• 제목/요약/키워드: Synthesis of advanced materials

검색결과 785건 처리시간 0.042초

Synthesis of Intermetallics and Nanocomposites by High-Energy Milling

  • Bernd F. Kieback;H. Kubsch;Alexander Bohm;M. Zumdick;Thomas Weissgaerber
    • 한국분말재료학회지
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    • 제9권6호
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    • pp.416-421
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    • 2002
  • Elemental powders are used in high energy milling processes for the synthesis of new compounds. The low temperature solid state reactions during milling in inert gas atmosphere may result in intermetallic phases, carbides, nitrides or silicides with a nanocrystalline structure. To obtain dense materials from the powders a pressure assisted densification is necessary. On the other side the defect-rich microstructure can be used for activated sintering of elemental powder mixtures to obtain dense bodies by pressureless sintering. Results are discussed for nanocrystalline cermet systems and for the sintering of aluminides and silicides.

Synthesis of SiNx:H films in PECVD using RF/UHF hybrid sources

  • Shin, K.S.;Sahu, B.B.;Lee, J.S.;Hori, M.;Han, Jeon G.
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2015년도 제49회 하계 정기학술대회 초록집
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    • pp.136.1-136.1
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    • 2015
  • In the present study, UHF (320 MHz) in combination with RF (13.56 MHz) plasmas was used for the synthesis of hydrogenated silicon nitride (SiNx:H) films by PECVD process at low temperature. RF/UHF hybrid plasmas were maintained at a fixed pressure of 410 mTorr in the N2/SiH4 and N2/SiH4/NH3 atmospheres. To investigate the radical generation and plasma formation and their control for the growth of the film, plasma diagnostic tools like vacuum ultraviolet absorption spectroscopy (VUVAS), optical emission spectroscopy (OES), and RF compensated Langmuir probe (LP) were utilized. Utilization of RF/UHF hybrid plasmas enables very high plasma densities ~ 1011 cm-3 with low electron temperature. Measurements using VUVAS reveal the UHF source is quite effective in the dissociation of the N2 gas to generate more active atomic N. It results in the enhancement of the Si-N bond concentration in the film. Consequently, the deposition rate has been significantly improved up to 2nm/s for the high rate synthesis of highly transparent (up to 90 %) SiNx:H film. The films properties such as optical transmittance and chemical composition are investigated using different analysis tools.

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펄스 전류 활성 연소합성과 소결에 의한 4.25 Co0.53Fe0.47-Al2O3 복합재료제조 (Fabrication of 4.25 Co0.53Fe0.47-Al2O3 Composite by High FrequencyInduction Heated Combustion Synthesis and Sintering)

  • 이동목;조광명;손인진
    • 대한금속재료학회지
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    • 제47권6호
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    • pp.344-348
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    • 2009
  • Dense $4.25Co_{0.53}Fe_{0.47}-Al_{2}O_{3}$ composite was simultaneously synthesized and consolidated by pulsed current activated combustion method within 2 min from mechanically activated powders. Consolidation was accomplished under the combined effects of a pulsed current and mechanical pressure. Dense $4.25Co_{0.53}Fe_{0.47}-Al_{2}O_{3}$ with relative density of up to 96% was produced under simultaneous application of 80 MPa pressure and the pulsed current. Fracture toughness and hardness of the composite are $6MPa{\cdot}m^{1/2}$ and $570kg/mm^{2}$ respectively.

Microwave-Assisted Synthesis of Flower-like and Plate-like CuO Nanopowder and Their Photocatalytic Activity for Polluted Lake Water

  • Xu, Ling;Xu, Hai-Yan;Wang, Feng;Zhang, Feng-Jun;Meng, Ze-Da;Zhao, Wei;Oh, Won-Chun
    • 한국세라믹학회지
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    • 제49권2호
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    • pp.151-154
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    • 2012
  • Flower-like and plate-like CuO nanopowder has been successfully synthesized using a facile microwave-assisted synthetic route. The morphology and size of the final products strongly depended on microwave power. The phase, structures and morphologies of the as-prepared products were investigated in detail by BET surface area analysis, X-ray diffraction (XRD) analysis, and scanning electron microscopy (SEM). In addition, the chemical oxygen demand of polluted lake water was employed for characterization of these new photocatalysts. The results showed correlations between the morphology of CuO micro-crystals and their catalytic properties.

PVA 용액법을 통한 나노 Cu 분말합성 및 소결체의 열적 특성 (Synthesis of Nano-Sized Cu Powder by PVA Solution Method and Thermal Characteristics of Sintered Cu Powder Compacts)

  • 오복현;마충일;이상진
    • 한국재료학회지
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    • 제30권2호
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    • pp.93-98
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    • 2020
  • Effective control of the heat generated from electronics and semiconductor devices requires a high thermal conductivity and a low thermal expansion coefficient appropriate for devices or modules. A method of reducing the thermal expansion coefficient of Cu has been suggested wherein a ceramic filler having a low thermal expansion coefficient is applied to Cu, which has high thermal conductivity. In this study, using pressureless sintering rather than costly pressure sintering, a polymer solution synthesis method was used to make nano-sized Cu powder for application to Cu matrix with an AlN filler. Due to the low sinterability, the sintered Cu prepared from commercial Cu powder included large pores inside the sintered bodies. A sintered Cu body with Zn, as a liquid phase sintering agent, was prepared by the polymer solution synthesis method for exclusion of pores, which affect thermal conductivity and thermal expansion. The pressureless sintered Cu bodies including Zn showed higher thermal conductivity (180 W/m·K) and lower thermal expansion coefficient (15.8×10-6/℃) than did the monolithic synthesized Cu sintered body.