• 한국공작기계학회논문집
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• 제17권2호
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• pp.65-70
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• 2008

This study deals with the friction welding of SKH55 and SM45C; The friction time was variable conditions under the conditions of spindle revolution 2,000rpm, friction pressure of 190MPa, upset pressure of 270MPa and upset time of 2.0 seconds. Under these conditions, the microstructure of weld interface, tensile fracture surface and mechanical tests were studied, and so the results were as follows. 1. When the friction time is 1.0 seconds, the tensile strength of friction welds was 926MPa, which is around as much as 84% of the tensile strength of base metal(SKH55), the bending strength of friction welds was 1,542MPa, which is around as much as 80% of the bending strength of base metal(SKH55), the shear strength of friction welds was 519MPa, which is around as much as 70% of the shear strength of base metal(SKH55). 2 According to the hardness test, the hardness distribution of the weld interface was formed from 964Hv to 254Hv. HAZ(Heat Affected Zone) was formed from the weld interface to 1.5mm of SKH55 and 2mm of SM45C.

• 대한화장품학회지
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• 제30권3호
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• pp.385-388
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• 2004

최근에 천연성분의 화장품 응용에 대한 관심이 높아지고 식물에 함유하고 있는 피토에스트로겐(Phytoestrogen)의 항노화 물질 연구가 중요해지고 있다. 태국 식물 Pueraria mirifica 추출물을 $4\%$ 함유한 크림제제(PM 크림)를 추출물 성분이 제외된 플라시보 크림과 비교하여 총 30명 여성을 대상으로 16주간 임상시험을 수행하였다. 피부 모사판을 제작하여 주름 측정을 하였고, 피부 탄력과 보습을 기기 평가하였다. 특히 피부 탄력도는 placebo 크림 사용군 대비 추출물 함유 크림 사용군이 통계적으로 유의하게 탄력도가 증가하였다. 주름이나 보습평가는 특이할 만한 결과를 나타내지는 못했다. Pueraria mirifiaca는 피부 탄력 개선을 주는 항노화 화장품 개발에 응용될 수 있을 것이라 기대된다.

• Corrosion Science and Technology
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• 제6권5호
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• pp.219-226
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• 2007

Pre-construction primer (PCP), or shopprimer, have been applied to steel plates to control temporary corrosion during ship fabrication. For surface preparation at ship block stage, in common shipyard practices, welding beads, burnt and rusted areas shall be blasted or power tool cleaned and the contamination such as zinc salt shall be removed with blasting or power tool. Whereas, the sound film of PCP needs not to be removed or roughened as the paint having good compatibility with PCP is used for the first coat. In many cases, however, full blasting or sweep blasting on the sound PCP treated block assemblies was requested. There still has been argument about the legitimacy of this practice, thus, it is critical to evaluate the quality of the coating system applied on the sound PCP retained condition, comparing with the one applied on the full blasted or sweep blasted condition. In this study, two different epoxy systems for water ballast tank were applied on the surfaces with sound PCP condition, full blasted condition, and sweep blasted condition. Coating performances such as durability, anti-corrosion, cathodic disbondment resistance were evaluated. The test results clearly indicated that the sound film of PCP needed not to be removed or roughened as the paint having good compatibility with PCP based on inorganic zinc silicate.

• 한국재료학회지
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• 제26권3호
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• pp.149-153
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• 2016

Nanosized zeolites were prepared in an autoclave using tetraethoxysilane (TEOS), tetrapropylammonium hydroxide (TPAOH), and $H_2O$, at various hydrothermal synthesis temperatures. Using transmission electron microscopy and particle size analysis, the nanopowder particulate sizes were revealed to be 10-300 nm. X-ray diffraction analysis confirmed that the synthesized nanopowder was silicalite-1 zeolite. Using atomic layer deposition, the fabricated zeolite nanopowder particles were coated with nanoscale $TiO_2$ films. The $TiO_2$ films were prepared at $300^{\circ}C$ by using $Ti[N(CH_3)_2]_4$ and $H_2O$ as precursor and reactant gas, respectively. In the TEM analysis, the growth rate was ${\sim}0.7{\AA}/cycle$. Zeta potential and sedimentation test results indicated that, owing to the electrostatic repulsion between $TiO_2$-coated layers on the surface of the zeolite nanoparticles, the dispersibility of the coated nanoparticles was higher than that of the uncoated nanoparticles. In addition, the effect of the coated nanoparticles on the photodecomposition was studied for the irradiation time of 240 min; the concentration of methylene blue was found to decrease to 48%.

• 한국수소및신에너지학회논문집
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• 제25권4호
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• pp.378-385
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• 2014

In this research, we investigate electrical performance and electrochemical properties of graphene supported Pt (Pt/G) and PtM (M = Ni and Y) alloy catalysts (PtM/Gs) that are synthesized by modified polyol method. With the PtM/Gs that are adopted for oxygen reduction reaction (ORR) as cathode of proton exchange membrane fuel cells (PEMFCs), their catalytic activity and ORR performance and electrical performance are estimated and compared with one another. Their particle size, particle distribution and electrochemically active surface (EAS) area are measured by TEM and cyclic voltammetry (CV), respectively. On the other hand, regarding ORR activity and electrical performance of the catalysts, (i) linear sweeping voltammetry by rotating disk electrode and rotating ring-disk electrode and (ii) PEMFC single cell tests are used. The TEM and CV measurements demonstrate particle size and EAS of PtM/Gs are compatible with those of Pt/G. In case of PtNi/G, its half-wave potential, kinetic current density, transferred electron number per oxygen molecule and $H_2O_2$ production % are excellent. Based on data obtained by half-cell test, when PEMFC singlecell tests are carried out, current density measured at 0.6V and maximum power density of the PEMFC single cell employing PtNi/G are better than those employing Pt/G. Conclusively, PtNi/Gs synthesized by modified polyol shows better ORR catalytic activity and PEMFC performance than other catalysts.

• 콘크리트학회논문집
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• 제13권4호
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• pp.406-413
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• 2001

본 연구는 기존 원심력 철근콘크리트관의 성능을 향상시킬 수 있는 방법으로 관체 표면을 일정한 두께로 방식 라이닝 모르타르로 처리함으로써 보다 더 내구적인 하수관을 개발하기 위하여 실시하였다. 이를 위해 원심력 철근콘크리트관 제작 시, 동시성형이 가능하고 촉진 증기양생 조건에서도 균열이 발생되지 않는 접착강도가 큰 폴리머 시멘트 모르타르를 제조하였다. 폴리머 시멘트 모르타르를 원심력 철근콘크리트관용 라이닝 재료로 사용하기 위한 기초적 실험결과, 보통 시멘트 모르타르에 비해 역학적 성질 및 내구성이 우수하였으며, 현장적용결과, 동시성형 및 양생조건에 따라 적용될 수 있는 방법은 다양하나, 폴리머의 종류에 관계없이 폴리머 시멘트비를 20% 이하로 하며, 양생온도는 8$0^{\circ}C$이하의 양생조건을 제안할 수 있었다. 또한 현장조건이 가능하면, 2일간 기중양생(2$0^{\circ}C$)을 실시하여 폴리머 시멘트 모르타르 속의 폴리머 필름이 형성된 후, 8$0^{\circ}C$에서 양생시키는 방법이 이상적인 것으로 나타났다.

• 한국항공우주학회지
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• 제40권12호
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• pp.1040-1047
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• 2012

본 논문에서는 소형 고정익기의 고장 발생시기와 부품 교체시기를 예측하여 유지보수 비용을 절감하고 정비 효율을 높이기 위하여 ANPSD와 PCA, 그리고 GC 방법을 이용하여 조종면의 고장에 대하여 이를 검출하고 위치와 정도를 분리하는 알고리즘을 제안하였다. 이때 ANPSD는 주파수 영역에서의 진동 분석을, PCA는 ANPSD의 중요 정보 추출을, GC는 고장 검출 및 분리 시의 오류 최소화를 위하여 사용되었다. 또한 모형 항공기에 가속도 센서를 부착하여 정상인 경우와 힌지 고장이 발생한 경우에 대하여 실제로 측정한 결과에 이와 같은 알고리즘을 적용한 결과 해당 알고리즘이 고장을 검출하고 분리하는 데에 적합함을 보였으며 제안된 알고리즘을 적용할 경우에 발생 가능한 문제들에 대하여 이를 완화할 수 있는 대응책을 함께 제시하였다.

• Tribology and Lubricants
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• 제17권4호
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• pp.267-275
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• 2001

Friction and wear properties of brake friction materials containing different metal fibers (Al, Cu or Steel fibers) were investigated. Based on a simple experimental formulation, friction materials with the same amount of metal fibers were tested using a pad-on-disk type friction tester. Two different materials (gray cast iron and aluminum metal matrix composite (MMC)) were used for disks rubbing against the friction materials. Results front ambient temperature tests revealed that the friction material containing Cu fibers sliding against gray cast iron disk showed a distinct negative $\mu$-v (friction coefficient vs. sliding velocity) relation implying possible stick-slip generation at low speeds. The negative $\mu$- v relation was not observed when the Cu-containing friction materials were rubbed against the Al-MMC counter surface. Elevated temperature tests showed that the friction level and the intensity of friction force oscillation were strongly affected by the thermal conductivity and melting temperature of metallic ingredients of the friction couple. Friction materials slid against cast iron disks exhibited higher friction coefficients than Al-MMC (metal matrix composite) disks during high temperature tests. On the other hand, high temperature test results suggested that copper fibers in the friction material improved fade resistance and that steel fibers were not compatible with Al-MMC disks showing severe material transfer and erratic friction behavior during sliding at elevated temperatures.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2009년도 제38회 동계학술대회 초록집
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• pp.277-277
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• 2010

The capacity of the carbonaceous materials reached ca. $350\;mAhg^{-1}$ which is close to theorestical value of the carbon intercalation composition $LiC_6$, resulting in a relatively low volumetric Li capacity. Notwithstanding the capacities of carbon, it will not adjust well to the need so future devices. Silicon shows the highest gravimetric capacities (up to $4000\;mAhg^{-1}$ for $Li_{21}Si_5$). Although Si is the most promising of the next generation anodes, it undergoes a large volume change during lithium insertion and extraction. It results in pulverization of the Si and loss of electrical contact between the Si and the current collector during the lithiation and delithiation. Thus, its capacity fades rapidly during cycling. We focused on electrode materials in the multiphase form which were composed of two metal compounds to reduce the volume change in material design. A combination of electrochemically amorphous active material in an inert matrix (Si-M) has been investigated for use as negative electrode materials in lithium ion batteries. The matrix composited of Si-M alloys system that; active material (Si)-inactive material (M) with Li; M is a transition metal that does not alloy with Li with Li such as Ti, V or Mo. We fabricated and tested a broad range of Si-M compositions. The electrodes were sputter-deposited on rough Cu foil. Electrochemical, structural, and compositional characterization was performed using various techniques. The structure of Si-M alloys was investigated using X-ray Diffractometer (XRD) and transmission electron microscopy (TEM). Surface morphologies of the electrodes are observed using a field emission scanning electron microscopy (FESEM). The electrochemical properties of the electrodes are studied using the cycling test and electrochemical impedance spectroscopy (EIS). It is found that the capacity is strongly dependent on Si content and cycle retention is also changed according to M contents. It may be beneficial to find materials with high capacity, low irreversible capacity and that do not pulverize, and that combine Si-M to improve capacity retention.

• 한국지반환경공학회 논문집
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• 제17권5호
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• pp.17-25
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• 2016

지표에 노출되는 암석은 기상작용 등의 영향으로 풍화가 가속되며, 풍화작용은 광물의 성질을 변화시켜 암석의 안정성을 저하시키게 되므로 암석의 풍화에 대한 저항은 광물의 조성을 파악하는 것이 중요하며 이는 풍화 민감도 분석을 통해 이루어진다. 따라서 본 연구에서는 시추된 시료에 대한 현미경 박편 시험을 실시하고 모드분석을 통해 풍화 취약광물의 구성비를 측정하였으며, 이를 통해 대상사면의 암석학적 광물학적 풍화요인을 평가하였다. 또한, X-Ray 회절분석을 이용하여 암석을 구성하는 실제적인 광물조성을 정량적으로 측정하고 주사현미경관찰을 통해 이차광물을 동정하여 풍화의 진행 정도를 파악하였다. 이러한 풍화 민감도 기법을 통하여 풍화 저항도를 판단할 수 있는 적절한 지시자를 결정할 수 있으며 화학적 풍화속도를 이용한 풍화등급의 예측이 가능할 것으로 분석되었다.