• Title/Summary/Keyword: Surface Treatments

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The effect of low temperature aging on the mechanical property & phase stability of Y-TZP ceramics

  • Kim, Hyung-Tae;Han, Jung-Suk;Yang, Jae-Ho;Lee, Jai-Bong;Kim, Sung-Hun
    • The Journal of Advanced Prosthodontics
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    • v.1 no.3
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    • pp.113-117
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    • 2009
  • STATEMENT OF PROBLEM. Recently Yttrium-stabilized tetragonal zirconia polycrystal (Y-TZP) has been introduced due to superior flexural strength and fracture toughness compared to other dental ceramic systems. Although zirconia has outstanding mechanical properties, the phenomenon of decrease in the life-time of zirconia resulted from degradation in flexural strength after low temperature aging has been reported. PURPOSE. The objective of this study was to investigate degradation of flexural strength of Y-TZP ceramics after various low temperature aging treatments and to evaluate the phase stability and micro-structural change after aging by using X-ray diffraction analysis and a scanning electron microscope (SEM). MATERIAL AND METHODS. Y-TZP blocks of Vita In-Ceram YZ (Vita Zahnfabrik, Bad $S\ddot{a}ckingen$, Germany) were prepared in 40 mm (length) $\times$ 4 mm (width) $\times$ 3 mm (height) samples. Specimens were artificially aged in distilled water by heat-treatment at a temperature of 75, 100, 125, 150, 175, 200, and $225^{\circ}C$ for 10 hours, in order to induce the phase transformation at the surface. To measure the mechanical property, the specimens were subjected to a four-point bending test using a universal testing machine (Instron model 3365; Instron, Canton, Mass, USA). In addition, X-ray diffraction analysis (DMAX 2500; Rigaku, Tokyo, Japan) and SEM (Hitachi s4700; Jeol Ltd, Tokyo, Japan) were performed to estimate the phase transformation. The statistical analysis was done using SAS 9.1.3 (SAS institute, USA). The flexural strength data of the experimental groups were analyzed by one-way analysis of variance and to detect statistically significant differences ($\alpha$= .05). RESULTS. The mean flexural strength of sintered Vita In-Ceram YZ without autoclaving was 798 MPa. When applied aging temperature at below $125^{\circ}C$ for 10 hours, the flexural strength of Vita In-Ceram YZ increased up to 1,161 MPa. However, at above $150^{\circ}C$, the flexural strength started to decrease. Although low temperature aging caused the tetragonal-to-monoclinic phase transformation related to temperature, the minimum flexural strength was above 700 MPa. CONCLUSION. The monoclinic phase started to appear after aging treatment above $100^{\circ}C$. With the higher aging temperature, the fraction of monoclinic phase increased. The ratio of monoclinic/tetragonal + monoclinic phase reached a plateau value, circa 75% above $175^{\circ}C$. The point of monoclinic concentration at which the flexural strength begins to decrease was between 12% and 54%.

Interfacial Pullout Characteristics of Recycled PET Fiber With Hydrophilic Chemical Treatments in Cement Based Composites (화학적 친수성 처리율에 따른 재생 PET 섬유와 시멘트 복합재료와의 계면 인발 특성)

  • Won, Jong-Pil;Park, Chan-Gi;Kim, Yoon-Jeong;Park, Kyung-Hoon
    • Journal of the Korea Concrete Institute
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    • v.19 no.3
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    • pp.333-339
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    • 2007
  • The purpose of this study was to enhance bond performance between recycled PET (polyethylene telephthalat) fiber and cement composites through hydrophilic treatment using maleic anhydride grafted polypropylene(mPP). The mPP with various concentration of 0%, 5%, 10%, 15% and 20% to determine effect on bond behavior of recycled PET fiber were applied as experimental variables. Dog bone shaped specimens according to JCI SF-8 was applied to evaluate the bond strength and pullout energy. The results showed increased bond strength and pullout energy as concentration of mPP. Concentration of 15% mPP showed the most effective results while 20% showed reduced performance results. Because 15% mPP ensures perfect coating while 20% makes thick coating area that resulted in crack propagation and consequent separation of PET fiber and coated area during pullout load occurred. Enhancement mechanism of bond performance of recycled PET fiber and cement composites with each concentration of mPP could be conformed through investigation of microstructure of fiber surface.

ORTHODONTIC TRACTION OF IMPACTED MANDIBULAR SECOND PRIMARY MOLAR (매복된 하악 제2유구치의 교정적 견인)

  • Kim, Min-Jung;Lee, Sang-Ho;Lee, Nan-Young;Jang, Hyang-Gil
    • Journal of the korean academy of Pediatric Dentistry
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    • v.38 no.3
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    • pp.303-308
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    • 2011
  • Tooth impaction refers to situations in which the eruption is inhibited by some physical barriers in eruptive path and the tooth remains unerupted beyond the normal time of eruption. The etiology of impacted tooth is controversial, but ankylosis has been suggested probably as a leading role. Impacted primary molars may cause several problems such as space loss, tipping of adjacent teeth, supra-eruption of the antagonists, dislocation of succeeding premolar, cystic change and infection. As one of conventional treatments of impacted primary molars, early tooth extraction or surgical extraction following space regaining when there is space loss has been suggested. However, when they are in normal formation and not ankylosed, orthodontic traction following surgical exposure can be the choice of treatment. In this case, a 3-year-old boy was referred to the department of pediatric dentistry for the unerupted mandibular right second primary molar. After surgical removal of gingiva on the occlusal surface, orthodontic traction was performed. After treatment, we could get normal alignment of primary teeth and the opportunity for normal development of permanent teeth.

Effect of Red LEDs during Healing and Acclimatization Process on the Survival Rate and Quality of Grafted Tomato Seedlings (토마토 접목묘의 순화과정에서 적색LED광조사가 접목 활착율과 묘소질에 미치는 영향)

  • Vu, Ngoc-Thang;Kim, Young-Shik;Kang, Ho-Min;Kim, Il-Seop
    • Journal of Bio-Environment Control
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    • v.23 no.1
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    • pp.43-49
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    • 2014
  • This study was designed to determine the effect of red LEDs during healing and acclimatization process on the survival rate and quality of grafted tomato seedlings. Red LEDs and no light (darkness) were used for treating three rootstock cultivars, which are 'B-Blocking', 'Kanbarune', 'High-power' in healing room. Results showed that survival rates of grafted seedlings in red LEDs were higher than those in no light treatment. Significant variation on survival rates of rootstock cultivars was observed in no light treatment but there was not significant variation in red LEDs treatment. Light treatment also reduced the percentage of infected plants, except for the 'Kanbarune' cultivar. Seedling quality in red LEDs was better than that in no light treatment by improving growth parameters such as plant height, leaf length, leaf width, leaf area, fresh and dry weight of shoot and root. Light treatments and rootstock cultivars did not affect number of leaves, leaf chlorophyll value and T/R ratio of seedlings, but seedlings in red LEDs were significantly more compact than those in no light treatment. Moreover, the root morphology of seedlings such as total root surface area, total root length, and number of toot tips in red LEDs was also greater than that in no light treatment.

Studies on Management of Effective Temperature and Humidity in Greenhouse at Summer Season (하절기 효율적인 하우스 온도 습도 관리에 관한 연구)

  • 우영회;남윤일;송천호;김형준;김동억
    • Journal of Bio-Environment Control
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    • v.3 no.1
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    • pp.58-65
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    • 1994
  • It is necessary to effective temperature and humidity management for normal growth of crops in protected cultivation during the summer season. Because the highest temperature of vinyl house inhibit normal growth of crop and decrease of crop production or marketability in summer season. Finally, the vinyl house was impossible some crop cultivation in summer season. This study was conducted to investigate effective and economic method for temperature drop in protected cultivation during the summer season. 1. In medium size vinyl house(5$\times$13$\times$3m), the effect of temperature drop appeared the highest in treatment of shading with aluminium thermal curtain+fog system+ventilation with fan. The effect of temperature drop was about 1$0^{\circ}C$ lower than outer air temperature and about 4$^{\circ}C$ lower than outer soil temperature. 2. The effect of temperature drop according to shading with aluminium thermal curtain+fog system+ventilation with fan during the highest temperature of summer season Jul., 20 to Aug., 21 was appeared about 8$^{\circ}C$ lower than outdoor above ground(1.2m) and about 7$^{\circ}C$ lower than outdoor surface ground. 3. The changes of solar radiation during a day according to shading with aluminium thermal curtain+ventilation with fan and shading with black curtain+ventilation with fan treatments was appeared respectively about 29.3%, 32.5% of outdoor solar radiation a fine day and respectively about 27.4%, 31.8% of outdoor solar radiation a cloudy day.

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Growth, Deficiency Symptom and Tissue Nutrient Contents of Leaf Perilla (Perilla frutesens) as Influenced by Nitrogen Concentrations in the Fertigation Solution (질소 시비농도가 잎들깨의 생육, 생리장해 발현 및 무기원소 함량에 미치는 영향)

  • Choi, Jong-Myung;Park, Jong-Yoon
    • Journal of Bio-Environment Control
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    • v.16 no.4
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    • pp.365-371
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    • 2007
  • Objective of this research was to investigate the effect of nitrogen concentrations in the fertilizer solution on growth and development of nutrient deficiency in leaf perilla (Perilla frutesens). The nutrient concentrations in above-ground plant tissue, petiole sap and soil solution of root media were also determined. Nitrogen deficiency resulted in dwarfed growth, small leaves, and bright yellow color of older leaves. The leaves of deficient plants became uniform yellowing in color and finally necrosis occurred on the deficient leaves. Elevation of N concentrations in the fertigation solution from 0 to 20 mM increased the crop growth in leaf length and width as well as fresh and dry weights of above ground plant tissue. That also resulted in the increase of chlorophyll contents. However, light toxicity symptoms such as abnormal leaf surface appeared on crops grown in 20 mM N fertilization. The plant growth was commercially acceptable in the treatments of 10 and 15 mM N. The plants with acceptable growth had 0.9 to 1.25% in N contents of above-ground plant tissue, 800 to $3,300mg{\cdot}kg^{-1}$ in the $NO_3-N$ concentrations of petiole sap, and 28.7 to $47.3mg{\cdot}kg^{-1}$ in the $NO_3-N$ concentrations of soil solution (1:2 extract) at 75 days after transplanting.

Effect of Undersoil Heating on Growth and Mineral Contents of Turfgrasses in Simulated Athletic Field During Winter Season (겨울철 지하부의 가온처리가 경기장 잔디의 생육 및 무기성분 함량에 미치는 영향)

  • 구자형;이혜정
    • Asian Journal of Turfgrass Science
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    • v.16 no.2
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    • pp.65-73
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    • 2002
  • Studies were conducted to determine the effect of undersoil heating on growth and quality of turfgrasses including Kentucky bluegrass (Poa pratensis L.‘Nuglade’), perennial ryegrass (Lolium perenne L.‘Accent’), tall fescue (Festuca arundinacea Schreb.‘Pixie’), and Korean lawngrass (Zoysia japonica Steud.) in simulated athletic field during winter season in Korea. Mineral contents in clippings of turfgrasses grown at different soil mixtures and temperatures were also analyzed. Undersoil heating (approximately 20$\pm$2$^{\circ}C$) was effective in protecting turfgrasses except Korean lawngrass from freezing injury and discoloration of shoots due to extremely cold temperatures during midwinter. Among turfgrasses grown at undersoil heating zone, tall fescue and perennial ryegrass showed the highest clipping weights and chlorophyll contents, respectively. However, anthocyanin contents of shoots were higher in Kentucky bluegrass. There was little or no difference in clipping weights, chlorophyll contents, anthocyanin contents and greenness of shoots between turfgrasses grown at two soil mixtures composed of 80% sand+10% peat moss+10% soil (v/v/v) and 80% sand+20% pea moss (v/v). Contents of mineral K, Ca and Mg in clippings of cool-season turfgrasses were comparatively higher in a soil mixture composed of 80% sand+10% peat moss+10% soil, but little difference in contents of N and P was observed between two soil treatments. Results indicated that undersoil heating can improve quality of turf surface by thawing soil, melting snow, and maintaining shoot growth and greenness of turfgrasses in sports field during winter season.

Growth response of Calla (Zantedeschia) to root zone environmental conditions in Highland (고랭지에서의 근권환경에 따른 유색칼라(Zantedeschia)의 생육반응)

  • Nam, Chun-Woo;Yoo, Dong-Lim;Kim, Su-Jeong;Suh, Jong-Teak;Paek, Kee-Yoeup;Lee, Sang Gyu;Yoon, Moo Kyung
    • Korean Journal of Agricultural Science
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    • v.40 no.4
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    • pp.325-331
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    • 2013
  • This experiment has been carried out to determine optimal culture conditions for the production of cut flowers and tubers of Calla (Zantedeschia 'Golden Affair' and 'Black Magic') in highlands. Treatments consisted of various levels of root zone environments, Results are as follows: Calla 'Golden Affair' were grown with different mulching materials such as Non-mulching, Black film, reflective film, Rice hull. Mulching materials resulted in no difference in the number of cut flowers but flower length was highest in reflective film. Calla 'Black Magic' were treated with various soil water content, soil type and watering time. Number of cut flowers and flower quality were greatest when the plants were watered at -80 kPa soil water content. No symptoms of soft rot (Erwinia carotovora) was observed at this soil water content. The occurrence of soft rot was observed with similar percentage according to soil type and the soil water content. When Calla 'Black Magic' were watered at the time of soil surface drying, growth was greater compared to others. Air temperature and PPF affected plant growth and photosynthesis. Photosynthetic rate was greatest at $25^{\circ}C$ and PPF $200{\mu}mol{\cdot}m^{-2}{\cdot}s^{-1}$, while lowest at $28^{\circ}C$ and PPF $800{\mu}mol{\cdot}m^{-2}{\cdot}s^{-1}$. Soft rot did not occur without regard to dipping treatment (0, 5, 10, 24, 48 hours) when the day and night temperature were maintained at $25^{\circ}C$ and $20^{\circ}C$, respectively.

Analysis of Deformation and Stability of Slope at the Wiri Region of Local Road 999 Nearby Andong, Gyeongsangbukdo in Korea. (999번 지방도로 경상북도 안동시 위리 지역의 사면 변형 및 안정성 분석)

  • 장현식;장보안
    • The Journal of Engineering Geology
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    • v.10 no.1
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    • pp.1-12
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    • 2000
  • Heaving of road and subsidence of slope took place at the Wiri region of the local highway 999 in Gyeongsangbukdo, Korea after heavy rain in the next year of construction. Although the state government had performed remedial treatments by reducing the angle and the height of the slope, deformation had never stopped. Therefore, we have preformed the analysis of deformation and stabilityof the slope. Study area consists of the Cretaceous shale, siltstone and sandstone and two faults are found. The major deformation occurred by sliding of rock mass along faults after heavy rain because not only thepore pressure at the fault plane and the unit weight of sliding mass increased, but did the shearstrength of saturated fault clay become very low. The decrease in shear strength of saturated fault clayis the major factor among the reasons for deformation. Numerical simulations using limit equilibriummodel, finite difference model and finite element model were performed for eight cross sections.Although safety factors are above 1.7 during the dry season, they become below 1.0 when groundwaterlevel raises to surface. The maximum displacement is about 15-3Ocm. However, safety factors increasedto above 2.4 and the maximum displacement is below 2.08cm after remedial treatment, Indicating thatthe slope becomes stable.

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Effects of Red-Koji Fermented Scutellariae Radix Extracts on Lipopolysaccharide-induced Rat Acute Lung Injury (홍국발효 황금이 Lipopolysaccharide 유발 급성 폐손상에 미치는 영향)

  • Kim, Koang Lok;Kwon, Kyoung Man;Yun, Yong Jae;Lee, Young Jun;Park, Dong Il;Kim, Jong Dae;Jung, Tae Young
    • Journal of Physiology & Pathology in Korean Medicine
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    • v.26 no.6
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    • pp.874-885
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    • 2012
  • In the present study, the possibility of whether the pharmacological effects of Scutellariae Radix Aqueous Extracts(SR) were favorably changed by report that lipopolysaccharide(LPS)-induced rat acute lung injury was treated with Red-Koji(Monascus purpureus 12002) fermentation. Three different dosages of Red-Koji fermented SR extract(fSR), 125, 250 and 500 mg/kg were orally administered once a day for 28 days before LPS(Escherichia coli 0111:B4) treatments, and then 5 hours after LPS treatment(500 ${\mu}g$/head, intra trachea instillation), all rats were sacrificed. Changes in the body weights, lung weights, pulmonary transcapillary albumin transit, arterial gas parameters(pH, $PaO_2$ and $PaCO_2$) bronchoalveolar lavage fluid(BALF) protein, lactate dehydrogenase(LDH) and proinflammatory cytokine tumor necrosis factor-${\alpha}$(TNF-${\alpha}$), interleukin-$1{\beta}$(IL-$1{\beta}$) contents, total cell numbers, neutrophil and alveolar macrophage ratios, lung malondialdehyde(MDA), myeloperoxidase(MPO), proinflammatory cytokine TNF-${\alpha}$ and IL-$1{\beta}$ contents were observed with histopathology of the lung, changes on luminal surface of alveolus(LSA), thickness of alveolar septum, number of polymorphonuclear neutrophils(PMNs). As results of LPS-injection, dramatical increases in lung weights, pulmonary transcapillary albumin transit increases in $PaCO_2$, decreases in pH of arterial blood and $PaO_2$, increases of BALF protein, LDH, TNF-${\alpha}$ and IL-$1{\beta}$ contents, total cells, neutrophil and alveolar macrophage ratios, lung MDA, MPO, TNF-${\alpha}$ and IL-$1{\beta}$ contents increases were detected with decreases in LSA and increases of alveolar septum and PMNs numbers, respectively as compared with intact control. Especially fSR 125 mg/kg showed quite similar favorable effects on the LPS-induced acute lung injuries as compared with 60 mg/kg of ${\alpha}$-lipoic acid and 250 mg/kg of SR. The results suggest that over 125 mg/kg of fSR extracts showed favorable effects on the LPS-induced acute lung injury mediated by their antioxidant and anti-inflammatory effects. Moreover, increases of the pharmacological effects of SR on LPS-induced acute lung injury were observed by Red-Koji fermentation in this study, at least 2-fold higher.