• Title/Summary/Keyword: Synthesis value

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Temperature Profile Analysis of $Ti5_Si_3$ in Self-Propagating High Temperature Synthesis (SHS 법에 의한 $Ti5_Si_3$의 합성시 온도 Profile 분석)

  • 김도경;이형직;김익진;이형복
    • Journal of the Korean Ceramic Society
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    • v.32 no.3
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    • pp.341-348
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    • 1995
  • An analysis of the use of temperature profiles in the determination of the kinetic parameters of combustion synthesis of Ti5Si3 were investigated. From profile analysis, an apparent activation energy of 12KJ/mol was calculated. The Maximum heating rate achieved during 10wt% Ti5Si3 reaction by the product dilution method was approximately $1.5\times$104 K/s. Coupling this value with the measured wave velocity of 7.02 cm/s yields a maximum thermal gradient of 2.14$\times$103 K/cm. The value of tr (=t*) was calculated to be 1.2$\times$10-1 s and the value of td (=tx) was calculated to be 32.89 s. Using the definition of t* and the measured wave velocity, the effective thermal diffusivity, $\alpha$, was calculated to be 0.59$\times$10 $\textrm{cm}^2$/s. From these analysis, the power function, G, was also calculated.

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Hydrothermal Synthesis of Rod-like Copper Oxide Crystals

  • Pee, Jae-Hwan;Lee, Dong-Wook;Kim, Ung-Soo;Choi, Eui-Seok
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.167-168
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    • 2006
  • A hyrdrothermal synthesis has been developd to prepare rod-like crystals of copper oxide using copper nitrate trihydrate as a function of synthesis temperature, stirring speed and solution pH value. The properties of the fabricated crystals were studied using scanning electron microscopy, X-ray diffraction and particle size analysis. The morphology of the synthesized CuO was dependent on both the pH value of the solution and the morphology of the seed materials. Synthesized particles have regular morphologies and a uniform size distribution.

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A Study on Synthesis and Characteristics of the Optimum Urea Type Greaes for Rolling Bearings (구름베어링용 우레아계 최적 그리이스의 합성과 특성평가)

  • Han, Jong-Dae;Kim, Sang-Keun;Kim, Byung-Kwan
    • Tribology and Lubricants
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    • v.22 no.5
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    • pp.269-275
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    • 2006
  • Rolling bearings are classified one of the most important machine elements. The various function of bearings are greatly influenced by grease, and higher performance of rolling bearing greases is required to improve bearing lubrication. Three urea/ether oil greases with different composition were synthesized to compare the performance of these greases. The typical grease physical properties were investigated, and life test of these greases was conducted by FE-9 grease life tester. The grease with higher content of the thickener showed higher performance. After these preliminary test, twelve greases were synthesized and evaluated the performance of dropping point and OIT value. And optimized conditions for grease synthesis were selected by SSRED (Six Sigma Robust Engineering Design) using dropping point and OIT value respectively. The optimized grease using OIT value showed longer grease life than that using dropping point. Two greases were synthesized following the optimum synthesis conditions by means of OIT value. Then grease life and other properties of these greases were investigated. These two greasaes showed longer grease life than typical urea/ether oil grease.

Compound Outlier Assessment and Verification for Multiple Field Monitoring Data (다수 계측 데이터에 대한 복합 이상치 평가 및 검증)

  • Jeon, Jesung
    • Journal of the Korean GEO-environmental Society
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    • v.19 no.1
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    • pp.5-14
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    • 2018
  • All kinds of monitoring data in construction site could have outlier created from diverse cause. In this study generation technique of synthesis value, its regression, final outlier detection and assessment are conducted to distinct outlier data included in extensive time series dataset. Synthesis value having weight factor of correlation between a number of datasets consist of many monitoring data enable to detect outlier by increasing its correlation. Standard artificial dataset in which intentional outliers are inserted has been used for assessment of synthesis value technique. These results showed increase of detection accuracy for outlier and general tendency in case of having different time series models in common. Accuracy of outlier detection increased in case of using more dataset and showing similar time series pattern.

Effects of Hardener and Extender Contents on Curing Behavior of Urea-Melamine-Formaldehyde Resin

  • Eom, Young-Geun;XU, Guang-Zhu;Lee, Young-Kyu;Kim, Hyun-Joong
    • Journal of the Korean Wood Science and Technology
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    • v.36 no.5
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    • pp.42-48
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    • 2008
  • This study was conducted to discuss the effects of hardener and extender contents on peak temperature, reaction enthalpy (${\Delta}H$), gelation time, viscosity change, and pH value in three types of UMF (urea-melamine- formaldehyde) resin with the help of perpHecT LogR meter, differential scanning calorimetry (DSC), and advanced rheometric expansion system (ARES), The results indicated that the pH value of Control A steeply decreased to 5,2 in the early stage but relatively remained constant thereafter as in Synthesis 1 and Synthesis 2, The peak temperature and time decreased as well, whereas ${\Delta}H$ and viscosity increased with the increase of hardener content. On the other hand, ${\Delta}H$ was not changed up to the extender content of 5% and then decreased with its further addition, And the pH value and peak temperature showed no change with the increase of extender content at the hardener content of 5% in three types of UMF resin, The effect of hardener content in this experiment, however, appeared more conspicuous in Control A than in the other two types of Synthesis 1 and Synthesis 2, These results might be caused by higher molecular weight with longer chains of methylene ($-CH_2-$) and methylene ($-CH_2-O-CH_2-$) ether bridges or much more branched chains in Control A.

Acoustic Analysis of Normal and Pathologic Voice Synthesized with Voice Synthesis Program of Dr. Speech Science (Dr. Speech Science의 음성합성프로그램을 이용하여 합성한 정상음성과 병적음성(Pathologic Voice)의 음향학적 분석)

  • 최홍식;김성수
    • Journal of the Korean Society of Laryngology, Phoniatrics and Logopedics
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    • v.12 no.2
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    • pp.115-120
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    • 2001
  • In this paper, we synthesized vowel /ae/ with voice synthesis program of Dr. Speech Science, and we also synthesized pathologic vowel /ae/ by some parameters such as high frequency gain (HFG), low frequency gain(LFG), pitch flutter(PF) which represents jitter value and flutter of amplitude(FA) which represents shimmer value, and grade ranked as mild, moderate and severe respectively. And then we analysed all pathologic voice by analysis program of Dr. Speech Science. We expect that this synthesized pathologic voices are useful for understanding the parameter such as noise, jitter and shimmer and feedback effect to patient with voice disorder.

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Robust Control of a Glass Fiber Composite Beam using $\mu$-Synthesis Algorithm

  • Lee, Seong-cheol;Kwon, Tae-Kyu;Yun, Yeo-Hung
    • International Journal of Precision Engineering and Manufacturing
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    • v.1 no.2
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    • pp.76-83
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    • 2000
  • A study on the robust control of a composite beam with a distributed PVDF sensor and piezo-ceramic actuator is presented in this paper. $1^{st}$ and $2^{nd}$ natural frequencies are considered in the modeling, because robust control theory which has robustness to structured uncertainty is adopted to suppress the vibration. If the controllers designed by $H_{\infty}$ theory do not satisfy control performance, it is improved by $\mu$-synthesis method with D-K iteration so that the $\mu$-controller based on the structured singular value satisfies the nominal performance and robust performance. Simulation and experiment were carried out with the designed controller and the verification of the robust control properties was presented by results.

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Synthesis of 4 bar linkage using genetic algorithm and overlay method (유전알고리즘과 겹쳐 그리기 법을 이용한 4절 링크 합성)

  • Yoon, Sung-Joon;Kim, Jun-Hwan
    • Proceeding of EDISON Challenge
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    • 2015.03a
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    • pp.476-478
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    • 2015
  • This paper deals with synthesis of 4 bar linkage by using optimum design. To design 4 bar linkage, overlay method is proposed and for optimization, genetic algorithm is applied with objective function. The accuracy of this method will be determined by errors between real value and test value. We will use Chebychev spacing to get 3 precision positions of input angles. The output angles will be determined by the function that the designer wants input and output relations to be. It will be applied to example to show the accuracy of this method. The advantages of using this method are that it is fast to get optimal solution and it is simple to use.

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Offset Slider-Rocker Linkage Synthesis Using Transmission Angles as Synthesis Parameters (전달각을 이용한 오프셋 슬라이더-로커 링크장치의 합성)

  • Gwon, Seong-Gyu
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.24 no.4 s.175
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    • pp.881-893
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    • 2000
  • An analytical synthesis technique for offset slider-rocker 4-bar linkages is devised where transmission angles are used as essential synthesis parameters. Finding the location where both the maximum and the minimum transmission angles arise leads to establishing the algorithm for limiting transmission angles of the slider-rocker linkage which has different offsets according to the direction of the slider. Position analysis by the algorithm gives formula for the dimensional synthesis for the linkage. Application to examples shows that the algorithm and the formula yield proper slider-rocker linkages with regard to limiting transmission angles to the maximum value.

Determination of Non-stoichiometry of Tubular Titanium Carbide Formed by Self-Propagating High Temperature Synthesis

  • Choi, Y.;Cho, N.I.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.782-783
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    • 2006
  • Titinium carbide $(TiC_x)$ was produced by self-propagating high temperature synthesis (SHS) method. The morphology and non-stoichiometric number of the SHS product were observed by scanning electron microscopy and neutron diffractometry, respectively. Tubular titanium carbide with hole inside was formed with different non-stoichiometric number (x), which value increased with combustion temperature.

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