• 제목/요약/키워드: Surface hardness change

검색결과 263건 처리시간 0.024초

Effect of Liquefied Digestive Medicine on the Surface of Composite Resin

  • Kim, Min-Young;Lim, Hee-Jung;Kim, Ha-Eun;Kim, Hyun-Jeong;Yu, Hye-Kang;Choi, Soo-Jin;Lim, Do-Seon
    • 치위생과학회지
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    • 제22권1호
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    • pp.20-29
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    • 2022
  • Background: The purpose of this study is to investigate the effect of liquefied digestive medicines on the composite resin surface. Methods: Three types of liquefied digestive medicines (Gashwalmyeongsu, Wicheongsu, and Saengrokcheon) were selected as experimental groups, Samdasoo and Chamisul as negative controls, and Trevi as positive controls were selected to measure pH and titratable acidity. The samples filled with resin at acrylic were made total 300, 50 per group. To evaluate the erosion risk of the composite resin, the specimens were immersed in a liquefied medicine for 1, 3, 5, 15, and 30 minutes, and then the surface microhardness was measured using the Vickers Hardness Number, and the surface change was observed with scanning electron microscope (SEM). Results: The average pH of the three liquefied medicine was 3.75±0.30, the Saengrokcheon was the lowest at 3.45±0.01, and the Trevi was 4.66 and Samdasoo and Chamisul were 7.40 and 8.58, respectively. The amount of NaOH reaching pH 5.5 and 7.0 was the lowest in the order of Trevi, Gashwalmyeongsu, Wicheongsu, and Saengrokcheon. The largest surface hardness reduction value was shown in Gashwalmyeongsu (-11.85±3.73), followed by Saengrokcheon (-9.79±3.11) and Wicheongsu (-8.28±2.83), and Samdasoo (-0.84±1.56) and Chamisul (-6.24±0.42) had relatively low surface hardness reduction values. However, Trevi (-16.67±5.41), a positive control group containing carbonic acid, showed a higher decrease in surface hardness than the experimental group. As a result of observation with SEM, experimental group and positive control group, showed rough surfaces and irregular cracks, and negative control groups showed smooth patterns similar to before immersion. Conclusion: The liquefied digestive medicine with low pH could weaken the composite resin surface, and the carbonic acid component could more effect on the physical properties of the composite resin than pH.

Cu계 비정질 입자의 가압 성형 (Consolidation of Cu-based amorphous particles)

  • 강은영;정영훈;유호근;박종우
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2005년도 추계학술대회 논문집
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    • pp.273-276
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    • 2005
  • Packing characteristics of amorphous alloy particles were investigated by scanning electron microscopy, compositional analysis, micro-hardness test and finite element method (FEM). Electroless Ni-plating was made on the surface of the Cu-based amorphous particles before consolidation in ambient atmosphere at an intermediate region of glass transition and crystallization temperatures $(T_g\;and\;T_x)$. Some parts of the Ni-layer in the interfaces of the consolidated particles disappeared, while some of them still remained without appreciable change in compositions. No cracks or fractures were found in the particles, which may occur at low temperatures below or near $T_g$ as anticipated by the FEM analysis. Crystallization and change in hardness were not observed after consolidation.

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가황조건에 따른 Wiper Blade 고무의 특성변화 (Physical Properties of the Windshied wiper Blade Rubber According to Vulcanization System)

  • 윤창한;권영배
    • 한국기계연구소 소보
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    • 통권13호
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    • pp.27-43
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    • 1984
  • In order to obtain the high resilience, low compression set and less of hardness change in the wiper blade rubber, vulcanization system and receipes must be controlled. To improve the above the above Physical properties, the system should be taken as follows. i) peroxide vulcanization system and sulfur vulcanization system. ii) rubber having more cis-form than trans-form. iii) moderate particle size cabon black. v) usage of other improvement agent. The rubber blade with 4.4% compression set, 76% resilience, Hs 0 $\pm$ 2 hardness change could be abtained through vulcanization system, In addition, the surface of wiper blade must be treated by chemically and physically to minimize for the skid and friction.

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고온 열화된 Inconel 600강의 미세조직 및 기계적 특성 평가 (Evaluation of Microstructure and Mechanical Property of Inconel 600 Degraded under High Temperature)

  • 정광후;김성종
    • 한국표면공학회지
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    • 제50권6호
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    • pp.492-497
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    • 2017
  • In this study, we investigated the effect of thermal aging on mechanical characteristics of Inconel 600 nickel-based alloy. The thermal aging was conducted up to 1000 hours at an atmosphere of $650^{\circ}C$. The microstructure of thermally aged specimens was investigated by an optical microscope (OM), scanning electron microscope (SEM) and energy dispersive spectrometer (EDS). In addition, tensile test (strain rate: 2 mm/min) and micro Vickers hardness test were conducted to evaluate mechanical properties with time. As a result of the experiment, Cr-rich carbide continuously precipitated during thermal aging, leading to the change of the mechanical characteristics and fracture mode. With the increase of aging time, tensile strength, yield strength, and hardness gradually decreased. The fracture mode changed from ductile to brittle with the increase of grain boundary carbide.

CGS를 잔골재로 활용하는 FA치환 콘크리트의 응결시간 추정시 개량형 듀로미터 사용 가능성 분석 (Utilization of Improved Durometer when Estimating Setting Time of FA Replacement Concrete Using CGS for Fine Aggregate)

  • 이혁주;신용섭;서항구;한인덕;한민철;한천구
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2019년도 추계 학술논문 발표대회
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    • pp.81-82
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    • 2019
  • In this study, the Proctor penetration resistance test value and the hardness value of the improved Durometer were compared and analyzed for the change in the FA replacement rate of the concrete using CGS fine aggregate. The results are summarized as follows. It is. 1) The Proctor penetration resistance test value and the hardness value of the improved Durometer showed a high correlation in the form of a curve. 2) About surface finish Super-resolution with the improved Durometer is considered to be useful when using about 50 HD and about 80 HD in the end to determine the surface finishing work time.

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일원분석을 통한 하이브리드 추정계의 측정횟수별 영향검증 (One-way ANOVA Analysis to Verify the Effect of Hybrid Strength Estimators by Number of Measurements)

  • 한수환;후윈야오;김수호;임군수;김종;한민철
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2022년도 봄 학술논문 발표대회
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    • pp.37-38
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    • 2022
  • This study is attempted to propose an appropriate number of measurements by checking and statistically analyzing the change in hardness according to the number of measurements. As a result, there was no significant difference between the 20th and 30th data, and in the 10th case, the effect on errors occurring during measurement was found to be dominant. Therefore, as the number of measurements, proposing 20 times in consideration of the convenience of use. In addition, in order to minimize the effect on the measurement error, it is proposed to remeasure the surface mane of the measurement surface and the test value in which the error occurs on the average of the test values.

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고체입자 충돌침식으로 인한 배관 재질의 손상에 관한 연구 (A Study of Damage on the Pipe Flow Materials Caused by Solid Particle Erosion)

  • 김경훈;최덕현;김형준
    • Corrosion Science and Technology
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    • 제13권4호
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    • pp.130-138
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    • 2014
  • Wall thinning can be classified into three types: flow-accelerated corrosion, cavitation erosion and solid particle erosion. This article presents a study of solid particle erosion, which frequently causes damages to power plants' pipe system. Unlike previous studies, this study uses a mechanism to make solid particles in a fluid flow collide with pipe materials in underwater condition. Experiment is conducted in three cases of velocity according to solid-water ratio using the three types of the materials of A106B, SS400, and A6061. The experiments were performed for 30 days, and the surface morphology and hardness of the materials were examined for every 7 days. Based on the velocity change of the solid particles in a fluid flow, the surface changes, the change in the amount of erosion, the erosion rate and the variation in the hardness of carbon steel and aluminum family pipe materials can all be determined. In addition, factor-based erosion rates are verified and a wall-thinning relation function is suggested for the pipe materials.

Ti-Al-Si-Cu-N 후막의 Cu 조성에 따른 기계적 특성과 미세구조 변화에 관한 연구 (Influence of Cu Composition on the Mechanical Properties and Microstructure of Ti-Al-Si-Cu-N thick films)

  • 이연학;허성보;박인욱;김대일
    • 한국표면공학회지
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    • 제56권5호
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    • pp.335-340
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    • 2023
  • Quinary component of 3㎛ thick Ti-Al-Si-Cu-N films were deposited onto WC-Co and Si wafer substrates by using an arc ion plating(AIP) system. In this study, the influence of copper(Cu) contents on the mechanical properties and microstructure of the films were investigated. The hardness of the films with 3.1 at.% Cu addition exhibited the hardness value of above 42 GPa due to the microstructural change as well as the solid-solution hardening. The instrumental analyses revealed that the deposited film with Cu content of 3.1 at.% was a nano-composites with nano-sized crystallites (5-7 nm in dia.) and a thin layer of amorphous Si3N4 phase.

초음파현미경을 이용한 Co 기 초내열 합금 열화재의 비파괴평가 (Nondestructive Evaluation for Thermally Degraded Co-base Superalloy by Scanning Acoustic Microscope)

  • 김정석;송진헌;권숙인;임재생;박익근
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2004년도 춘계학술대회
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    • pp.336-341
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    • 2004
  • This research investigates the feasibility of ultrasonic microscope for nondestructive assessment of thermal degradation in artificially aged commercial Co-base superalloy, FSX414. This alloy has been used for high temperature structure applications such as stationary gas turbine blade and nozzle chamber in fossil plant. Microstructural change was found that the fine carbides became coarser and spheroidized in matrix as aging time increased. The leaky surface acoustic wave velocity gradually decreases by a maximum of 4.7% with increasing aging time up to 4,000hours. However, the longitudinal wave velocity has a little change. Also, it has a good correlation between leaky surface acoustic wave velocity and Vickers hardness. Consequently, LSAW can be used to examine the degree of degradation in thermally aged Co-base superalloy.

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진공침탄을 위한 처리조건 설정에 관한 연구 (A Study on Setting up Condition of Treatment for Vacuum Carburizing)

  • 이상길;강순배;정병호;김한군
    • 열처리공학회지
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    • 제5권4호
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    • pp.195-200
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    • 1992
  • SCM 415 has been vacuum carburized in the carburizing pressure of 60-65kpa and the carburizing temperature of 1233k and 1273k after varied to 0-20 in the ratio of $N_2/C_3H_8$ and then diffusion treated for various times at 1123k. The results obtained from the experiment are as follows. 1. With increasing from 0 to 20 in ratio of $N_2/C_3H_8$ the sooting formation of surface after carburizing considerably decreased. 2. The hardness control and surface carbon content of carburizing surface has been modified by the addition of nitrogen to the propan. 3. The appoximate value of k is indirectry calculated at 1123k which results are obtained to $0.58{\times}10^{-2}(wt.%.S^{-1/2})$. 4. A great deal of propan by addition of nitrogen gas in carburizing gas was possible to saving without considerable change in case hardening depth. 5. The effective carburizing depth range is obtained to 0.8-1.1mm by diffusion temperature of 1123k after carburization at 1273k-3.6ks, and the surface hardness is increased as the increasing of $T_D/T_c$ in our experimental condition, and the maximum hardness as reachin distance from surface is decreased.

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