• Title/Summary/Keyword: T1 relaxation time

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Evaluation on Clamping Force of High Strength Bolts By Coating Parameters of Faying Surfaces (고력볼트 접합부표면의 방식도장변수에 따른 체결력 평가)

  • Nah, Hwan Seon;Lee, Hyeon Ju
    • Corrosion Science and Technology
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    • v.11 no.2
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    • pp.48-55
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    • 2012
  • Clamping force of a high strength bolt is reduced by a certain period of time after the initial set-up. In case of special treatments on faying surfaces such as protective coating, clamping force is relaxed more severely. Tests for slip critical joints subject to various faying surface parameters were conducted. Five different surface treatments were tested including mill scale surface, blast surface, rust surface and coated surfaces. Each specimen was composed of F10T M20 of high strength bolts and steel plates. Based on the result of slip coefficient test, blast treatment surface showed 0.59, rust treatment surface showed 0.54 and inorganic zinc treatment surface exhibited 0.44. Clean mill treatment surface and red lead paint treatment surface were 0.23, 0.21 respectively. It is identified that the slip coefficient in Korean structural design guide should be determined for various surface conditions. Subsequently from long term relaxation test of ASTM A 490 high strength bolts, relaxation of no-coated surfaces such as blast, clean mill, rust treatment, the loss of initial clamping load was 10.5%, 13.6% and 7.9% for 1,000 hours, while the loss of initial clamping force was reached as 15.0%, 18.7% more than the required redundancy 10% in case of inorganic zinc and red lead painted treatment. It is required that the limit of relaxation on coated faying surface should be established separately for various surfaces.

NMR Study of the Electrooptic Material $KTiOPO_4(KTP)$ (Electrooptic 물질 $KTiOPO_4(KTP)$의 핵자기공명 연구)

  • 한정관;오동근;이창훈;이철의;김정남;김성철
    • Journal of the Korean Magnetics Society
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    • v.6 no.5
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    • pp.294-297
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    • 1996
  • We have carried out a $^{31}P$ nuclear magnetic resonance (NMR) study on the electrooptic material $KTiOPO_{4}(KTP)$. From the spin -lattice relaxation time ($T_{1}$) measurements at 17.9 MHz in the temperature range 77-390 K, two phase transitions associated with the change of the dominant charge carriers were observed and the activation energies were obtained in each phase.

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The ALTADENA and PASADENA studies in benchtop NMR spectrometer

  • So, Howon;Jeong, Keunhong
    • Journal of the Korean Magnetic Resonance Society
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    • v.23 no.1
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    • pp.6-11
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    • 2019
  • Parahydrogen induced hyperpolarization (PHIP) technique is extensively studied to increase the sensitivity of the conventional NMR spectroscopy and recently try to apply this advanced technique into the revolutionary future of the MRI. The other hyperpolarization technique, which is widely utilized, is DNP (Dynamic Nuclear Polarization)-based hyperpolarization one. Despite its great advances in these fields, it contains several drawbacks to overcome: fast relaxation time, expensive equipment is needed, long build-up time is required (several hours), and batch scale material is hyperpolarized. To overcome all those limitations, one can effectively harness the hyperpolarized spin state of parahydrogen. One important step for utilizing the spin state of parahydrogen is doing well-developed experiments of ALTADENA and PASADENA. Based on those concepts, we successfully obtain the hydrogenation signals of ALTADENA and PASADENA from styrene by using benchtop NMR spectrometer. Also those signals were conceptually analyzed and confirmed with different mechanisms. To our best knowledge, those experiments using 1.4T (benchtop NMR) is the first reported one. Considering these experiments, we hope that parahydrogen-based hyperpolarization transfer studies in NMR/MRI will be broadened in Korea in the future.

Dual Component Analysis for In Vivo T2* Decay of Hyperpolarized 13C Metabolites

  • Joe, Eunhae;Lee, Joonsung;Lee, Hansol;Yang, Seungwook;Choi, Young-Suk;Wang, Eunkyung;Song, Ho-Taek;Kim, Dong-Hyun
    • Investigative Magnetic Resonance Imaging
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    • v.21 no.1
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    • pp.1-8
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    • 2017
  • Purpose: To investigate the exchange and redistribution of hyperpolarized $^{13}C$ metabolites between different pools by temporally analyzing the relative fraction of dual $T_2{^*}$ components of hyperpolarized $^{13}C$ metabolites. Materials and Methods: A dual exponential decay analysis of $T_2{^*}$ is performed for [1-$^{13}C$] pyruvate and [1-$^{13}C$] lactate using nonspatially resolved dynamic $^{13}C$ MR spectroscopy from mice brains with tumors (n = 3) and without (n = 4) tumors. The values of shorter and longer $T_2{^*}$ components are explored when fitted from averaged spectrum and temporal variations of their fractions. Results: The $T_2{^*}$ values were not significantly different between the tumor and control groups, but the fraction of longer $T_2{^*}$ [1-$^{13}C$] lactate components was more than 10% in the tumor group over that of the controls (P < 0.1). The fraction of shorter $T_2{^*}$ components of [1-$^{13}C$] pyruvate showed an increasing tendency while that of the [1-$^{13}C$] lactate was decreasing over time. The slopes of the changing fraction were steeper for the tumor group than the controls, especially for lactate (P < 0.01). In both pyruvate and lactate, the fraction of the shorter $T_2{^*}$ component was always greater than the longer $T_2{^*}$ component over time. Conclusion: The exchange and redistribution of pyruvate and lactate between different pools was investigated by dual component analysis of the free induction decay signal from hyperpolarized $^{13}C$ experiments. Tumor and control groups showed differences in their fractions rather than the values of longer and shorter $T_2{^*}$ components. Fraction changing dynamics may provide an aspect for extravasation and membrane transport of pyruvate and lactate, and will be useful to determine the appropriate time window for acquisition of hyperpolarized $^{13}C$ images.

Efficient Algorithm for the Solidification Simulation by FDM (FDM에 의한 응고해석시 계산기간 단축을 위한 Algorithm연구)

  • Lee, Jae-Kyung;Jeon, Ju-Mae;Jun, Ghi-Chan
    • Journal of Korea Foundry Society
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    • v.14 no.5
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    • pp.412-418
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    • 1994
  • Efficient algorithm for the solidification simulation by FDM is described from the practical point of views. If a proper time step ${\Delta}t$ is selected, the calculation is accelerated by implicit algorithm with the temperature recovery method of latent heat method. The implicit routine in the calculation is processed by SOR method(relaxation factor=1.5, truncation error=$10^{-4}$). The calculation is more accelerated by linear-interpolated explicite algorithm with a time step larger than the minimum value of the time step. This explicit method, which is applicable to the practical casting simulation problems, produces almost same results with about 40% faster calculation speed compared with the conventional explicit method.

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The Synthesis and MR Properties of New Macromolecular MR Contrast Agent (새로운 거대분자 MR 조영제의 합성 및 MR 특성에 관한 연구)

  • 장용민;장영환;황문정;박현정;전경녀;이종민;배경수;강봉석
    • Investigative Magnetic Resonance Imaging
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    • v.6 no.1
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    • pp.35-40
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    • 2002
  • Purpose : To evaluate the NMR relaxation properties and imaging characteristics of tissue-specificity for a newly developed macromolecular MR agent. Materials and methods : Phthalocyanine (PC) was chelated with paramagnetic ion, Mn.2.01g (5.2 mmol) of Phthalocyanine was mixed with 0.37g (1.4 mmol) of Mn chloride at $310^{\circ}C$ for 36 hours and then purified by chromatography (CHC13/CH3OH 98/2 v/v, Rf, 0.76) to obtain 1.04g (46%) of MnPC (molecular weight= 2000d). The $T1}T2$ relaxivity of MnPC was measured in 1.5T(64 MHz) MR using 0.1 mM MnPC. The MR image characteristics of MnPC was evaluated using spin-echo (TR/TE=500/14 msec) and gradient-echo (FLASH) (TR/TE=80/4 msec, flip angle=60) techniques in 1.57 MR scanner. The images of rabbit liver were obtained every 10 minutes up to 4 hours. To study the effect of concentration on image, 20 mM, 50 mM, 100 mM of MnPC were tested. Results : The relaxivities of MnPC at 1.5T(64MHz) were Rl=7.28 $mM^{-1}S^{-1},{\;}R2=55.56mM^{-1}S^{-1}$. Compared to the values of Gd-DTPA (Rl[=4.8 $mM^{-1}S^{-1})$], R2[=5.2 $mM^{-1}S^{-1}])$]), both T1/T2 relaxivities of MnPC were higher than those of Gd-DTPA. For both of SE and FLASH techniques, the contrast enhancement reached maximum at 10 minutes after bolus injection and the enhancement continued for more than 2 hours. When compared with small molecular weight liver agents such as Gd-EOB-DTPA, Gd-BOPTA and MnDPDP, MnPC was characterized by more prolonged enhancement time. The time course of MR images also revealed biliary excretion of MnPC. Conclusion : We developed a new macromolecular MR agent, MnPC. The relaxivities of MnPC were higher than those of small molecular weight Gd-chelate. Hepatic uptake and biliary excretion of MnPC suggests that this agent is a new liver-specific MR agent.

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Effects of the Structured Nursing Intervention Program on Dysmenorrhea of Middle School Girls (구조화된 간호중재 프로그램이 여중생의 월경곤란증 완화에 미치는 영향)

  • Choi, Soung-Hee;Kim, Hyeon Ok
    • Journal of the Korean Society of School Health
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    • v.14 no.1
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    • pp.145-160
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    • 2001
  • The main purpose of this study is to identify the effects of a structured nursing intervention program on dysmenorrhea in middle school girls. This study employed two methods of research at the same time: a quasi-experiment pre- and post-test to use for comparison. Subjects were middle school girls assigned to the research program: 40 girls in the second grade, 40 girls in the third grade at K Girls' Middle School and H Girls' Middle School located in J city. The data were collected for 68 days from August 23 to October 30, 1999. The data were collected by observation technique and by a self-administered questionnaire. The instruments used for this study were as follows: the "Face Interval Pain Scale" menstrual pain instrument developed by McGreth(1987) and the "Menstrual Distress Questionnaire" dysmenorrhea instrument developed by Moos(1968). The dysmenorrhea knowledge instrument was developed by the researcher and refered to above. The research procedure was as follows: after preliminary examination, the experimental groups were provided educational programs with O.H.P. films developed by the researcher and with the videotape "first meeting" supported by P&G company and produced by EBS. The groups followed the educational programs twice for two weeks. At the beginning of menstruation, these subjects could choose one among the following choices: * Jacobson's progressively muscle relaxation method and massage treatment * Jacobson's progressively muscle relaxation method and hot bag treatment * Jacobson's progressively muscle relaxation method, a pain killer treatment, and massage treatment * Jacobson's progressively muscle relaxation method, a pain killer treatment, and hot bag treatment The dysmenorrhea of the control group were measured during the same period. The analysis of the collected data was done using an SPSS-PC+, descriptive statistic including real numbers, percentage, averages, standard deviations and t-test, $x^2$ test, and ANCOVA. The results of this study were as follows. (1) The knowledge level of the girls provided with the planned nursing intervention program was higher when compared to these who did not follow the educational programs. (2) The original difference in the dysmenorrhea level having been controled, the dysmenorrhea level made, nevertheless, a statistical difference between the experimental group and the control group(F=63.8, p=.00). Observed pain on quantity measurement of dysmenorrhea showed significant difference depending on the treatment(t=4.6, p=.00). In conclusion, those in the planned nursing intervention program had a higher knowledge level and fewer symptoms than the control group. Accordingly, the nursing intervention program for dysmenorrhea developed by the researcher can be effectively applied in nursing practice and can be the foundation for this kind of program.

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The Effect of Number of Echoes and Random Noise on T2 Relaxography : Development of 8-Echo CPMG (에코의 개수와 임의 잡음이 T2 이완영상의 구성에 미치는 영향연구 : 8에코 CPMG영상화 펄스열의 개발)

  • 정은기
    • Investigative Magnetic Resonance Imaging
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    • v.2 no.1
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    • pp.67-72
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    • 1998
  • The mapping of the spin-spin relaxation time T2 in pixel-by-pixel was suggested as a quantitative diagnostic tool in medicine. although the CPMG pulse sequence has been known to be the best pulse sequence for T2 measurement in physics NMR, the supplied pulse sequence by the manufacture of MRI system was able to obtain the maximum of 4 CPMG images. Eight or more images with different echo time TEs are required to construct a reliable T2 map, so that two or more acquisitions were required, which easily took more than 10 minutes. 4-echo CPMG imaging pulse sequence was modified to generate the maximum of 8 MR images with evenly spaced echo time TEs. In human MR imaging, since patients tend to move at least several pixels between the different acquisitions, 8-echo CPMG imaging sequence reduces the acquisition time and may remove any mis-regitration of each pixels signal for the fitting of T2. The resultant T2 maps using the theoretically simulated images and using the MR images of the human brain suggested that 8 echo CPMG sequence with short echo spacing such as 17-20 msec can give the reliable T2 map.

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Aging Diagnosis of Underground Distribution Power Cables by Isothermal Relaxation Current Measurement Equipment (완화전류 측정에 의한 지중배전케이블의 열화진단)

  • Kim, Ju-Yong;Song, Il-Keun;Kim, Dong-Myung;Yun, Tae-Sang;Jeong, Sang-Bong
    • Proceedings of the Korean Institute of IIIuminating and Electrical Installation Engineers Conference
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    • 2004.05a
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    • pp.502-505
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    • 2004
  • The purpose of this experiment is to modify diagnosis criterion of isothermal relaxation current(IRC) measurement equipment which is using for distribution cable diagnosis. We're using this system for several years in the field instead of DC leakage current measurement and lots of cables were replaced. But we have to investigate on the reliability of this equipment for our cables because we didn't carried out condition assessment of extracted cables after field diagnosis by this equipment. It is important thing for cable maintenance. If the replacement criterion is improper we can not prevent failures or will waste budget on account of replacement of the sound cables. In this papar we selected field installed cables and injected silicone fluid to the cables for insulation rehabilitation. In order to prove reliability of the diagnosis equipment we compared diagnosis results and AC breakdown strength according to operating time after silicone treatment. This is the results of the field test for 1 year.

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Aging Diagnosis and Characteristic Analysis of Distribution ,Power Cables I to Prepare Optimal Replacement Criterion (지중 배전케이블의 최적 교체기준 수립을 위한 열화진단 및 특성분석)

  • 김주용;송일근;정익중;한명관;심유종;문재덕
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.53 no.5
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    • pp.258-263
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    • 2004
  • The purpose of this experiment is to modify diagnosis criterion of isothermal relaxation current(IRC) measurement equipment which is using for distribution cable diagnosis. We're using this system for several years in the field instead of DC leakage current measurement and lots of cables were replaced. But we have to investigate on the reliability of this equipment for our cables because we didn't carried out condition assessment of extracted cables after field diagnosis by this equipment. It is important thing for cable maintenance. If the replacement criterion is improper we can not prevent failures or will waste budget on account of replacement of the sound cables. In this paper we selected field installed cables and injected silicone fluid to the cables for insulation rehabilitation. In order to prove reliability of the diagnosis equipment we compared diagnosis results and AC breakdown strength according to operating time after silicone treatment. This is the results of the field test for 1 year.