis, room and high temperature tensile test and hardness test were pursued. The tensile strength and hardness of Ag-added alloy after heat treatment was increased with increasing Ag contents. However, the elongation of extruded alloys was not increased as much as to be expected. The reason of this result seems to be related to $the{\Omega}$ phase, which contribute to the high temperature strength stability of Al-Cu-Zn alloys through the formation of eutectoid with Ag addition.

• 한국주조공학회지
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• 제32권6호
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• pp.284-288
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• 2012

The effects of Si content on the variation of microstructure and processing window of austempered ductile cast iron were investigated. Four different Si contents between 2.42 and 3.37 wt.% were used. The influence of silicon on the microstructure and processing window of these materials were studied. Austenitizing was performed at $900^{\circ}C$ for 60min and austempering temperature were both $340^{\circ}C$ and $360^{\circ}C$ and austempering time were for 4min upto 119min and for 5min upto 160min respectively. After heat treatment, the evolution of stage I and stage II were performed by optical metallography, XRD, hardness test. The results showed that $t_2$ was delayed as Si contents was increased due to the fact that Si retarded the formation of cementite ($Fe_3C$). The high silicon content promoted the stability of the metastable two-phase combination of austenite and ausferrite.

• 열처리공학회지
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• 제14권2호
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• pp.89-95
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• 2001

The 7175Al alloy is particularly interesting for its high strength and sufficient ductility, fracture toughness and corrosion resistance. Currently vigorous efforts have been made to develop large rockets usable for various purposes in the space. This has created the demand of big size of 7175Al billet which would be applied to heavy forgings. The aim of this study is to investigate the quality level of big billet and the effect of billet size on the mechanical properties of large 7175Al ring roll forgings. The billets range from 370 mm to 720 mm in diameter were homogenized and forged after direct chill casting. The size and volume fraction of second phase particles In ${\Phi}720$ mm billet are larger than those of ${\Phi}370$ mm billet, and its ductility is lower for the condition of homogenization and T6 treatment. The Cu-rich phases formed in interdendritic sites are considered to provide the preferential crack path during cold upsetting. The fracture toughness of ring roll forgings which are made by ${\Phi}370$ mm billet is higher than those of ${\Phi}720$ mm billet.

• Corrosion Science and Technology
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• 제16권6호
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• pp.305-316
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• 2017

Austenitic stainless steels have been widely used for various systems of nuclear power plants. Among these stainless steels, small pipes with diameter less than 14 inch have been produced in the form of seamless pipe. Annealing and cooling process during the manufacturing process can affect corrosion properties of seamless stainless steels. Therefore, 12 inch-diameter of as-received 304L stainless steel pipe was annealed and aged in this study. Intergranular corrosion resistance was evaluated by ASTM A262 Practice A, C, and E methods. The degree of sensitization was determined using a DL-EPR test. U-bend method in an autoclave was used to evaluate the SCC resistance in 0.01 M $Na_2S_4O_6$ or 40% NaOH solution at $340^{\circ}C$. As-received specimen showed relatively high degree of sensitization and intergranular corrosion rate. Carbon segregation was also observed near grain boundaries. Annealing treatment could give the dissolution of segregated carbon into the matrix. Aging treatment could induce segregation of carbon and finally form carbides. Microstructural analysis confirmed that high intergranular corrosion rate of the as-received seamless pipe was due to micro-galvanic corrosion between carbon segregation and grains.

• 열처리공학회지
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• 제35권6호
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• pp.303-313
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• 2022

The purpose of this study was to test and analyze the effects of the mechanical properties and structural changes of the austenitized and tempered martensite STS 410 stainless steel containing 11.5~13%Cr and 0.10%C on its temper embrittlement. The STS 410 stainless steel test pieces for each 3 hours at 960℃, 1000℃ and then, tempered them for 2 hours at 300℃, 350℃, 400℃, 450℃, 500℃, 550℃, 600℃, 650℃ and 700℃ known as the intervals vulnerable to temper embrittlement to observe the changes of their structures and mechanical properties. In case autenitizing was insufficient due to lower temperature of thermal treatment for solution, unsolved carbides and ferrites remained in the structure after quenching, which meant that the parts could wear out and corrode to embrittle at the room temperature. Elongation and impact energy changes with Tempering conditions showed minimum results in range of 400~500℃. The decrease in elongation and impact energy at 400~500℃ was the hardening effect of the subgrain due to the precipitation of many M₃C or M₇C₃, M₂₃C₆. And STS 410 stainless steel corrosion tested in 10% NaCl solution at 30℃ after tempering treatment. The degree of corrosion sensitization showed increasing tendency with increase of tempering temperature and Cr carbide precipitation were observed in grain boundary.

• 동력기계공학회지
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• 제15권6호
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• pp.73-80
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• 2011

The experimental investigation focuses on an influence of artificial aging time in longitudinal butt welded Al 6013-T4 aluminum alloy on the fatigue crack growth resistance. The preferred welding processes for this alloy are frequently tungsten inert gas welding (TIG) process due to its comparatively easier applicability and better weldability than other gas metal arc welding. Fatigue crack growth tests were carried out on compact tension specimens (CT) in longitudinal butt TIG welded after T82 heat treatment was varied in three artificial aging times of 6 hours, 18 hours and 24 hours. Of the three artificial aging times, 24 hours of artificial aging time are offering better resistance against the growing fatigue cracks. The superior fatigue crack growth resistance preferred spatial variation of materials within each specimen in the Paris equation based on reliability theory and fatigue crack growth rate by crack length are found to be the reasons for superior fatigue resistance of 24 hours of artificial aging time was compared to other joints. The highest of crack propagation resistance occurs in artificial aging times of 24 hours due to the increase in grain size (fine grained microstructures).